Synthesis
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1-PHENYLNAPHTHALENE

Synthesis
Product Name
1-PHENYLNAPHTHALENE
CAS No.
605-02-7
Chemical Name
1-PHENYLNAPHTHALENE
Synonyms
1-naphthylbenzene;1-PHENYLNAPHTHALENE;α-Phenylnaphthalene;1-Phenylnaphthalene>1-Phenylnaphthalene,96%;1-Phenylnaphthalene 96%;1-Phenylnaphthalene,97%;1-Phenylnaphthalene, ≥ 95.0%;1-Phenylnaphthalene 100mg [605-02-7];1-Phenylnaphthalene@50 μg/mL in Toluene
CBNumber
CB5342871
Molecular Formula
C16H12
Formula Weight
204.27
MOL File
605-02-7.mol
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1-PHENYLNAPHTHALENE Property

Melting point:
45°C
Boiling point:
324-325 °C (lit.)
Density 
1.085 g/mL at 25 °C (lit.)
refractive index 
n20/D 1.664(lit.)
Flash point:
>230 °F
storage temp. 
Sealed in dry,Room Temperature
form 
clear liquid
color 
Light orange to Yellow to Green
BRN 
1906885
CAS DataBase Reference
605-02-7(CAS DataBase Reference)
EPA Substance Registry System
1-Phenylnaphthalene (605-02-7)
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Safety

Safety Statements 
24/25
WGK Germany 
3
HS Code 
2902.90.9000
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Hazard and Precautionary Statements (GHS)

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N-Bromosuccinimide Price

Sigma-Aldrich
Product number
P27402
Product name
1-Phenylnaphthalene
Purity
96%
Packaging
5g
Price
$105
Updated
2024/03/01
TCI Chemical
Product number
P0632
Product name
1-Phenylnaphthalene
Purity
>97.0%(GC)
Packaging
5g
Price
$186
Updated
2024/03/01
Alfa Aesar
Product number
B21953
Product name
1-Phenylnaphthalene, 97%
Packaging
5g
Price
$62.65
Updated
2024/03/01
Alfa Aesar
Product number
B21953
Product name
1-Phenylnaphthalene, 97%
Packaging
25g
Price
$206.65
Updated
2024/03/01
Alfa Aesar
Product number
B21953
Product name
1-Phenylnaphthalene, 97%
Packaging
100g
Price
$751.65
Updated
2024/03/01
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1-PHENYLNAPHTHALENE Chemical Properties,Usage,Production

Synthesis


To a suspension of potassium phenyltriflfluoroborate (92.3 mg, 0.5 mmol), 1-bromonapthalene (103.5 mg, 0.5 mmol), and K2CO3 (204.5 mg, 1. 5 mmol) in MeOH  (0.75 mL) was added Pd(OAc)2 in methanol (1.25 mL, 2 × 10–3 M) and then the reaction mixture was stirred and heated at reflflux for 2 h. The mixture was cooled to room temperature and diluted with water (10 mL). The aqueous phase was extracted with CH2Cl2 (3 × 4 mL). The combined organic extracts were washed with brine (10 mL) and dried (MgSO4). The crude product was then purifified via chromatography (silica gel) eluting with hexane to deliver 76.1 mg (75%) of 1-phenylnaphthalene. Reference: Molander, G. A.; Biolatto, B. J. Org. Chem. 2003, 68, 4302−4314.

Chemical Properties

Clear colorless to yellow viscous liquid

Synthesis Reference(s)

Journal of the American Chemical Society, 101, p. 2246, 1979 DOI: 10.1021/ja00502a074
Organic Syntheses, Coll. Vol. 3, p. 729, 1955

1-PHENYLNAPHTHALENE Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 1-PHENYLNAPHTHALENE manufacturers

hebei hongtan Biotechnology Co., Ltd
Product
1-PHENYLNAPHTHALENE 605-02-7
Price
US $30.00/kg
Min. Order
1kg
Purity
98%
Supply Ability
2000kg
Release date
2024-03-26
Hebei Yanxi Chemical Co., Ltd.
Product
1-PHENYLNAPHTHALENE 605-02-7
Price
US $50.00-15.00/kg
Min. Order
1kg
Purity
0.99
Supply Ability
20 tons
Release date
2023-09-27
Hebei Mojin Biotechnology Co., Ltd
Product
1-PHENYLNAPHTHALENE 605-02-7
Price
US $0.00/KG
Min. Order
1KG
Purity
99%
Supply Ability
50000KG/month
Release date
2023-11-22

605-02-7, 1-PHENYLNAPHTHALENERelated Search:


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