Ethanone, 1,1-bicyclo[1.1.1]pentane-1,3-diylbis- (9CI)
- Product Name
- Ethanone, 1,1-bicyclo[1.1.1]pentane-1,3-diylbis- (9CI)
- CAS No.
- 115913-30-9
- Chemical Name
- Ethanone, 1,1-bicyclo[1.1.1]pentane-1,3-diylbis- (9CI)
- Synonyms
- 1,1′-(BicycL;o[1.1.1]pentane-1,3-diyL;1,3-Diacetylbicyclo(1,1,1)pentane;1,1-bicyclo[1.1.1]pentane-1,3-diylbis- (9CI);1-(3-acetyl-1-bicyclo[1.1.1]pentanyl)ethanone;1-(3-Acetyl-bicyclo[1.1.1]pent-1-yl)-ethanone;1,1'-(bicyclo[1.1.1]pentane-1,3-diyl)diethanone;1,1'-(bicyclo[1.1.1]pentane-1,3-diyl)diethanone;1-{3-acetylbicyclo[1.1.1]pentan-1-yl}ethan-1-one;Ethanone, 1,1'-bicyclo[1.1.1]pentane-1,3-diylbis-
- CBNumber
- CB61067862
- Molecular Formula
- C9H12O2
- Formula Weight
- 152.19
- MOL File
- 115913-30-9.mol
Ethanone, 1,1-bicyclo[1.1.1]pentane-1,3-diylbis- (9CI) Property
- Melting point:
- 65.1-66.9 °C
- Boiling point:
- 224.8±40.0 °C(Predicted)
- Density
- 1.249±0.06 g/cm3(Predicted)
- storage temp.
- Sealed in dry,Room Temperature
- form
- solid
- Appearance
- Off-white to light brown Solid
Safety
- HS Code
- 2914790090
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H319Causes serious eye irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- B111400
- Product name
- 1,1''-(Bicyclo[1.1.1]pentane-1,3-diyl)diethanone
- Packaging
- 50mg
- Price
- $75
- Updated
- 2021/12/16
- Product number
- AS55665
- Product name
- 1,1'-(Bicyclo[1.1.1]pentane-1,3-diyl)diethanone
- Purity
- 97+%
- Packaging
- 250mg
- Price
- $90
- Updated
- 2021/12/16
- Product number
- 3946AQ
- Product name
- 1-(3-acetyl-1-bicyclo[1.1.1]pentanyl)ethanone
- Packaging
- 100mg
- Price
- $131.6
- Updated
- 2021/12/16
- Product number
- OR317272
- Product name
- 1,1'-(Bicyclo[1.1.1]pentane-1,3-diyl)diethanone
- Packaging
- 1g
- Price
- $163
- Updated
- 2021/12/16
- Product number
- AS55665
- Product name
- 1,1'-(Bicyclo[1.1.1]pentane-1,3-diyl)diethanone
- Purity
- 97+%
- Packaging
- 1g
- Price
- $171
- Updated
- 2021/12/16
Ethanone, 1,1-bicyclo[1.1.1]pentane-1,3-diylbis- (9CI) Chemical Properties,Usage,Production
Synthesis
35634-10-7
431-03-8
115913-30-9
The general procedure for the synthesis of 1,1'-(bicyclo[1.1.1]pentane-1,3-diyl)diethyl ketone from the compound (CAS: 35634-10-7) and 2,3-butanedione was as follows: 2,3-butanedione (35 mL) was added to the solution of compound 2, and the temperature of the reaction was controlled to be between 15°C and 25°C. The reaction was carried out under the irradiation of a medium pressure mercury lamp of 80 W to 150 W for 16 hours. Upon completion of the reaction, the reaction system was concentrated directly to obtain the crude product. Subsequently, the crude product was recrystallized using hexane to give pure compound 4 (23 g) in 43% yield.
References
[1] Journal of Organic Chemistry, 1988, vol. 53, # 19, p. 4593 - 4594
[2] Journal of Organic Chemistry, 1988, vol. 53, # 19, p. 4593 - 4594
[3] European Journal of Organic Chemistry, 2004, # 3, p. 493 - 498
[4] Journal of Medicinal Chemistry, 2012, vol. 55, # 7, p. 3414 - 3424
[5] Patent: CN105294442, 2016, A. Location in patent: Paragraph 0006; 0009
Ethanone, 1,1-bicyclo[1.1.1]pentane-1,3-diylbis- (9CI) Preparation Products And Raw materials
Raw materials
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View Lastest Price from Ethanone, 1,1-bicyclo[1.1.1]pentane-1,3-diylbis- (9CI) manufacturers
- Product
- Ethanone, 1,1-bicyclo[1.1.1]pentane-1,3-diylbis- (9CI) 115913-30-9
- Price
- US $0.00/kg
- Min. Order
- 1kg
- Purity
- 98%
- Supply Ability
- 1000kg
- Release date
- 2025-06-19
- Product
- Ethanone, 1,1-bicyclo[1.1.1]pentane-1,3-diylbis- (9CI) 115913-30-9
- Price
- US $0.00-0.00/KG
- Min. Order
- 1KG
- Purity
- 98%
- Supply Ability
- 1ton
- Release date
- 2022-09-19
- Product
- Ethanone, 1,1-bicyclo[1.1.1]pentane-1,3-diylbis- (9CI) 115913-30-9
- Price
- US $7.00/KG
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- 1000kg
- Release date
- 2020-01-12