4-aminopicolinonitrile

Product Name: 4-aminopicolinonitrile
CAS No.: 98139-15-2
Chemical Name: 4-aminopicolinonitrile
Synonyms: 4-AMINOPICOLINONITRILE;4-AMINO-2-CYANOPYRIDINE;4-Aminopyridine-2-carbonitrile;2-Pyridinecarbonitrile, 4-amino-;2-Pyridinecarbonitrile,4-amino-(9CI);4-AMINOPYRIDINE-2-CARBONITRILE ISO 9001：2015 REACH
CBNumber: CB61253490
Molecular Formula: C6H5N3
Formula Weight: 119.12
MOL File: 98139-15-2.mol

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4-aminopicolinonitrile Property

Melting point:: 145 °C
Boiling point:: 368.2±22.0 °C(Predicted)
Density: 1.23±0.1 g/cm3(Predicted)
storage temp.: Keep in dark place,Inert atmosphere,Room temperature
pka: 3.87±0.30(Predicted)
Appearance: Off-white to brown Solid
InChI: InChI=1S/C6H5N3/c7-4-6-3-5(8)1-2-9-6/h1-3H,(H2,8,9)
InChIKey: GMKRESMCPMIWGU-UHFFFAOYSA-N
SMILES: C1(C#N)=NC=CC(N)=C1

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Safety

RIDADR: UN2811
HS Code: 2933399990

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC

Product number: A630023
Product name: 4-Aminopyridine-2-carbonitrile
Packaging: 50mg
Price: $45
Updated: 2021/12/16

TRC

Product number: A630023
Product name: 4-Aminopyridine-2-carbonitrile
Packaging: 100mg
Price: $65
Updated: 2021/12/16

TRC

Product number: A630023
Product name: 4-Aminopyridine-2-carbonitrile
Packaging: 500mg
Price: $285
Updated: 2021/12/16

Ark Pharm

Product number: P000724815
Product name: 4-Aminopyridine-2-carbonitrile
Purity: 97%
Packaging: 250mg
Price: $57
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FA148691
Product name: 4-Amino-2-cyanopyridine
Packaging: 50mg
Price: $78
Updated: 2021/12/16

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4-aminopicolinonitrile Chemical Properties,Usage,Production

Synthesis

557-21-1

14432-12-3

98139-15-2

2-Chloro-4-aminopyridine (0.642 g, 5 mmol), zinc cyanide (0.323 g, 2.75 mmol) and tetrakis(triphenylphosphine)palladium (0.288 g, 0.025 mmol) were mixed in 5 mL N,N-dimethylformamide (DMF). The reaction mixture was heated at 145°C for 20 hours. After completion of the reaction, it was cooled to room temperature and subsequently partitioned between ethyl acetate and water. The aqueous layer was extracted with additional ethyl acetate. The organic layers were combined, washed with saturated brine, dried over anhydrous magnesium sulfate, filtered and concentrated under reduced pressure. The crude product was purified by fast column chromatography on silica gel, using 9:1 hexane/ethyl acetate as eluent to give 0.29 g (20% yield) of 4-aminopyridine-2-carbonitrile. Mass spectrum (DCI) m/e 120 (M + H)+; 1H NMR (300 MHz, DMSO-D6) δ 8.08 (d, J = 5.76 Hz, 1H), 6.94 (d, J = 2.34 Hz, 1H), 6.68 (dd, J = 5.76,2.37 Hz, 1H), 6.59 (s, 2H).

References

[1] Patent: WO2004/76424, 2004, A1. Location in patent: Page 131

4-aminopicolinonitrile Preparation Products And Raw materials

Raw materials

Preparation Products

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4-aminopicolinonitrile Suppliers

China 84 Europe 1 India 1 United Kingdom 2 United States 10 Global 98

Zhengzhou Lingzhiyue Technology Co., LTD

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Modachem Shanghai Co., Ltd

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View Lastest Price from 4-aminopicolinonitrile manufacturers

Shaanxi Dideu Medichem Co. Ltd

Product: 4-AMINOPYRIDINE-2-CARBONITRILE 98139-15-2
Price: US $1.10/g
Min. Order: 1g
Purity: 99.0% min
Supply Ability: 100 tons min
Release date: 2021-05-26

Career Henan Chemical Co

Product: 4-AMINOPYRIDINE-2-CARBONITRILE 98139-15-2
Price: US $6.60/KG
Min. Order: 1KG
Purity: 97%-99%
Supply Ability: 1kg-1000kg
Release date: 2019-12-30

98139-15-2, 4-aminopicolinonitrileRelated Search:

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2-Pyridinecarbonitrile,4-amino-(9CI)

4-AMINO-2-CYANOPYRIDINE

4-Aminopyridine-2-carbonitrile

2-Pyridinecarbonitrile, 4-amino-

4-AMINOPYRIDINE-2-CARBONITRILE ISO 9001：2015 REACH

4-AMINOPICOLINONITRILE

98139-15-2

Pyridine series

Pyridines

PYRIDINE