Ethyl-2-fluoro-5-iodobenzoate

Product Name: Ethyl-2-fluoro-5-iodobenzoate
CAS No.: 773136-66-6
Chemical Name: Ethyl-2-fluoro-5-iodobenzoate
Synonyms: Ethyl-2-fluoro-5-iodobenzoate;Benzoic acid, 2-fluoro-5-iodo-, ethyl ester
CBNumber: CB61114537
Molecular Formula: C9H8FIO2
Formula Weight: 294.06
MOL File: 773136-66-6.mol

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Ethyl-2-fluoro-5-iodobenzoate Property

storage temp.: 2-8°C(protect from light)
Appearance: Colorless to light yellow Liquid

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Safety

HS Code: 2916399090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H226Flammable liquid and vapour

Precautionary statements

P210Keep away from heat/sparks/open flames/hot surfaces. — No smoking.

P233Keep container tightly closed.

P240Ground/bond container and receiving equipment.

P241Use explosion-proof electrical/ventilating/lighting/…/equipment.

P242Use only non-sparking tools.

P243Take precautionary measures against static discharge.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P303+P361+P353IF ON SKIN (or hair): Remove/Take off Immediately all contaminated clothing. Rinse SKIN with water/shower.

P370+P378In case of fire: Use … for extinction.

P403+P235Store in a well-ventilated place. Keep cool.

P501Dispose of contents/container to..…

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N-Bromosuccinimide Price

American Custom Chemicals Corporation

Product number: HCH0014154
Product name: ETHYL-2-FLUORO-5-IODOBENZOATE
Purity: 95.00%
Packaging: 1G
Price: $720.37
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: HCH0014154
Product name: ETHYL-2-FLUORO-5-IODOBENZOATE
Purity: 95.00%
Packaging: 5G
Price: $1285.52
Updated: 2021/12/16

Ambeed

Product number: A179873
Product name: Ethyl2-Fluoro-5-iodobenzoate
Purity: 95+%
Packaging: 250mg
Price: $22
Updated: 2021/12/16

Ambeed

Product number: A179873
Product name: Ethyl2-Fluoro-5-iodobenzoate
Purity: 95+%
Packaging: 1g
Price: $50
Updated: 2021/12/16

AHH

Product number: MB-16775
Product name: ethyl2-fluoro-5-iodobenzoate
Purity: 97%
Packaging: 1g
Price: $110
Updated: 2021/12/16

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Ethyl-2-fluoro-5-iodobenzoate Chemical Properties,Usage,Production

Synthesis

64-17-5

124700-41-0

773136-66-6

General procedure for the synthesis of ethyl 2-fluoro-5-iodobenzoate from ethanol and 2-fluoro-5-iodobenzoic acid: 2-Fluoro-5-iodobenzoic acid (Oakwood, 0.99 g, 3.72 mmol) and H2SO4 (198 μL, 3.72 mmol) were added to EtOH (7.4 mL). The reaction mixture was stirred at 100 °C overnight. After completion of the reaction, the mixture was concentrated in vacuum. The crude product was purified by fast column chromatography (gradient of 0 to 10% EtOAc/hexane) to afford the title compound ethyl 2-fluoro-5-iodobenzoate (916 mg, 84%) as a colorless oil. 1H NMR (CDCl3) δ 8.24 (dd, J = 6.8, 2.4 Hz, 1H), 7.81 (ddd, J = 8.8, 4.5, 2.4 Hz, 1H), 6.93 (dd, J = 10.3, 8.6 Hz, 1H), 4.41 (q, J = 7.0 Hz, 2H), 1.42 (t, J = 7.2 Hz, 3H).

References

[1] Patent: WO2012/162365, 2012, A1. Location in patent: Page/Page column 173-174

Ethyl-2-fluoro-5-iodobenzoate Preparation Products And Raw materials

Raw materials

Preparation Products

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Ethyl-2-fluoro-5-iodobenzoate Suppliers

China 32 India 1 United Kingdom 1 United States 4 Global 38

Wuhan Chemwish Technology Co., Ltd

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Wuhan Chemwish Technology Co.， Ltd

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773136-66-6, Ethyl-2-fluoro-5-iodobenzoateRelated Search:

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Ethyl-2-fluoro-5-iodobenzoate

Benzoic acid, 2-fluoro-5-iodo-, ethyl ester

773136-66-6