2-HYDRAZINOQUINOLINE
- Product Name
- 2-HYDRAZINOQUINOLINE
- CAS No.
- 15793-77-8
- Chemical Name
- 2-HYDRAZINOQUINOLINE
- Synonyms
- AKOS AUF02055;2-QUINOLYLHYDRAZINE;2-HYDRAZINOQUINOLINE;2-HYDRAZINEQUINOLINE;OTAVA-BB BB0138210067;2-hydrazinylquinoline;QUINOLIN-2-YL-HYDRAZINE;QUINOLINE, 2-HYDRAZINO-;alpha-Quinolylhydrazine;2-Hydrazinoquinoline>
- CBNumber
- CB5329001
- Molecular Formula
- C9H9N3
- Formula Weight
- 159.19
- MOL File
- 15793-77-8.mol
2-HYDRAZINOQUINOLINE Property
- Melting point:
- 142°C
- Boiling point:
- 303.1±45.0 °C(Predicted)
- Density
- 1.25±0.1 g/cm3(Predicted)
- storage temp.
- Keep in dark place,Inert atmosphere,Store in freezer, under -20°C
- solubility
- Soluble in methanol.
- pka
- 5.41±0.20(Predicted)
- form
- powder to crystal
- color
- Light yellow to Brown
- CAS DataBase Reference
- 15793-77-8(CAS DataBase Reference)
- EPA Substance Registry System
- 2(1H)-Quinolinone, hydrazone (15793-77-8)
Safety
- Hazard Codes
- Xn
- Risk Statements
- 20/21/22-36/37/38-41-22
- Safety Statements
- 26-36/37/39-39
- TSCA
- Yes
- HS Code
- 2933491090
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P270Do not eat, drink or smoke when using this product.
P271Use only outdoors or in a well-ventilated area.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P405Store locked up.
P501Dispose of contents/container to..…
N-Bromosuccinimide Price
- Product number
- H0178
- Product name
- 2-Hydrazinoquinoline
- Purity
- >98.0%(HPLC)(T)
- Packaging
- 1g
- Price
- $98
- Updated
- 2025/07/31
- Product number
- H0178
- Product name
- 2-Hydrazinoquinoline
- Purity
- >98.0%(HPLC)(T)
- Packaging
- 5g
- Price
- $285
- Updated
- 2025/07/31
- Product number
- H0178
- Product name
- 2-Hydrazinoquinoline
- Purity
- >98.0%(HPLC)(T)
- Packaging
- 25g
- Price
- $897
- Updated
- 2025/07/31
- Product number
- H716523
- Product name
- 2-Hydrazinylquinoline
- Packaging
- 500mg
- Price
- $65
- Updated
- 2021/12/16
- Product number
- CHM0020927
- Product name
- 2-HYDRAZINOQUINOLINE
- Purity
- 95.00%
- Packaging
- 1G
- Price
- $692.46
- Updated
- 2021/12/16
2-HYDRAZINOQUINOLINE Chemical Properties,Usage,Production
Uses
2-Hydrazinoquinoline acts as as a derivatization agent for LC-MS-based metabolomic investigation of diabetic ketoacidosis. It is used in agrochemical, pharmaceutical and dyestuff field.
Synthesis
612-62-4
15793-77-8
The general procedure for the synthesis of 2-hydrazinoquinoline from 2-chloroquinoline was as follows: 21.0 g (128.4 mmol) of 2-chloroquinoline was first dissolved in 210 mL of ethanol. Subsequently, 64.3 g (1.3 mol) of hydrazine hydrate was added and the reaction mixture was stirred under reflux conditions for 16 hours. Upon completion of the reaction, the mixture was cooled to 0 °C and the precipitated solid product was collected by filtration and washed with a small amount of ethanol. After initial drying, the product was further dried under high vacuum. Finally, 14.5 g of product was obtained in 71% yield. The product was analyzed by LC-MS (Method 1): retention time Rt = 1.95 min; mass spectrum (ESIpos): m/z = 160 [M + H]+; 1H-NMR (400 MHz, DMSO-d6) data were as follows: δ= 8.08 (broad peaks, 1H), 7.87 (double peaks, 1H), 7.63 (double peaks, 1H), 7.57-7.43 (multiple peaks, 2H), 7.16 (triple peaks, 1H), 6.85 (double peaks, 1H), 4.35 (broad peaks, 2H).
References
[1] Patent: US2012/264704, 2012, A1. Location in patent: Page/Page column 17
[2] Journal of the Chemical Society, 1913, vol. 103, p. 1981
[3] Journal of the Indian Chemical Society, 1981, vol. 58, p. 840 - 843
[4] Spectrochimica Acta - Part A: Molecular and Biomolecular Spectroscopy, 2006, vol. 65, # 2, p. 463 - 466
[5] Spectrochimica Acta - Part A: Molecular and Biomolecular Spectroscopy, 2007, vol. 66, # 4-5, p. 972 - 975
2-HYDRAZINOQUINOLINE Preparation Products And Raw materials
Raw materials
Preparation Products
2-HYDRAZINOQUINOLINE Suppliers
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View Lastest Price from 2-HYDRAZINOQUINOLINE manufacturers
- Product
- 2-HYDRAZINOQUINOLINE 15793-77-8
- Price
- US $0.00/KG
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- 20 tons
- Release date
- 2021-10-14
- Product
- 2-HYDRAZINOQUINOLINE 15793-77-8
- Price
- US $1.00/KG
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- Kg/T
- Release date
- 2019-12-19