ETHYL 4-CHLORO-3-NITROBENZOATE

Product Name: ETHYL 4-CHLORO-3-NITROBENZOATE
CAS No.: 16588-16-2
Chemical Name: ETHYL 4-CHLORO-3-NITROBENZOATE
Synonyms: RARECHEM AL BI 0170;4-CHLORO-3-NITROBENZOATE;ETHYL 4-CHLORO-3-NITROBENZOATE;Ethyl 4-chloro-3-nitrobenzoate,98%;4-CHLORO-3-NITROBENZOIC ACID ETHYL ESTER;Benzoic acid, 4-chloro-3-nitro-, ethyl ester
CBNumber: CB5314937
Molecular Formula: C9H8ClNO4
Formula Weight: 229.62
MOL File: 16588-16-2.mol

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ETHYL 4-CHLORO-3-NITROBENZOATE Property

Melting point:: 57-61 °C
Boiling point:: 326.2±22.0 °C(Predicted)
Density: 1.369±0.06 g/cm3(Predicted)
storage temp.: Sealed in dry,Room Temperature
Appearance: White to yellow Solid
CAS DataBase Reference: 16588-16-2(CAS DataBase Reference)

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Safety

Hazard Codes: Xi
Risk Statements: 36/37/38
Safety Statements: 37/39-26
HS Code: 2921490090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P405Store locked up.

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N-Bromosuccinimide Price

TRC

Product number: E903780
Product name: Ethyl4-Chloro-3-nitrobenzoate
Packaging: 250mg
Price: $45
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FC71000
Product name: 4-Chloro-3-nitrobenzoic acid ethyl ester
Packaging: 50g
Price: $40
Updated: 2021/12/16

AK Scientific

Product number: 8428AA
Product name: Ethyl4-chloro-3-nitrobenzoate
Packaging: 1g
Price: $14
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FC71000
Product name: 4-Chloro-3-nitrobenzoic acid ethyl ester
Packaging: 250g
Price: $150
Updated: 2021/12/16

Matrix Scientific

Product number: 130500
Product name: 4-Chloro-3-nitro-benzoicacidethylester
Purity: 95%+
Packaging: 5g
Price: $152
Updated: 2021/12/16

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ETHYL 4-CHLORO-3-NITROBENZOATE Chemical Properties,Usage,Production

Chemical Properties

pale yellow crystalline powder

Synthesis

96-99-1

16588-16-2

Step 1: Preparation of ethyl 4-chloro-3-nitrobenzoate 4-Chloro-3-nitrobenzoic acid (300 g) was dissolved in ethanol (1500 mL) and concentrated sulfuric acid (100 mL) was added slowly under ice bath cooling. The reaction mixture was heated to reflux for 7 hours. After completion of the reaction, the mixture was poured into ice water and the precipitated crystals were collected by filtration to afford the target product ethyl 4-chloro-3-nitrobenzoate (332 g, 97% yield). 1H-NMR (300 MHz, CDCl3): δ 8.50 (1H, d, J = 2.1 Hz), 8.16 (1H, dd, J = 8.4, 2.1 Hz), 7.63 (1H, d, J = 8.4 Hz), 4.43 (2H, q, J = 7.5 Hz), 1.42 (3H, t, J = 7.5 Hz).

References

[1] Patent: US2003/50320, 2003, A1
[2] Patent: WO2004/29050, 2004, A1. Location in patent: Page 105;106
[3] Synthetic Communications, 2002, vol. 32, # 11, p. 1703 - 1707
[4] Patent: US6204264, 2001, B1

ETHYL 4-CHLORO-3-NITROBENZOATE Preparation Products And Raw materials

Raw materials

Preparation Products

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ETHYL 4-CHLORO-3-NITROBENZOATE Suppliers

Belgium 1 China 66 Germany 4 India 5 Switzerland 1 Ukraine 1 United Kingdom 10 United States 14 Global 102

Alfa Aesar

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Heterochem

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Thermo Fisher Scientific

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9ding chemical ( Shanghai) Limited

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View Lastest Price from ETHYL 4-CHLORO-3-NITROBENZOATE manufacturers

Career Henan Chemical Co

Product: ETHYL 4-CHLORO-3-NITROBENZOATE 16588-16-2
Price: US $1.00/g
Min. Order: 1g
Purity: 99%
Supply Ability: 10000KGS
Release date: 2020-01-11

16588-16-2, ETHYL 4-CHLORO-3-NITROBENZOATERelated Search:

4-Chloro-3-nitrobenzoic acid ETHYL 2-CHLORO-5-NITROBENZOATE ETHYL 2-CHLORO-3-NITROBENZOATE ethyl 4-chloro-2-nitrobenzoate Dodecyl 4-chloro-3-nitrobenzoate 4-CHLORO-3,5-DINITRO-BENZOIC ACID BUTYL ESTER 3-(1-[(4-CHLORO-3-NITROBENZOYL)OXY]ETHYL)-1-[2-(4-NITROPHENYL)-2-OXOETHYL]PYRIDINIUM BROMIDE 4-Chloro-3-nitro-1,8-naphthalic anhydride AURORA 17317 SPECS AC-907/25004921 ETHYL 4-CHLORO-3-NITROBENZOATE 4-CHLORO-3,5-DINITRO-BENZOIC ACID ISOBUTYL ESTER (1-BENZYL-5-NITRO-1H-INDOL-3-YL)METHYL 4-CHLORO-3-NITROBENZOATE 2-(4-CHLOROPHENYL)-2-OXOETHYL 4-CHLORO-3-NITROBENZOATE 9-METHYL-5-OXO-6-PHENYL-2,3-DIHYDRO-1H,5H-PYRIDO[3,2,1-IJ]QUINOLIN-7-YL 4-CHLORO-3-NITROBENZOATE

RARECHEM AL BI 0170

ETHYL 4-CHLORO-3-NITROBENZOATE

4-CHLORO-3-NITROBENZOIC ACID ETHYL ESTER

Ethyl 4-chloro-3-nitrobenzoate,98%

4-CHLORO-3-NITROBENZOATE

Benzoic acid, 4-chloro-3-nitro-, ethyl ester

16588-16-2

C9H8NO4Cl

Aromatic Esters