4-Acetyl-N,N-dimethylbenzamide
- Product Name
- 4-Acetyl-N,N-dimethylbenzamide
- CAS No.
- 1008119-09-2
- Chemical Name
- 4-Acetyl-N,N-dimethylbenzamide
- Synonyms
- 4-Acetyl-N,N-dimethylbenzamide;Benzamide, 4-acetyl-N,N-dimethyl-
- CBNumber
- CB53052605
- Molecular Formula
- C11H13NO2
- Formula Weight
- 191.23
- MOL File
- 1008119-09-2.mol
4-Acetyl-N,N-dimethylbenzamide Property
- Boiling point:
- 357.4±25.0 °C(Predicted)
- Density
- 1.084±0.06 g/cm3(Predicted)
- storage temp.
- Sealed in dry,Room Temperature
- pka
- -1.76±0.70(Predicted)
- Appearance
- White to off-white Solid
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- A192558
- Product name
- 4-Acetyl-N,N-dimethylbenzamide
- Packaging
- 250mg
- Price
- $330
- Updated
- 2021/12/16
- Product number
- 2435CZ
- Product name
- 4-Acetyl-N,N-dimethylbenzamide
- Packaging
- 250mg
- Price
- $168
- Updated
- 2021/12/16
- Product number
- 61-10929
- Product name
- 4-Acetyl-N,N-dimethylbenzamide
- Purity
- 95-98%
- Packaging
- 1g
- Price
- $180
- Updated
- 2021/12/16
- Product number
- A119200
- Product name
- 4-Acetyl-N,N-dimethylbenzamide
- Purity
- 98%
- Packaging
- 1g
- Price
- $189
- Updated
- 2021/12/16
- Product number
- A119200
- Product name
- 4-Acetyl-N,N-dimethylbenzamide
- Purity
- 98%
- Packaging
- 100mg
- Price
- $59
- Updated
- 2021/12/16
4-Acetyl-N,N-dimethylbenzamide Chemical Properties,Usage,Production
Synthesis
586-89-0
68-12-2
1008119-09-2
To a 50 mL pressure-resistant reaction tube (equipped with a PTFE high-pressure valve) equipped with a magnetic stirrer was sequentially added Cu(OTf)2 (0.05 mmol), 4-acetylbenzoic acid (0.5 mmol), N,N-dimethylformamide (2.0 mmol), di-tert-butyl peroxide (DTBP, 1 mmol) and 1,2-dichloroethane (DCE, 1 mL). The reaction mixture was stirred at 130 °C for 12 h and subsequently cooled to room temperature. The reaction mixture was diluted with ethyl acetate and filtered through a diatomaceous earth pad. The filtrate was washed sequentially with saturated aqueous sodium bicarbonate (5 mL) and saturated saline (5 mL x 2). The organic phase was dried over anhydrous sodium sulfate and concentrated under reduced pressure. The residue was purified by preparative thin layer chromatography (TLC) on silica gel to afford the target product 4-acetyl-N,N-dimethylbenzamide.
References
[1] Chinese Chemical Letters, 2015, vol. 26, # 1, p. 11 - 14
4-Acetyl-N,N-dimethylbenzamide Preparation Products And Raw materials
Raw materials
Preparation Products
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