5-Bromo-2,3-dihydro-1H-inden-1-amine
- Product Name
- 5-Bromo-2,3-dihydro-1H-inden-1-amine
- CAS No.
- 185122-74-1
- Chemical Name
- 5-Bromo-2,3-dihydro-1H-inden-1-amine
- Synonyms
- 5-BROMO-2,3-DIHYDRO-1H-INDEN-1-AMINE;5-BROMO-2,3-DIHYDRO-1H-INDEN-1-AMINE HYDROCHLORIDE;5-bromoindan-1-amine;5-BROMO-INDAN-1-YLAMINE;5-bromo-2,3-dihydro-1H-indene-1-amine;1H-INDEN-1-AMINE, 5-BROMO-2,3-DIHYDRO-
- CBNumber
- CB5359459
- Molecular Formula
- C9H10BrN
- Formula Weight
- 212.09
- MOL File
- 185122-74-1.mol
5-Bromo-2,3-dihydro-1H-inden-1-amine Property
- Boiling point:
- 278.2±40.0 °C(Predicted)
- Density
- 1.490±0.06 g/cm3(Predicted)
- storage temp.
- 2-8°C(protect from light)
- pka
- 9.05±0.20(Predicted)
- InChI
- InChI=1S/C9H10BrN/c10-7-2-3-8-6(5-7)1-4-9(8)11/h2-3,5,9H,1,4,11H2
- InChIKey
- IEUKCNPRRGOGDG-UHFFFAOYSA-N
- SMILES
- C1(N)C2=C(C=C(Br)C=C2)CC1
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- FB164681
- Product name
- 5-Bromo-2,3-dihydro-1H-inden-1-amine
- Packaging
- 100mg
- Price
- $160
- Updated
- 2021/12/16
- Product number
- FB164681
- Product name
- 5-Bromo-2,3-dihydro-1H-inden-1-amine
- Packaging
- 250mg
- Price
- $250
- Updated
- 2021/12/16
- Product number
- FB164681
- Product name
- 5-Bromo-2,3-dihydro-1H-inden-1-amine
- Packaging
- 500mg
- Price
- $400
- Updated
- 2021/12/16
- Product number
- FB164681
- Product name
- 5-Bromo-2,3-dihydro-1H-inden-1-amine
- Packaging
- 50mg
- Price
- $100
- Updated
- 2021/12/16
- Product number
- FB164681
- Product name
- 5-Bromo-2,3-dihydro-1H-inden-1-amine
- Packaging
- 1g
- Price
- $600
- Updated
- 2021/12/16
5-Bromo-2,3-dihydro-1H-inden-1-amine Chemical Properties,Usage,Production
Synthesis
To a solution of 5-bromo-2,3-dihydro-1H-inden-1-one (100 g, 474 mmol, 1.00 equiv) in methanol (1.5 L) was added ammonium formate (300 g, 4.76 mol, 10.0 equiv). After stirring for 1 h, NaBH3CN (90 g, 1.43 mol, 3.02 equiv) was added. The mixture was heated at 60 ℃ for 2 h, concentrated under reduced pressure, and purified by silica gel chromatography (EA/PE, 1/10) to afford 64 g (64%) of 5-Bromo-2,3-dihydro-1H-inden-1-amine as a brown solid.
5-Bromo-2,3-dihydro-1H-inden-1-amine Preparation Products And Raw materials
Raw materials
Preparation Products
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