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4(1H)-Pyrimidinone, 2-amino-6-methyl-5-nitro-

Product Name
4(1H)-Pyrimidinone, 2-amino-6-methyl-5-nitro-
CAS No.
4214-85-1
Chemical Name
4(1H)-Pyrimidinone, 2-amino-6-methyl-5-nitro-
Synonyms
2-amino-6-methyl-5-nitropyrimidin-4(3H)-one;2-aMino-6-Methyl-5-nitropyriMidin-4-ol;2-Amino-6-methyl-5-nitro-4(3H)-pyrimidinone;2-amino-6-methyl-5-nitropyrimidin-4(1H)-one;2-amino-6-methyl-5-nitro-1H-pyrimidin-4-one;2-amino-4-hydroxy-6-methyl-5-nitropyrimidine;2-azanyl-6-methyl-5-nitro-1H-pyrimidin-4-one;2-Amino-6-methyl-5-nitro-3H-pyrimidine-4-one;2-AMINO-4-HYDROXY-5-NITRO-6-METHYL-PYRIMIDINE;4(1H)-Pyrimidinone, 2-amino-6-methyl-5-nitro-
CBNumber
CB61211393
Molecular Formula
C5H6N4O3
Formula Weight
170.13
MOL File
4214-85-1.mol
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4(1H)-Pyrimidinone, 2-amino-6-methyl-5-nitro- Property

Melting point:
>300 °C
Boiling point:
305.9±45.0 °C(Predicted)
Density 
1.83±0.1 g/cm3(Predicted)
storage temp. 
2-8°C, protect from light
pka
7.18±0.50(Predicted)
Appearance
Light yellow to yellow Powder
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Safety

HazardClass 
IRRITANT
HS Code 
2933599590
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H332Harmful if inhaled

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

AstaTech
Product number
50736
Product name
2-AMINO-6-METHYL-5-NITROPYRIMIDIN-4(3H)-ONE
Purity
97%
Packaging
1G
Price
$37
Updated
2026/04/30
AstaTech
Product number
50736
Product name
2-AMINO-6-METHYL-5-NITROPYRIMIDIN-4(3H)-ONE
Purity
97%
Packaging
5G
Price
$159
Updated
2026/04/30
AstaTech
Product number
50736
Product name
2-AMINO-6-METHYL-5-NITROPYRIMIDIN-4(3H)-ONE
Purity
97%
Packaging
25G
Price
$617
Updated
2026/04/30
TRC
Product number
A898778
Product name
2-Amino-6-methyl-5-nitro-3H-pyrimidin-4-one
Packaging
1g
Price
$200
Updated
2021/12/16
Biosynth Carbosynth
Product number
FA139523
Product name
2-Amino-6-methyl-5-nitropyrimidin-4(3H)-one
Packaging
500mg
Price
$85
Updated
2021/12/16
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4(1H)-Pyrimidinone, 2-amino-6-methyl-5-nitro- Chemical Properties,Usage,Production

Synthesis

3977-29-5

4214-85-1

The general procedure for the synthesis of 2-amino-6-methyl-5-nitro-3H-pyrimidin-4-one from 2-amino-4-hydroxy-6-methylpyrimidine was as follows: 2-amino-6-methylpyrimidin-4(3H)-one (50 g, 0.4 mol) was dissolved in 250 mL of concentrated sulfuric acid at 0°C, and 40 mL of concentrated nitric acid was slowly added through a dropping funnel. The reaction mixture was stirred at room temperature for 3 hours and then slowly poured into 3.6 L of diethyl ether and continued stirring for 15 minutes. The ether layer was decanted off and 1.0 L of ethyl acetate was added to the remaining solid and stirred for 10 hours. The solid product (54.8 g, 81% yield) was collected by filtration, which could be used in subsequent reactions without further purification.

References

[1] Synthetic Communications, 2009, vol. 39, # 12, p. 2244 - 2249
[2] Journal of Heterocyclic Chemistry, 2009, vol. 46, # 6, p. 1151 - 1153
[3] Journal of Organic Chemistry, 1995, vol. 60, # 24, p. 7947 - 7952
[4] Patent: WO2006/122003, 2006, A2. Location in patent: Page/Page column 32; 34
[5] Nucleosides and Nucleotides, 1999, vol. 18, # 3, p. 363 - 376

4(1H)-Pyrimidinone, 2-amino-6-methyl-5-nitro- Preparation Products And Raw materials

Raw materials

Preparation Products

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4(1H)-Pyrimidinone, 2-amino-6-methyl-5-nitro- Suppliers

SiChuang NanBu Honesty Technology Co., Ltd.
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0838-5675166 15883665058
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0838-5675535
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nbcxkj@126.com
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China
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J & K SCIENTIFIC LTD.
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jkinfo@jkchemical.com
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Wuhan Chemwish Technology Co., Ltd
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86-027-67849912
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86-027-87531808
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Shanghai Hanhong Scientific Co.,Ltd.
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021-54306202 13764082696
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Shanghai Ennopharm Co., Ltd.
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Hangzhou Yuhao Chemical Technology Co., Ltd
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Heterochem
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Shanghai Topbiochem Technology Co., Ltd
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SuZhou ShiYa Biopharmaceuticals, Inc.
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View Lastest Price from 4(1H)-Pyrimidinone, 2-amino-6-methyl-5-nitro- manufacturers

Shaanxi Dideu Medichem Co. Ltd
Product
2-Amino-6-methyl-5-nitropyrimidin-4(3H)-one 4214-85-1
Price
US $20.00-100.00/KG
Min. Order
1KG
Purity
99%
Supply Ability
200000KG
Release date
2024-08-09
Career Henan Chemical Co
Product
4(1H)-Pyrimidinone, 2-amino-6-methyl-5-nitro- 4214-85-1
Price
US $2.00/KG
Min. Order
1KG
Purity
98%MIN
Supply Ability
ASK
Release date
2019-12-25

4214-85-1, 4(1H)-Pyrimidinone, 2-amino-6-methyl-5-nitro-Related Search:


  • 4(1H)-Pyrimidinone, 2-amino-6-methyl-5-nitro-
  • 2-AMINO-4-HYDROXY-5-NITRO-6-METHYL-PYRIMIDINE
  • 2-Amino-6-methyl-5-nitro-3H-pyrimidine-4-one
  • 2-amino-6-methyl-5-nitropyrimidin-4(3H)-one
  • 2-amino-6-methyl-5-nitro-1H-pyrimidin-4-one
  • 2-azanyl-6-methyl-5-nitro-1H-pyrimidin-4-one
  • 2-amino-6-methyl-5-nitropyrimidin-4(1H)-one
  • 2-Amino-6-methyl-5-nitro-4(3H)-pyrimidinone
  • 2-amino-4-hydroxy-6-methyl-5-nitropyrimidine
  • 2-aMino-6-Methyl-5-nitro-3,4-dihydropyriMidin-4-one
  • 2-aMino-6-Methyl-5-nitropyriMidin-4-ol
  • 4(3H)-Pyrimidinone, 2-amino-6-methyl-5-nitro-
  • 4(1H)-Pyrimidinone, 2-amino-6-methyl-5-nitro- ISO 9001:2015 REACH
  • 4214-85-1
  • Pyrimidine series