2-Hydroxy-5-phenylpyridine

Product Name: 2-Hydroxy-5-phenylpyridine
CAS No.: 76053-45-7
Chemical Name: 2-Hydroxy-5-phenylpyridine
Synonyms: 5-phenylpyridin-2-ol;5-phenylpyridin-2(1H)-one;5-Phenyl-1H-pyridin-2-one;2-Hydroxy-5-phenylpyridine;2(1H)-Pyridinone, 5-phenyl-
CBNumber: CB61471142
Molecular Formula: C11H9NO
Formula Weight: 171.2
MOL File: 76053-45-7.mol

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2-Hydroxy-5-phenylpyridine Property

Melting point:: 128 °C
Boiling point:: 394.7±35.0 °C(Predicted)
Density: 1.158±0.06 g/cm3(Predicted)
storage temp.: Sealed in dry,Room Temperature
pka: 11.60±0.10(Predicted)

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Hazard and Precautionary Statements (GHS)

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N-Bromosuccinimide Price

ChemScene

Product number: CS-0060511
Product name: 5-Phenyl-1H-pyridin-2-one
Packaging: 100mg
Price: $161
Updated: 2021/12/16

ChemScene

Product number: CS-0060511
Product name: 5-Phenyl-1H-pyridin-2-one
Packaging: 250mg
Price: $268
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: CHM0385851
Product name: 2-HYDROXY-5-PHENYLPYRIDINE
Purity: 95.00%
Packaging: 5MG
Price: $501.96
Updated: 2021/12/16

ChemScene

Product number: CS-0060511
Product name: 5-Phenyl-1H-pyridin-2-one
Packaging: 1g
Price: $536
Updated: 2021/12/16

AK Scientific

Product number: V7648
Product name: 2-Hydroxy-5-phenylpyridine
Packaging: 1g
Price: $566
Updated: 2021/12/16

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2-Hydroxy-5-phenylpyridine Chemical Properties,Usage,Production

Synthesis

53698-47-8

76053-45-7

GENERAL METHOD: 2-methoxy-5-phenylpyridine (9.19 mmol) was combined with pyridine hydrochloride (10.55 g, 91.9 mmol) in a 100 mL round bottom flask and heated with continuous stirring for 20 minutes at 160°C in an oil bath. After completion of the reaction, the mixture was cooled to room temperature. Subsequently, saturated sodium chloride solution (40 mL) and deionized water (20 mL) were added for dilution. The precipitated white solid was collected by filtration and dissolved in ethyl acetate. The resulting solution was filtered through a short silica gel column and washed well with ethyl acetate until thin layer chromatography (TLC) detection showed complete conversion of the raw material to the product.

References

[1] Tetrahedron, 2014, vol. 70, # 45, p. 8624 - 8635
[2] Patent: US2009/318455, 2009, A1. Location in patent: Page/Page column 67; 83
[3] Journal of Medicinal Chemistry, 2012, vol. 55, # 23, p. 10584 - 10600

2-Hydroxy-5-phenylpyridine Preparation Products And Raw materials

Raw materials

Preparation Products

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2-Hydroxy-5-phenylpyridine Suppliers

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76053-45-7, 2-Hydroxy-5-phenylpyridineRelated Search:

5-phenylpyridin-2-ol

2-Hydroxy-5-phenylpyridine

2(1H)-Pyridinone, 5-phenyl-

5-Phenyl-1H-pyridin-2-one

5-phenylpyridin-2(1H)-one

76053-45-7