4-AMINO-4'-NITRODIPHENYL SULFIDE
Uses- Product Name
- 4-AMINO-4'-NITRODIPHENYL SULFIDE
- CAS No.
- 101-59-7
- Chemical Name
- 4-AMINO-4'-NITRODIPHENYL SULFIDE
- Synonyms
- AI3-16817;ASISCHEM D50976;4-AMINO-4'-NITRODIPH;4-(4-NITROPHENYLTHIO)ANILINE;sulfide,anilino(p-nitrophenyl);p-((p-nitrophenyl)thio)-anilin;4-[(P-NITROPHENYL)THIO]ANILINE;p-[(p-Nitrophenyl)thio]aniline;4-(4-nitrophenyl)sulfanylaniline;4-Amino-4'-nitrodiphenyl Sulfide
- CBNumber
- CB6128205
- Molecular Formula
- C12H10N2O2S
- Formula Weight
- 246.29
- MOL File
- 101-59-7.mol
4-AMINO-4'-NITRODIPHENYL SULFIDE Property
- Melting point:
- 143-145 °C(lit.)
- Boiling point:
- 479.1±30.0 °C(Predicted)
- Density
- 1.3031 (rough estimate)
- refractive index
- 1.5950 (estimate)
- storage temp.
- Keep in dark place,Sealed in dry,Room Temperature
- form
- powder to crystal
- pka
- 2.99±0.10(Predicted)
- color
- Orange prisms with blue reflex from C6H6, crystfrom EtOH
- InChI
- 1S/C12H10N2O2S/c13-9-1-5-11(6-2-9)17-12-7-3-10(4-8-12)14(15)16/h1-8H,13H2
- InChIKey
- ZBPKGHOGUVVDLF-UHFFFAOYSA-N
- SMILES
- Nc1ccc(Sc2ccc(cc2)[N+]([O-])=O)cc1
- CAS DataBase Reference
- 101-59-7(CAS DataBase Reference)
- EPA Substance Registry System
- 4-[(4-Nitrophenyl)thio]aniline (101-59-7)
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P271Use only outdoors or in a well-ventilated area.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P302+P352IF ON SKIN: wash with plenty of soap and water.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- A69188
- Product name
- 4-Amino-4′-nitrodiphenyl sulfide
- Purity
- 98%
- Packaging
- 5g
- Price
- $44.3
- Updated
- 2023/06/20
- Product number
- A2077
- Product name
- 4-Amino-4'-nitrodiphenyl Sulfide
- Purity
- >98.0%(GC)(T)
- Packaging
- 25g
- Price
- $85
- Updated
- 2025/07/31
- Product number
- A618633
- Product name
- 4-Amino-4'-nitrodiphenyl Sulfide
- Packaging
- 250mg
- Price
- $45
- Updated
- 2021/12/16
- Product number
- JK136030
- Product name
- 4-Amino-4'-nitrodiphenyl Sulfide
- Purity
- 98%
- Packaging
- 5g
- Price
- $57
- Updated
- 2021/12/16
- Product number
- FA33720
- Product name
- 4-Amino-4'-nitrodiphenyl sulfide
- Packaging
- 5G
- Price
- $60
- Updated
- 2021/12/16
4-AMINO-4'-NITRODIPHENYL SULFIDE Chemical Properties,Usage,Production
Uses
4-Amino-4'-nitrodiphenyl sulfide is an ether derivative that can be used as an intermediate in organic synthesis.
Safety Profile
Poison by intravenous route.Mutation data reported. When heated to decomposition it emits very toxic fumesof NOx and SOx.
Synthesis
A solution of 4-amino-benzenethiol (1.00 Kg, 7.99 mol) was dissolved in toluene (2 liters) under nitrogen and slowly added with mechanical stirring to a reactor containing 4-1-chloro-4-nitrobenzene (1.32 Kg; 8.38 mol), toluene (2 liters), 30% sodium hydroxide (1.17 Kg; 8.78 mol), and tetrabutylammonium hydrogensulfate (68 g; 0.2 mol). mixture in a reactor. The reaction temperature was maintained at about 85??C during addition; the mixture was then maintained at the same temperature for about 2 hours. Toluene was added to the mixture and then the phases were separated at about 85??C. The organic phase was then flushed with dilute sulfuric acid. The organic phase was then flushed with dilute sulfuric acid and the organic phase was concentrated under vacuum to about 4 liters and cooled. It was then separated by filtration at 60??C under vacuum, rinsed and the crystalline product was dried. 1.87 Kg of pure 4-amino-4'-nitrodiphenyl sulfide was obtained (95% yield; 99% purity).
4-AMINO-4'-NITRODIPHENYL SULFIDE Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 4-AMINO-4'-NITRODIPHENYL SULFIDE manufacturers
- Product
- 4-AMINO-4'-NITRODIPHENYL SULFIDE 101-59-7
- Price
- US $3.00/KG
- Min. Order
- 1KG
- Purity
- 99
- Supply Ability
- 100kg
- Release date
- 2019-07-10