ChemicalBook > CAS DataBase List > 3-Bromo-5-methylphenol

3-Bromo-5-methylphenol

Product Name: 3-Bromo-5-methylphenol
CAS No.: 74204-00-5
Chemical Name: 3-Bromo-5-methylphenol
Synonyms: 5-Bromo-3-methylphenol;3-methyl-5-bromophenol;Phenol,3-broMo-5-Methyl-;5-Bromo-3-hydroxytoluene;3-Bromo-5-hydroxytoluene;3-Bromo-5-methylphenol 98%
CBNumber: CB61456853
Molecular Formula: C7H7BrO
Formula Weight: 187.03
MOL File: 74204-00-5.mol

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3-Bromo-5-methylphenol Property

Melting point:: 61-62℃
Boiling point:: 249℃
Density: 1.554
refractive index: 1.5772 (estimate)
Flash point:: 105℃
storage temp.: Sealed in dry,2-8°C
solubility: Chloroform (Slightly), Methanol (Slightly)
pka: 9.11±0.10(Predicted)
form: Solid
color: Very Dark Red
InChI: InChI=1S/C7H7BrO/c1-5-2-6(8)4-7(9)3-5/h2-4,9H,1H3
InChIKey: OTUYBYTUBWJBLO-UHFFFAOYSA-N
SMILES: C1(O)=CC(C)=CC(Br)=C1

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Safety

HS Code: 2908190090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H332Harmful if inhaled

H335May cause respiratory irritation

Precautionary statements

P280Wear protective gloves/protective clothing/eye protection/face protection.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P310Immediately call a POISON CENTER or doctor/physician.

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N-Bromosuccinimide Price

TRC

Product number: B697428
Product name: 3-Bromo-5-methylphenol
Packaging: 250mg
Price: $65
Updated: 2021/12/16

TRC

Product number: B697428
Product name: 3-Bromo-5-methylphenol
Packaging: 1g
Price: $110
Updated: 2021/12/16

TRC

Product number: B697428
Product name: 3-Bromo-5-methylphenol
Packaging: 2.5g
Price: $225
Updated: 2021/12/16

Matrix Scientific

Product number: 073765
Product name: 3-Bromo-5-methylphenol
Purity: 95+%
Packaging: 1g
Price: $38
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FB67528
Product name: 3-Bromo-5-methylphenol
Packaging: 5G
Price: $60
Updated: 2021/12/16

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3-Bromo-5-methylphenol Chemical Properties,Usage,Production

Chemical Properties

White Solid

Uses

3-Bromo-5-methylphenol is a useful raw material for organic synthesis and pharmaceuticals.

Synthesis

849062-36-8

74204-00-5

In a three-necked flask equipped with a mechanical stirrer, (3-bromo-5-methylphenyl)boronic acid (15.0 g, 69.8 mmol) was dissolved in an aqueous solution (100 mL) of potassium hydroxide (11.8 g, 209.4 mmol). A 30% hydrogen peroxide solution (57.0 mL) was added slowly and dropwise at room temperature and the reaction lasted for 20 min. Upon completion of the reaction, the pH of the reaction solution was adjusted with 2 mol/L dilute hydrochloric acid to 7. Subsequently, extraction was performed with dichloromethane (50 mL × 3), and the organic phases were combined and dried over anhydrous sodium sulfate. After filtration to remove the desiccant, the solvent was removed by distillation under reduced pressure to afford 3-bromo-5-methylphenol as an oily liquid (11.3 g, 86.5% yield).

References

[1] Patent: CN107501132, 2017, A. Location in patent: Paragraph 0016-0018; 0031-0033; 0046-0048; 0061-0063

3-Bromo-5-methylphenol Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 3-Bromo-5-methylphenol manufacturers

Career Henan Chemical Co

Product: 3-Bromo-5-methylphenol 74204-00-5
Price: US $1.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: 200kg
Release date: 2019-12-31

74204-00-5, 3-Bromo-5-methylphenolRelated Search:

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3-Bromo-5-methylphenol 98%

74204-00-5