ChemicalBook > CAS DataBase List > 2,6-DIBROMONAPHTHALENE

2,6-DIBROMONAPHTHALENE

Product Name
2,6-DIBROMONAPHTHALENE
CAS No.
13720-06-4
Chemical Name
2,6-DIBROMONAPHTHALENE
Synonyms
DibroMonaphthalene;2,6-DibromonaphthaL;2,6-dibroMophthalene;2,6-Dibromonapthalene;2,6-DIBROMONAPHTHALENE;Naphthalene, 2,6-dibroMo-;2,6-Dibromonaphthalene>2,6-Dibromonaphthalene 99%;2,6-DIBROMONAPHTHALENE, 98.5%;2,6-DIBROMONAPHTHALENE 13720-06-4
CBNumber
CB5697353
Molecular Formula
C10H6Br2
Formula Weight
285.96
MOL File
13720-06-4.mol
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2,6-DIBROMONAPHTHALENE Property

Melting point:
163-166°C
Boiling point:
339.1±15.0 °C(Predicted)
Density 
1.834±0.06 g/cm3(Predicted)
storage temp. 
Sealed in dry,Room Temperature
form 
powder to crystal
color 
White to Gray to Brown
Water Solubility 
Insoluble in water.
InChI
InChI=1S/C10H6Br2/c11-9-3-1-7-5-10(12)4-2-8(7)6-9/h1-6H
InChIKey
PJZDEYKZSZWFPX-UHFFFAOYSA-N
SMILES
C1=C2C(C=C(Br)C=C2)=CC=C1Br
CAS DataBase Reference
13720-06-4(CAS DataBase Reference)
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Safety

Hazard Codes 
Xi,N
Risk Statements 
37/38-41-51/53
Safety Statements 
22-24/25-61-39-26
RIDADR 
UN 3077 9 / PGIII
WGK Germany 
3
HS Code 
29039990
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Danger
Hazard statements

H315Causes skin irritation

H318Causes serious eye damage

H335May cause respiratory irritation

H411Toxic to aquatic life with long lasting effects

Precautionary statements

P273Avoid release to the environment.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P302+P352IF ON SKIN: wash with plenty of soap and water.

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N-Bromosuccinimide Price

Sigma-Aldrich
Product number
762652
Product name
2,6-Dibromonaphthalene
Purity
97%
Packaging
1g
Price
$65.4
Updated
2024/03/01
TCI Chemical
Product number
D4154
Product name
2,6-Dibromonaphthalene
Purity
>98.0%(GC)
Packaging
1g
Price
$55
Updated
2024/03/01
Alfa Aesar
Product number
L16134
Product name
2,6-Dibromonaphthalene, 99%
Packaging
1g
Price
$60.65
Updated
2024/03/01
Alfa Aesar
Product number
L16134
Product name
2,6-Dibromonaphthalene, 99%
Packaging
5g
Price
$213.65
Updated
2024/03/01
Alfa Aesar
Product number
L16134
Product name
2,6-Dibromonaphthalene, 99%
Packaging
25g
Price
$832.65
Updated
2024/03/01
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2,6-DIBROMONAPHTHALENE Chemical Properties,Usage,Production

Description

2,6-Dibromonaphthalene is an important material intermediate compound used as building blocks to construct small semiconductor molecules or polymers in organic photovoltaic, OLED and OFET devices.

Chemical Properties

Light yellow solid

Uses

2,6-Dibromonaphthalene is an important raw material and intermediate used in organic synthesis, pharmaceuticals and agrochemicals. It reacts with hexylmagnesium bromide to form 2,6-Dihexyl-naphthalene.

Synthesis

2,6-Dibromonaphthalene is synthesised using 6-Bromo-2-naphthol as a raw material by chemical reaction. The specific synthesis steps are as follows:
Bromine (78.8 g, 493 mmol) was added dropwise to a cooled (0 °C) solution of triphenylphosphine (129 g, 493 mmol) in anhydrous CH3CN (200 mL) and the solution was stirred for 30 min at rt. A solution of 6-bromo-2-naphthol (100 g, 448 mmol) in anhydrous acetonitrile (CH3CN) (200 mL) was added, and the reaction mixture was stirred for a further 2 h at 70 °C. After removal of the solvent (bath temp was increased to 140 °C), the residue was heated to 300 °C for 1 h. After being cooled to 100 °C, the black tar was dissolved in toluene (100 mL), and cooled to rt while stirring. The resulting solution was washed with 1 N NaOH and water, followed by drying over MgSO4. The solvent was removed in vacuo and the residue was dissolved in MeOH (50 mL). The precipitate was filtered and washed with MeOH (200 mL) and diisopropylether (iPr2O), successively, to give 2 (37.2 g, 29%) as a grey powder. The analytical sample was obtained by recrystallization from AcOEt (light brown plates). 1H NMR (CDCl3) δ: 7.51-7.62 (4H, m), 7.94 (2H, s). IR (KBr): 1568, 1481, 1175, 1134, 1065, 885, 853, 816 cm-1. Anal. Calcd for C10H6Br2: C, 42.00; H, 2.11. Found: C, 42.28; H, 2.18.

2,6-DIBROMONAPHTHALENE Preparation Products And Raw materials

Raw materials

Preparation Products

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2,6-DIBROMONAPHTHALENE Suppliers

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View Lastest Price from 2,6-DIBROMONAPHTHALENE manufacturers

Henan Fengda Chemical Co., Ltd
Product
2,6-DIBROMONAPHTHALENE 13720-06-4
Price
US $100.00-1.00/KG
Min. Order
1KG
Purity
99%
Supply Ability
g-kg-tons, free sample is available
Release date
2023-12-26
Hebei Duling International Trade Co. LTD
Product
2,6-DIBROMONAPHTHALENE 13720-06-4
Price
US $20.00/kg
Min. Order
1kg
Purity
99%
Supply Ability
5000 tons
Release date
2023-01-16
Hebei Yanxi Chemical Co., Ltd.
Product
2,6-DIBROMONAPHTHALENE 13720-06-4
Price
US $20.00-1.00/kg
Min. Order
1kg
Purity
0.99
Supply Ability
10 tons
Release date
2023-11-29

13720-06-4, 2,6-DIBROMONAPHTHALENERelated Search:

6,7-DIBROMONAPHTHALENE-2,3-DICARBONITRILE 1,5-DIHYDROXY-2,6-DIBROMONAPHTHALENE,2,6-dibromonaphthalene-1,5-dio 6,12-Dibromochrysene 2,6-DIBROMONAPHTHALENE 2-Hydroxy-1,6-dibromonaphthalene 1,8-DIBROMONAPHTALENE (S)-(-)-3,3'-DIBROMO-1,1'-BI-2-NAPHTHOL 1,4-dibromonaphthalene 2,3-DIBROMONAPHTHALENE 1,2-Dibromonaphthalene 2,7-DIBROMONAPHTHALENE, 98.0+%(GC),2,7-DIBROMONAPHTHALENE 1,3-Dibromonaphthalene-2-ol 1,7-Dibromonaphthalene 4,8-diamino-2,6-dibromonaphthalene-1,5-diol 1,6-Dibromonaphthalene 1,3-Dibromonaphthalene 2,6-DIBROMO-1,5-DIMETHOXYNAPHTHALENE 2,3,6,7-TETRABROMONAPHTHALENE

  • 2,6-DIBROMONAPHTHALENE
  • 2,6-DIBROMONAPHTHALENE, 98.5%
  • 2,6-Dibromonapthalene
  • Naphthalene, 2,6-dibroMo-
  • DibroMonaphthalene
  • 2,6-dibroMophthalene
  • 2,6-Dibromonaphthalene 99%
  • 2,6-Dibromonaphthalene&gt
  • 2,6-DibromonaphthaL
  • 2,6-DIBROMONAPHTHALENE ISO 9001：2015 REACH
  • 2,6-DIBROMONAPHTHALENE 13720-06-4
  • 13720-06-4
  • Dibromonaphthalene