ChemicalBook > CAS DataBase List > 4-(3-HYDROXY-PROPYL)-BENZONITRILE

4-(3-HYDROXY-PROPYL)-BENZONITRILE

Product Name: 4-(3-HYDROXY-PROPYL)-BENZONITRILE
CAS No.: 83101-12-6
Chemical Name: 4-(3-HYDROXY-PROPYL)-BENZONITRILE
Synonyms: 4-(3-HYDROXY-PROPYL)-BENZONITRILE;Benzonitrile, 4-(3-hydroxypropyl)-
CBNumber: CB5840948
Molecular Formula: C10H11NO
Formula Weight: 161.2
MOL File: 83101-12-6.mol

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4-(3-HYDROXY-PROPYL)-BENZONITRILE Property

storage temp.: 2-8°C
Appearance: Colorless to light yellow Liquid

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Safety

HS Code: 2926907090

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Hazard and Precautionary Statements (GHS)

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N-Bromosuccinimide Price

TRC

Product number: A425510
Product name: 4-(3-Hydroxypropyl)benzonitrile
Packaging: 50mg
Price: $110
Updated: 2021/12/16

TRC

Product number: A425510
Product name: 4-(3-Hydroxypropyl)benzonitrile
Packaging: 100mg
Price: $175
Updated: 2021/12/16

AK Scientific

Product number: Z5162
Product name: 4-(3-Hydroxypropyl)benzonitrile
Packaging: 1g
Price: $386
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: CHM0138377
Product name: 4-(3-HYDROXYPROPYL)BENZONITRILE
Purity: 95.00%
Packaging: 1G
Price: $918.06
Updated: 2021/12/16

Alichem

Product number: 83101126
Product name: 4-(3-Hydroxypropyl)benzonitrile
Packaging: 500mg
Price: $980
Updated: 2021/12/16

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4-(3-HYDROXY-PROPYL)-BENZONITRILE Chemical Properties,Usage,Production

Synthesis

42287-94-5

83101-12-6

4) Synthesis of 3-(4-cyanophenyl)propanol Borane-tetrahydrofuran complex (1.0 M, 33.0 mL, 33.0 mmol, dissolved in tetrahydrofuran) was slowly added dropwise to a stirred tetrahydrofuran solution (50 mL) of 3-(4-cyanophenyl)propanoic acid (4.40 g, 25.1 mmol). The reaction mixture was stirred continuously for 14 hours at room temperature. Upon completion of the reaction, water (50 mL) and potassium carbonate (10.0 g, 72.4 mmol) were added to the mixture. Subsequently, the mixture was extracted with ethyl acetate, and the combined organic phases were washed with saturated brine, dried over anhydrous magnesium sulfate, and concentrated under reduced pressure to afford 3-(4-cyanophenyl)propanol as a yellow oil (3.20 g, 79% yield). 1H-NMR (200 MHz, CDCl3) δ: 7.58 (2H, d, J = 8.2 Hz), 7.31 (2H, d, J = 8.2 Hz), 3.68 (2H, t, J = 6.2 Hz), 2.79 (2H, t, J = 7.8 Hz), 2.00-1.75 (2H, m). IR (pure): 3319, 2943, 2229, 1608, 1505, 1415, 1054, 854, 817 cm-1.

References

[1] Patent: US6235731, 2001, B1

4-(3-HYDROXY-PROPYL)-BENZONITRILE Preparation Products And Raw materials

Raw materials

Preparation Products

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4-(3-HYDROXY-PROPYL)-BENZONITRILE Suppliers

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83101-12-6, 4-(3-HYDROXY-PROPYL)-BENZONITRILERelated Search:

N-tert-Butoxycarbonyl-4-cyanophenyl-D-alanine (S)-N-Boc-4-Cyanophenylalanine FMOC-L-4-CYANOPHENYLALANINE L-4-Cyanophenylalanine Fmoc-D-4-Cyanophenylalanine DL-4-Cyanophenylalanine 3-AMINO-3-(4-CYANOPHENYL)PROPANOIC ACID L-4-CYANOPHENYLALANINE 3-(4-CYANO-PHENYL)-3-OXO-PROPIONIC ACID ETHYL ESTER 3-(4-Cyanobenzoyl)-5,7-dimethoxycoumarin 2-([(4-CHLOROPHENYL)SULFONYL]AMINO)-3-(4-CYANOPHENYL)PROPANOIC ACID 3-(4-CYANOPHENYL)-2-([(4-METHOXYPHENYL)SULFONYL]AMINO)PROPANOIC ACID 3-(4-CYANOPHENYL)-2-[(PHENYLSULFONYL)AMINO]PROPANOIC ACID 3-N-FMOC-3-(4-CYANOPHENYL)PROPIONIC ACID (S)-2-ACETYLAMINO-3-(4-CYANO-PHENYL)-PROPIONIC ACID 3-(4-CYANOPHENYL)-2-(1-OXO-1,3-DIHYDRO-2H-ISOINDOL-2-YL)PROPANOIC ACID 3-(4-CYANOPHENYL)-2-([(4-IODOPHENYL)SULFONYL]AMINO)PROPANOIC ACID 3-(4-CYANOPHENYL)-2-([(2,4-DIFLUOROPHENYL)SULFONYL]AMINO)PROPANOIC ACID

4-(3-HYDROXY-PROPYL)-BENZONITRILE

Benzonitrile, 4-(3-hydroxypropyl)-

83101-12-6