Tert-butyl (S)-(1-(3-fluorophenyl)-2-hydroxyethyl)carbamate
- Product Name
- Tert-butyl (S)-(1-(3-fluorophenyl)-2-hydroxyethyl)carbamate
- CAS No.
- 1035490-58-4
- Chemical Name
- Tert-butyl (S)-(1-(3-fluorophenyl)-2-hydroxyethyl)carbamate
- Synonyms
- (S)-2-(Boc-amino)-2-(3-fluorophenyl)ethanol;tert-butyl (S)-(1-(3-fluorophenyl)-2-hydroxyethyl)carbamate;tert-butyl N-[(1S)-1-(3-fluorophenyl)-2-hydroxyethyl]carbamate;(S)-1-(3-fluoro-phenyl)-2-hydroxy-ethyl]-carbamic acid tert-butyl ester;Carbamic acid, N-[(1S)-1-(3-fluorophenyl)-2-hydroxyethyl]-, 1,1-dimethylethyl ester
- CBNumber
- CB610468902
- Molecular Formula
- C13H18FNO3
- Formula Weight
- 255.29
- MOL File
- 1035490-58-4.mol
Tert-butyl (S)-(1-(3-fluorophenyl)-2-hydroxyethyl)carbamate Property
- Boiling point:
- 381.4±37.0 °C(Predicted)
- Density
- 1.162±0.06 g/cm3(Predicted)
- pka
- 11.38±0.46(Predicted)
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
- Precautionary statements
-
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P302+P352IF ON SKIN: wash with plenty of soap and water.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P332+P313IF SKIN irritation occurs: Get medical advice/attention.
P337+P313IF eye irritation persists: Get medical advice/attention.
Tert-butyl (S)-(1-(3-fluorophenyl)-2-hydroxyethyl)carbamate Chemical Properties,Usage,Production
Physical properties
A white crystal,melting point:106.5 - 107.9
Uses
Tert-butyl (S)-(1-(3-fluorophenyl)-2-hydroxyethyl)carbamate is a useful research chemical for a range of applications.
Preparation
Amino alcohol hydrochloride (192.22 mmol) and di-f-butyl dicarbonate (262.63 mmol, 1.37 eq) were suspended in f-BuOH (250 mL, 6.25 volumes) and then treated with aqueous 2 N NaOH (120 mL, 240 mmol). The contents were warmed to 75 °C (immediate effervescence was observed) for 4 h. The internal temp was then reduced to 50 °C, and the contents were added to water (2 L) with vigorous stirring. Tert-butyl (S)-(1-(3-fluorophenyl)-2-hydroxyethyl)carbamate was obtained after purification.
Tert-butyl (S)-(1-(3-fluorophenyl)-2-hydroxyethyl)carbamate Preparation Products And Raw materials
Raw materials
Preparation Products
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