2-chloro-4-nitrobenzyl alcohol
- Product Name
- 2-chloro-4-nitrobenzyl alcohol
- CAS No.
- 52301-88-9
- Chemical Name
- 2-chloro-4-nitrobenzyl alcohol
- Synonyms
- Einecs 257-828-2;2-chloro-4-nitrobenzyl alcohol;2-Chloro-4-nitrobenzenemethanol;Benzenemethanol, 2-chloro-4-nitro-
- CBNumber
- CB5926473
- Molecular Formula
- C7H6ClNO3
- Formula Weight
- 187.58
- MOL File
- 52301-88-9.mol
2-chloro-4-nitrobenzyl alcohol Property
- Melting point:
- 83 °C
- Boiling point:
- 337.0±27.0 °C(Predicted)
- Density
- 1.476±0.06 g/cm3(Predicted)
- storage temp.
- Sealed in dry,Room Temperature
- pka
- 13.20±0.10(Predicted)
- Appearance
- Light yellow to brown Solid
Safety
- HS Code
- 2906290090
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P270Do not eat, drink or smoke when using this product.
P271Use only outdoors or in a well-ventilated area.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.
P302+P352IF ON SKIN: wash with plenty of soap and water.
P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P330Rinse mouth.
P332+P313IF SKIN irritation occurs: Get medical advice/attention.
P337+P313IF eye irritation persists: Get medical advice/attention.
P362Take off contaminated clothing and wash before reuse.
P403+P233Store in a well-ventilated place. Keep container tightly closed.
P405Store locked up.
P501Dispose of contents/container to..…
N-Bromosuccinimide Price
- Product number
- C596748
- Product name
- (2-Chloro-4-nitrophenyl)methanol
- Packaging
- 100mg
- Price
- $60
- Updated
- 2021/12/16
- Product number
- FC53475
- Product name
- (2-Chloro-4-Nitrophenyl)Methanol
- Packaging
- 25mg
- Price
- $60
- Updated
- 2021/12/16
- Product number
- FC53475
- Product name
- (2-Chloro-4-Nitrophenyl)Methanol
- Packaging
- 50mg
- Price
- $104.5
- Updated
- 2021/12/16
- Product number
- W6712
- Product name
- 2-chloro-4-nitrobenzylalcohol
- Packaging
- 250mg
- Price
- $109
- Updated
- 2021/12/16
- Product number
- OR401008
- Product name
- 2-Chloro-4-nitrobenzylalcohol
- Packaging
- 1g
- Price
- $138
- Updated
- 2021/12/16
2-chloro-4-nitrobenzyl alcohol Chemical Properties,Usage,Production
Synthesis
13324-11-3
52301-88-9
General procedure for the synthesis of 2-chloro-4-nitrobenzyl alcohol from methyl 2-chloro-4-nitrobenzoate: In a 250 mL round-bottom flask, methyl 2-chloro-4-nitrobenzoate (5 g, 23 mmol) was dissolved in anhydrous dichloromethane (100 mL). The reaction system was cooled to -78 °C under nitrogen protection. Bis(2-methylpropyl)alumina (35 mL, 35 mmol, 1 M solution in hexane) was added slowly and dropwise. The reaction mixture was kept stirred at -78 °C for 4 h. The reaction was subsequently quenched by the addition of water (5 mL). The reaction mixture was gradually warmed to room temperature over 20 min. Anhydrous sodium sulfate (15 g) was added to dry it. after 10 min, the desiccant was removed by filtration. The filtrate was concentrated under reduced pressure to give 2-chloro-4-nitrobenzyl alcohol in 95% yield.
References
[1] Patent: WO2010/132999, 2010, A1. Location in patent: Page/Page column 91
2-chloro-4-nitrobenzyl alcohol Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 2-chloro-4-nitrobenzyl alcohol manufacturers
- Product
- 2-chloro-4-nitrobenzyl alcohol 52301-88-9
- Price
- US $1.00/KG
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- 200kg
- Release date
- 2020-01-09