METHYL 6-CHLORO-1H-INDAZOLE-3-CARBOXYLATE
- Product Name
- METHYL 6-CHLORO-1H-INDAZOLE-3-CARBOXYLATE
- CAS No.
- 717134-47-9
- Chemical Name
- METHYL 6-CHLORO-1H-INDAZOLE-3-CARBOXYLATE
- Synonyms
- METHYL 6-CHLORO-1H-INDAZOLE-3-CARBOXYLATE;6-Chloro-1H-indazole-3-carboxylic acid Methyl ester;1H-Indazole-3-carboxylic acid, 6-chloro-, methyl ester
- CBNumber
- CB5471029
- Molecular Formula
- C9H7ClN2O2
- Formula Weight
- 210.62
- MOL File
- 717134-47-9.mol
METHYL 6-CHLORO-1H-INDAZOLE-3-CARBOXYLATE Property
- Boiling point:
- 378.7±22.0 °C(Predicted)
- Density
- 1.453±0.06 g/cm3(Predicted)
- storage temp.
- Sealed in dry,Room Temperature
- pka
- 10.75±0.40(Predicted)
- Appearance
- White to off-white Solid
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P271Use only outdoors or in a well-ventilated area.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P302+P352IF ON SKIN: wash with plenty of soap and water.
P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P312Call a POISON CENTER or doctor/physician if you feel unwell.
P321Specific treatment (see … on this label).
P332+P313IF SKIN irritation occurs: Get medical advice/attention.
P337+P313IF eye irritation persists: Get medical advice/attention.
P362Take off contaminated clothing and wash before reuse.
P403+P233Store in a well-ventilated place. Keep container tightly closed.
P405Store locked up.
P501Dispose of contents/container to..…
N-Bromosuccinimide Price
- Product number
- B499200
- Product name
- methyl6-chloro-1H-indazole-3-carboxylate
- Packaging
- 100mg
- Price
- $60
- Updated
- 2021/12/16
- Product number
- HCH0353840
- Product name
- METHYL-6-CHLORO-1H-INDAZOLE-3-CARBOXYLATE
- Purity
- 95.00%
- Packaging
- 5MG
- Price
- $499.79
- Updated
- 2021/12/16
- Product number
- Y5535
- Product name
- Methyl6-chloro-1H-indazole-3-carboxylate
- Packaging
- 5g
- Price
- $651
- Updated
- 2021/12/16
- Product number
- Y5535
- Product name
- Methyl6-chloro-1H-indazole-3-carboxylate
- Packaging
- 250mg
- Price
- $131
- Updated
- 2021/12/16
- Product number
- Y5535
- Product name
- Methyl6-chloro-1H-indazole-3-carboxylate
- Packaging
- 25g
- Price
- $2456
- Updated
- 2021/12/16
METHYL 6-CHLORO-1H-INDAZOLE-3-CARBOXYLATE Chemical Properties,Usage,Production
Synthesis
717134-46-8
717134-47-9
General procedure for the synthesis of methyl 6-chloro-1H-indazole-3-carboxylate from the compound (CAS: 717134-46-8): to a stirred solution of methyl (2-acetamido-4-chlorophenyl)acetate (32.0 g, 133 mmol) in acetic acid (200 mL), tert-butyl nitrite (20.5 mL, 172.3) was slowly added dropwise at 90 °C. mmol), and the dropwise addition time was controlled at 1 hour. Upon completion of the reaction, the reaction mixture was poured into water (1.4 L) and the solid product was recovered by filtration. The resulting yellow precipitate was dissolved in ethyl acetate (EtOAc) and subsequently washed with saturated sodium chloride (NaCl) solution. The organic phase was dried with anhydrous magnesium sulfate (MgSO?), filtered and concentrated to obtain a solid. Finally, the solid was ground with hexane and filtered to afford the target product methyl 6-chloro-1H-indazole-3-carboxylate (21.63 g, 77% yield).
References
[1] Patent: WO2004/56806, 2004, A1. Location in patent: Page 37
METHYL 6-CHLORO-1H-INDAZOLE-3-CARBOXYLATE Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from METHYL 6-CHLORO-1H-INDAZOLE-3-CARBOXYLATE manufacturers
- Product
- METHYL 6-CHLORO-1H-INDAZOLE-3-CARBOXYLATE 717134-47-9
- Price
- US $9.80/KG
- Min. Order
- 1g
- Purity
- ≥99%
- Supply Ability
- 100kg
- Release date
- 2020-01-13