6-chlorophenanthridine

Product Name: 6-chlorophenanthridine
CAS No.: 15679-03-5
Chemical Name: 6-chlorophenanthridine
Synonyms: MFCD01628084;6-Chloropyridine;6-chlorophenidine;6-chlorophenanthridine;Phenanthridine,6-chloro-;6-Chlorophenanthridine 95+%
CBNumber: CB61458352
Molecular Formula: C13H8ClN
Formula Weight: 213.66
MOL File: 15679-03-5.mol

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6-chlorophenanthridine Property

Melting point:: 117-118 °C
Boiling point:: 377.7±15.0 °C(Predicted)
Density: 1.312±0.06 g/cm3(Predicted)
storage temp.: under inert gas (nitrogen or Argon) at 2–8 °C
form: solid
pka: 2.36±0.40(Predicted)
color: Light beige
InChI: InChI=1S/C13H8ClN/c14-13-11-7-2-1-5-9(11)10-6-3-4-8-12(10)15-13/h1-8H
InChIKey: XHZTZKAXCPJABO-UHFFFAOYSA-N
SMILES: C1C2C(=NC(Cl)=C3C=2C=CC=C3)C=CC=1

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Safety

HS Code: 2933998090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P271Use only outdoors or in a well-ventilated area.

P280Wear protective gloves/protective clothing/eye protection/face protection.

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N-Bromosuccinimide Price

Biosynth Carbosynth

Product number: FC131663
Product name: 6-Chlorophenanthridine
Packaging: 250mg
Price: $85
Updated: 2021/12/16

SynQuest Laboratories

Product number: 3H32-5-0S
Product name: 6-Chlorophenanthridine
Packaging: 1g
Price: $114
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FC131663
Product name: 6-Chlorophenanthridine
Packaging: 500mg
Price: $150
Updated: 2021/12/16

Matrix Scientific

Product number: 155771
Product name: 6-Chlorophenanthridine
Packaging: 0.500g
Price: $240
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FC131663
Product name: 6-Chlorophenanthridine
Packaging: 1g
Price: $255
Updated: 2021/12/16

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6-chlorophenanthridine Chemical Properties,Usage,Production

Synthesis

1015-89-0

15679-03-5

General procedure for the synthesis of 6-chlorophenanthridine from 6(5H)-phenanthridone: Phosphoryl chloride (15 mL) and dimethylaniline (0.63 mL) were sequentially added to a reaction flask containing phenanthridine (2.0 g), followed by heating and refluxing for 3 hours. Upon completion of the reaction, the reaction solution was slowly poured into water and the solid product was precipitated. The solid was extracted with chloroform and the combined organic phases were dried over anhydrous sodium sulfate. The desiccant was removed by filtration and the filtrate was concentrated to dryness under reduced pressure. The resulting crude product was purified by column chromatography (eluent: chloroform) to afford the target compound 6-chlorophenanthridine (2.1 g, yield: 96%).1H NMR (300 MHz, CDCl3, TMS, room temperature): δ 8.63-8.60 (1H, d), 8.55-8.52 (1H, d), 8.50-8.48 (1H, d), 8.11-8.09 (1H, d). 8.09 (1H, d), 7.94-7.92 (1H, t), 7.79-7.66 (3H, m).

References

[1] Patent: US2011/201802, 2011, A1. Location in patent: Page/Page column 10
[2] Patent: US9281483, 2016, B2. Location in patent: Page/Page column 83
[3] Patent: KR2016/30582, 2016, A. Location in patent: Paragraph 0162; 0163; 0164; 0165; 0166
[4] Dalton Transactions, 2014, vol. 43, # 44, p. 16872 - 16879
[5] Patent: CN105949246, 2016, A. Location in patent: Paragraph 0025; 0044-0046; 0049

6-chlorophenanthridine Preparation Products And Raw materials

Raw materials

Preparation Products

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6-chlorophenanthridine Suppliers

China 66 Germany 1 India 2 United Kingdom 2 United States 5 Global 76

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View Lastest Price from 6-chlorophenanthridine manufacturers

Henan Fengda Chemical Co., Ltd

Product: 6-Chlorophenanthridine 15679-03-5
Price: US $30.00-0.90/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: g-kg-tons, free sample is available
Release date: 2024-04-26

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