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Methyl 2,3-dimethylbenzoate-

Product Name
Methyl 2,3-dimethylbenzoate-
CAS No.
15012-36-9
Chemical Name
Methyl 2,3-dimethylbenzoate-
Synonyms
2,3-DiMethoxyMethylbenzoate;2,3-Dimethylbenzoic Acid Methyl Ester;Benzoic acid, 2,3-dimethyl-, methyl ester
CBNumber
CB5946949
Molecular Formula
C10H12O2
Formula Weight
164.2
MOL File
15012-36-9.mol
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Methyl 2,3-dimethylbenzoate- Property

Boiling point:
233.9±9.0 °C(Predicted)
Density 
1.027±0.06 g/cm3(Predicted)
storage temp. 
Sealed in dry,Room Temperature
form 
liquid
color 
Yellow
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Safety

HS Code 
2916399090
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P271Use only outdoors or in a well-ventilated area.

P280Wear protective gloves/protective clothing/eye protection/face protection.

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N-Bromosuccinimide Price

TRC
Product number
D464675
Product name
2,3-DimethylbenzoicAcidMethylEster
Packaging
25g
Price
$1175
Updated
2021/12/16
American Custom Chemicals Corporation
Product number
CHM0003703
Product name
METHYL 2,3-DIMETHYLBENZOATE
Purity
95.00%
Packaging
1G
Price
$688.72
Updated
2021/12/16
Matrix Scientific
Product number
083274
Product name
Methyl 2,3-dimethylbenzoate
Purity
97%
Packaging
1g
Price
$157
Updated
2021/12/16
AK Scientific
Product number
X2847
Product name
Methyl2,3-dimethylbenzoate
Packaging
25g
Price
$251
Updated
2021/12/16
Apolloscientific
Product number
OR7024
Product name
Methyl2,3-dimethylbenzoate
Packaging
1g
Price
$22
Updated
2021/12/16
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Methyl 2,3-dimethylbenzoate- Chemical Properties,Usage,Production

Uses

2,3-Dimethylbenzoic Acid Methyl Ester is a useful synthetic intermediate in the synthesis of 2,3-Dihydro-1H-isoindole-4-carboxylic Acid (D450070); a reagent used in the synthesis of aminoalkylbenzoic acid derivatives for the treatment of faintness attacks, hypokinesia, cranial disorders, neurodegenerative disorders, depression, anxiety, neuropathic pain, neuropathological disorders and sleep disorders.

Synthesis

67-56-1

603-79-2

15012-36-9

Step 1. Thionyl chloride (62 mL, 0.83 mol) was added slowly and dropwise to a solution of 2,3-dimethylbenzoic acid (50.2 g, 0.33 mol) in methanol (1 L), taking care to control the rate of acceleration of the dropwise addition in order to avoid intense exothermicity. The reaction mixture was heated to reflux and stirred overnight and subsequently cooled to room temperature. The solvent was removed by distillation under reduced pressure to afford methyl 2,3-dimethylbenzoate (53.3 g, 98% yield) as a yellow liquid.1H-NMR (300 MHz, CDCl3) data were as follows: δ 2.34 (s, 3H), 3.45 (s, 3H), 3.90 (s, 3H), 7.15 (t, 1H), 7.28 (d, 1H), 7.62 (d, 1H). 7.62 (d, 1H).

References

[1] Patent: WO2008/53319, 2008, A1. Location in patent: Page/Page column 55
[2] Patent: WO2015/116923, 2015, A1. Location in patent: Paragraph 0503; 0505
[3] Tetrahedron, 1998, vol. 54, # 7, p. 1207 - 1220
[4] Tetrahedron Letters, 2009, vol. 50, # 49, p. 6803 - 6806

Methyl 2,3-dimethylbenzoate- Preparation Products And Raw materials

Raw materials

Preparation Products

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Methyl 2,3-dimethylbenzoate- Suppliers

China 64 Germany 1 India 1 United Kingdom 4 United States 7 Global 77
Shanghai Hanhong Scientific Co.,Ltd.
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021-54306202 13764082696
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info@hanhongsci.com
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China
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42934
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64
Beijing Eternalchem Co,. Ltd.
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010-59484199 18611897322
Email
sales@eternalchem.com
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China
ProdList
4383
Advantage
60
NovoChemy Ltd.
Tel
021-31261262/ 49 (0)17662837245
Fax
(0)21-33250524
Email
sales@novochemy.com
Country
Germany
ProdList
6328
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58
Bide Pharmatech Ltd.
Tel
400-164-7117 13681763483
Fax
+86-21-61629029
Email
product02@bidepharm.com
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China
ProdList
39966
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Jiangsu Aikon Biopharmaceutical R&D co.,Ltd.
Tel
025-66028182 18626450290
Email
yftan@aikonchem.com
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China
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16679
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50
Bellen Chemistry Co., Ltd.
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010-60400365-8001 15910885229
Fax
010-60400361
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service@bellenchem.com
Country
China
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4514
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60
Accela ChemBio Inc.
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+1(858) 699-3322
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+1(858) 876-1948
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marketing@accelachem.com
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United States
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6024
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Changzhou Anxuan Chemical, Co., Ltd.
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13912302692 13912302692;
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0519-88064678
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sales@anxuanchem.com
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China
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4828
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SanoChem (Chengdu) Tech. Co., Ltd.
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28-87999436 02887999436
Fax
QQ:2746983436
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sales@sano-chem.com
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China
ProdList
3795
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Chengdu Research Accelerators Technology Co., Ltd.
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028-64353063
Fax
028-64353063 QQ:784253935
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reacchemical@163.com
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China
ProdList
5253
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15012-36-9, Methyl 2,3-dimethylbenzoate- Related Search:

TETRAPHENYLPHTHALIC ANHYDRIDE 2,3-DIMETHYLBENZOIC ACID ETHYL ESTER METHYL 9-OXO-9H-FLUORENE-4-CARBOXYLATE BENZENEHEXACARBOXYLIC ACID HEXAMETHYL ESTER 2,2,3,3,4,4,5,5,5-NONAFLUOROPENTYL 2,5,7-TRINITRO-9-OXO-9H-FLUORENE-4-CARBOXYLATE 2-ETHOXYETHYL 9-(DICYANOMETHYLIDENE)-2,5,7-TRINITRO-9H-FLUORENE-4-CARBOXYLATE 4,4'-(2-ACETYL-1,3-GLYCEROL) BISANHYDRO MELLITATE RARECHEM AL BF 0260 ethyl 9-oxo-9H-fluorene-4-carboxylate BUTYL 2,5,7-TRINITRO-9-OXO-9H-FLUORENE-4-CARBOXYLATE 2,2,3,3,4,4,5,5-OCTAFLUOROPENTYL 2,5,7-TRINITRO-9-OXO-9H-FLUORENE-4-CARBOXYLATE 2-ETHOXYETHYL 2,5,7-TRINITRO-9-OXO-9H-FLUORENE-4-CARBOXYLATE PENTYL 2,5,7-TRINITRO-9-OXO-9H-FLUORENE-4-CARBOXYLATE METHYL 2-BROMO-7-NITRO-9-FLUORENONE-4-CARBOXYLATE ISOBUTYL 2,5,7-TRINITRO-9-OXO-9H-FLUORENE-4-CARBOXYLATE 2,2,3,3,4,4,5,5,5-NONAFLUOROPENTYL 2,7-DINITRO-9-OXO-9H-FLUORENE-4-CARBOXYLATE HEXYL 2,5,7-TRINITRO-9-OXO-9H-FLUORENE-4-CARBOXYLATE METHYL 9-[DI(DIMETHYLAMINO)METHYLIDENE]-2,5,7-TRINITRO-9H-FLUORENE-4-CARBOXYLATE

  • 2,3-DiMethoxyMethylbenzoate
  • 2,3-Dimethylbenzoic Acid Methyl Ester
  • Benzoic acid, 2,3-dimethyl-, methyl ester
  • 15012-36-9