5-bromo-2-nitro-N-phenyl-aniline

Product Name: 5-bromo-2-nitro-N-phenyl-aniline
CAS No.: 6311-47-3
Chemical Name: 5-bromo-2-nitro-N-phenyl-aniline
Synonyms: 5-bromo-2-nitro-N-phenyl-aniline;N-(5-bromo-2-nitrophenyl)benzenamine;BenzenaMine, 5-broMo-2-nitro-N-phenyl-
CBNumber: CB61258369
Molecular Formula: C12H9BrN2O2
Formula Weight: 293.12
MOL File: 6311-47-3.mol

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5-bromo-2-nitro-N-phenyl-aniline Property

storage temp.: Keep in dark place,Inert atmosphere,Room temperature
Appearance: Orange to yellow Solid

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P271Use only outdoors or in a well-ventilated area.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P312Call a POISON CENTER or doctor/physician if you feel unwell.

P321Specific treatment (see … on this label).

P332+P313IF SKIN irritation occurs: Get medical advice/attention.

P337+P313IF eye irritation persists: Get medical advice/attention.

P362Take off contaminated clothing and wash before reuse.

P403+P233Store in a well-ventilated place. Keep container tightly closed.

P405Store locked up.

P501Dispose of contents/container to..…

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N-Bromosuccinimide Price

American Custom Chemicals Corporation

Product number: HCH0366897
Product name: 5-BROMO-2-NITRO-N-PHENYLANILINE
Purity: 95.00%
Packaging: 5MG
Price: $503.75
Updated: 2021/12/16

AK Scientific

Product number: 9585AB
Product name: 5-Bromo-2-nitro-N-phenylaniline
Packaging: 1g
Price: $647
Updated: 2021/12/16

Matrix Scientific

Product number: 132111
Product name: 5-Bromo-2-nitro-N-phenylaniline
Purity: 97%
Packaging: 100g
Price: $1764
Updated: 2021/12/16

AK Scientific

Product number: 9585AB
Product name: 5-Bromo-2-nitro-N-phenylaniline
Packaging: 5g
Price: $2136
Updated: 2021/12/16

Matrix Scientific

Product number: 132111
Product name: 5-Bromo-2-nitro-N-phenylaniline
Purity: 97%
Packaging: 250g
Price: $3240
Updated: 2021/12/16

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5-bromo-2-nitro-N-phenyl-aniline Chemical Properties,Usage,Production

Synthesis

321-23-3

62-53-3

6311-47-3

General procedure for the synthesis of 5-bromo-2-nitro-N-phenyl-aniline from 2-fluoro-4-bromonitrobenzene and aniline: 4-bromo-2-fluoronitrobenzene (5.6 g, 20.9 mmol) and aniline (2.5 g, 72.2 mmol) were dissolved in 50 mL of anhydrous N-methylpyrrolidone (NMP). The reaction mixture was heated to 110 °C and the reaction was stirred overnight. After completion of the reaction, it was cooled to room temperature and the solvent was removed by distillation under reduced pressure. The crude product was purified by silica gel column chromatography with the eluent cyclohexane/ethyl acetate (9:1, v/v) to give an orange solid product in 92% yield (5.7 g). The 1H-NMR (400 MHz, CD2Cl2) data of the product were as follows: δ= 9.48 (s, 1H), 8.06 (d, 1H), 7.46 (t, 2H), 7.30 (t, 4H), 6.89 (d, 1H).

References

[1] Patent: WO2015/14944, 2015, A1. Location in patent: Page/Page column 115; 116
[2] Patent: WO2015/150203, 2015, A1. Location in patent: Page/Page column 85
[3] Patent: WO2014/100695, 2014, A1. Location in patent: Paragraph 00349
[4] Patent: US2015/30588, 2015, A1. Location in patent: Page/Page column 71
[5] Patent: US9295673, 2016, B2. Location in patent: Page/Page column 351; 352

5-bromo-2-nitro-N-phenyl-aniline Preparation Products And Raw materials

Raw materials

Preparation Products

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5-bromo-2-nitro-N-phenyl-aniline Suppliers

China 25 India 1 United States 4 Global 30

SiChuang NanBu Honesty Technology Co., Ltd.

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Aikon International Limited

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Rhawn Reagent

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6311-47-3, 5-bromo-2-nitro-N-phenyl-anilineRelated Search:

5-bromo-2-nitro-N-phenyl-aniline

BenzenaMine, 5-broMo-2-nitro-N-phenyl-

N-(5-bromo-2-nitrophenyl)benzenamine

6311-47-3