5-IODO-1,2,3-TRIMETHOXYBENZENE
- Product Name
- 5-IODO-1,2,3-TRIMETHOXYBENZENE
- CAS No.
- 25245-29-8
- Chemical Name
- 5-IODO-1,2,3-TRIMETHOXYBENZENE
- Synonyms
- 3,4,5-Trimethoxyiodobenzene;1-jodo-3,4,5-trimetoxibensen;1-Iodo-3,4,5-Trimethoxybenzene;5-IODO-1,2,3-TRIMETHOXYBENZENE;Benzene, 5-iodo-1,2,3-trimethoxy-;5-IODO-1,2,3-TRIMETHOXYBENZENE, 98+%
- CBNumber
- CB5418479
- Molecular Formula
- C9H11IO3
- Formula Weight
- 294.09
- MOL File
- 25245-29-8.mol
5-IODO-1,2,3-TRIMETHOXYBENZENE Property
- Melting point:
- 85-87°C
- Boiling point:
- 312.6±42.0 °C(Predicted)
- Density
- 1.602±0.06 g/cm3(Predicted)
- storage temp.
- Keep in dark place,Sealed in dry,Room Temperature
- form
- solid
- color
- Pale yellow
- Water Solubility
- Insoluble in water.
- Sensitive
- Light Sensitive
- BRN
- 1529690
Safety
- Hazard Codes
- Xi
- Risk Statements
- 36/37/38-43
- Safety Statements
- 24/25-36/37-26
- WGK Germany
- 3
- Hazard Note
- Irritant
- HS Code
- 29093090
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H317May cause an allergic skin reaction
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P271Use only outdoors or in a well-ventilated area.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P302+P352IF ON SKIN: wash with plenty of soap and water.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- 711535
- Product name
- 5-Iodo-1,2,3-trimethoxybenzene
- Purity
- ≥97.0% (GC)
- Packaging
- 5g
- Price
- $237
- Updated
- 2024/03/01
- Product number
- 711535
- Product name
- 5-Iodo-1,2,3-trimethoxybenzene
- Purity
- ≥97.0% (GC)
- Packaging
- 1g
- Price
- $97.7
- Updated
- 2023/06/20
- Product number
- T4144
- Product name
- 5-Iodo-1,2,3-trimethoxybenzene
- Purity
- min. 95.0 %
- Packaging
- 1G
- Price
- $131
- Updated
- 2025/07/31
- Product number
- T4144
- Product name
- 5-Iodo-1,2,3-trimethoxybenzene
- Purity
- min. 95.0 %
- Packaging
- 5G
- Price
- $392
- Updated
- 2025/07/31
- Product number
- 2608-H-01
- Product name
- 5-Iodo-1,2,3-trimethoxybenzene
- Packaging
- 5G
- Price
- $256
- Updated
- 2021/12/16
5-IODO-1,2,3-TRIMETHOXYBENZENE Chemical Properties,Usage,Production
Uses
5-Iodo-1,2,3-trimethoxybenzene is used as a primary and secondary intermediate in organic synthesis.
Synthesis
1017601-55-6
25245-29-8
GENERAL METHOD: Trifluoroborate (1 mmol) was dissolved in 3 mL of a mixture of DMF and water (2:1 volume ratio) and cesium triiodide (1 mmol) was added. The reaction mixture was stirred at 80 °C until the reaction was complete (see Table 3 for reaction times). After completion of the reaction, the reaction solution was diluted with 10 mL of ether. The aqueous layer was extracted twice with ether (5 mL), and the organic phases were combined and dried with anhydrous Na2SO4. After evaporation of the solvent, the residue was purified by silica gel column chromatography [eluent: solvent mixture of hexane (or pentane) and ethyl acetate (or ether)].
References
[1] Tetrahedron, 2012, vol. 68, # 19, p. 3738 - 3743
5-IODO-1,2,3-TRIMETHOXYBENZENE Preparation Products And Raw materials
Raw materials
Preparation Products
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