ChemicalBook > CAS DataBase List > 1-butyl-2-methyl-imidazole

1-butyl-2-methyl-imidazole

Product Name
1-butyl-2-methyl-imidazole
CAS No.
13435-22-8
Chemical Name
1-butyl-2-methyl-imidazole
Synonyms
30198-05-9;1-butyl-2-methyl-imidazole;1H-Imidazole,1-butyl-2-methyl-;1-Butyl-2-methylimidazole, >98%;IMidazole,1-butyl-2-Methyl- (7CI,8CI);1-butyl-2-methyl-imidazole ISO 9001：2015 REACH
CBNumber
CB61519831
Molecular Formula
C8H14N2
Formula Weight
138.21
MOL File
13435-22-8.mol
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1-butyl-2-methyl-imidazole Property

Boiling point:
244.8±9.0 °C(Predicted)
Density 
0.94±0.1 g/cm3(Predicted)
storage temp. 
Sealed in dry,Room Temperature
pka
7.84±0.31(Predicted)
InChI
InChI=1S/C8H14N2/c1-3-4-6-10-7-5-9-8(10)2/h5,7H,3-4,6H2,1-2H3
InChIKey
WHLZPGRDRYCVRQ-UHFFFAOYSA-N
SMILES
C1(C)N(CCCC)C=CN=1
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

American Custom Chemicals Corporation
Product number
CHM0362804
Product name
1-BUTYL-2-METHYLIMIDAZOLE
Purity
98.00%
Packaging
5MG
Price
$500.85
Updated
2021/12/16
AK Scientific
Product number
7208BA
Product name
1-Butyl-2-methylimidazole
Packaging
1g
Price
$856
Updated
2021/12/16
Chemenu
Product number
CM187670
Product name
1-butyl-2-methyl-1H-imidazole
Purity
95+%
Packaging
1g
Price
$920
Updated
2021/12/16
Alichem
Product number
13435228
Product name
1-Butyl-2-methyl-1H-imidazole
Packaging
5g
Price
$2040
Updated
2021/12/16
Crysdot
Product number
CD11291112
Product name
1-Butyl-2-methyl-1H-imidazole
Purity
97%
Packaging
1g
Price
$692
Updated
2021/12/16
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1-butyl-2-methyl-imidazole Chemical Properties,Usage,Production

Synthesis

109-65-9

693-98-1

13435-22-8

The general procedure for the synthesis of 1-butyl-2-methylimidazole from n-butyl bromide and 2-methylimidazole was as follows: 0.82 g of 2-methylimidazole (10 mmol) was dissolved in 20 mL of N,N-dimethylformamide (DMF), heated to 40 °C and then 0.84 g of potassium hydroxide (15 mmol) was added. The reaction mixture was stirred for 15 min, followed by the slow dropwise addition of 1.438 g of n-bromobutane (10.5 mmol). After the dropwise addition was completed, the reaction continued to be stirred at 40 °C for 12 hours. After completion of the reaction, the mixture was cooled to room temperature, diluted with an appropriate amount of water, and then extracted three times with dichloromethane. The organic phases were combined, washed three times with water and dried by adding anhydrous sodium sulfate. The dried organic phase was allowed to stand for 1 hour, followed by diafiltration to remove the desiccant. Finally, the solvent was removed by rotary evaporation to give 1-butyl-2-methylimidazole in 97% yield.

References

[1] Patent: CN108440416, 2018, A. Location in patent: Paragraph 0030; 0031
[2] Journal of Materials Chemistry A, 2014, vol. 2, # 12, p. 4413 - 4421
[3] New Journal of Chemistry, 2012, vol. 36, # 3, p. 702 - 722
[4] Chemical Communications, 2018, vol. 54, # 50, p. 6879 - 6882
[5] Bioscience, Biotechnology and Biochemistry, 2000, vol. 64, # 4, p. 919 - 923

1-butyl-2-methyl-imidazole Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 1-butyl-2-methyl-imidazole manufacturers

ZHENGZHOU JIUYI TIME NEW MATERIALS CO,.LTD
Product
1H-Imidazole,1-butyl-2-methyl- 13435-22-8
Price
US $3.00-9.00/KG
Min. Order
0.1KG
Purity
99%
Supply Ability
g-kg-tons, free sample is available
Release date
2025-06-25
Career Henan Chemical Co
Product
1-butyl-2-methyl-imidazole 13435-22-8
Price
US $1.00/KG
Min. Order
1KG
Purity
99%
Supply Ability
Customized
Release date
2018-08-20

13435-22-8, 1-butyl-2-methyl-imidazoleRelated Search:

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  • 1-butyl-2-methyl-imidazole
  • IMidazole,1-butyl-2-Methyl- (7CI,8CI)
  • 1H-Imidazole,1-butyl-2-methyl-
  • 30198-05-9
  • 1-butyl-2-methyl-imidazole ISO 9001：2015 REACH
  • 1-Butyl-2-methylimidazole, >98%
  • 13435-22-8