4-MORPHOLIN-4-YL-BUTAN-1-OL
- Product Name
- 4-MORPHOLIN-4-YL-BUTAN-1-OL
- CAS No.
- 5835-79-0
- Chemical Name
- 4-MORPHOLIN-4-YL-BUTAN-1-OL
- Synonyms
- AKOS BB/0085;AKOS BBB/436;CHEMBRDG-BB 4001148;4-Morpholinebutanol;4-Morpholino-1-butanol;4-Morpholinobutan-1-ol;4-MORPHOLIN-4-YL-BUTAN-1-OL;4-morpholin-4-ylbutan-1-ol(SALTDATA: FREE)
- CBNumber
- CB5838471
- Molecular Formula
- C8H17NO2
- Formula Weight
- 159.23
- MOL File
- 5835-79-0.mol
4-MORPHOLIN-4-YL-BUTAN-1-OL Property
- storage temp.
- 2-8°C
Safety
- Hazard Codes
- Xi
- HazardClass
- IRRITANT
- HS Code
- 2934999090
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P302+P352IF ON SKIN: wash with plenty of soap and water.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P321Specific treatment (see … on this label).
P332+P313IF SKIN irritation occurs: Get medical advice/attention.
P362Take off contaminated clothing and wash before reuse.
N-Bromosuccinimide Price
- Product number
- M732733
- Product name
- 4-(4-Morpholinyl)-1-butanol
- Packaging
- 100mg
- Price
- $65
- Updated
- 2021/12/16
- Product number
- M732733
- Product name
- 4-(4-Morpholinyl)-1-butanol
- Packaging
- 1g
- Price
- $330
- Updated
- 2021/12/16
- Product number
- OR963360
- Product name
- 4-(4-Morpholinyl)-1-butanol
- Purity
- 95%
- Packaging
- 1g
- Price
- $345
- Updated
- 2021/12/16
- Product number
- 024209
- Product name
- 4-(4-Morpholinyl)-1-butanol
- Packaging
- 1g
- Price
- $154
- Updated
- 2021/12/16
- Product number
- 024209
- Product name
- 4-(4-Morpholinyl)-1-butanol
- Packaging
- 500mg
- Price
- $101
- Updated
- 2021/12/16
4-MORPHOLIN-4-YL-BUTAN-1-OL Chemical Properties,Usage,Production
Synthesis
110-91-8
928-51-8
5835-79-0
Example 3; 1-(4-Hydroxybutyl)morpholine was synthesized as follows: to a 250 mL three-necked flask were sequentially added morpholine (65.5 g, 750 mmol), 4-chloro-1-butanol (27.2 g, 250 mmol), sodium iodide (3.8 g, 25 mmol) and 75 mL of dioxane. The reaction mixture was heated to reflux for 48 hours. After completion of the reaction, the mixture was cooled to room temperature. The solvent was removed by rotary evaporator to give a brown oily crude product. The crude product was dissolved in 100 mL of 2N sodium hydroxide solution, extracted with ethyl acetate (EtOAc), the organic phases were combined and dried over anhydrous sodium sulfate (Na2SO4). After removal of the desiccant by filtration, the solvent was removed by distillation under reduced pressure to give an orange colored oil. Finally, the oily substance was subjected to reduced pressure distillation (90 °C, 1 mmHg) to collect the target product 1-(4-hydroxybutyl)morpholine (13.9 g, 87 mmol, 35% yield) as a colorless oil.
References
[1] Patent: WO2008/66874, 2008, A1. Location in patent: Page/Page column 74-75
[2] Journal of the American Chemical Society, 1939, vol. 61, p. 3439
[3] Journal of the American Chemical Society, 1942, vol. 64, p. 970,972
4-MORPHOLIN-4-YL-BUTAN-1-OL Preparation Products And Raw materials
Raw materials
Preparation Products
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