3-Methylpyridazin-6-ylhydrazine

Product Name: 3-Methylpyridazin-6-ylhydrazine
CAS No.: 38956-79-5
Chemical Name: 3-Methylpyridazin-6-ylhydrazine
Synonyms: 3-Methylpyridazin-6-ylhydrazine;3-Hydrazinyl-6-methylpyridazine;(6-methyl-3-pyridazinyl)hydrazine;(6-methylpyridazin-3-yl)hydrazine;Pyridazine, 3-hydrazinyl-6-methyl-;3-Methylpyridazin-6-ylhydrazine ISO 9001：2015 REACH
CBNumber: CB61526323
Molecular Formula: C5H8N4
Formula Weight: 124.14
MOL File: 38956-79-5.mol

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3-Methylpyridazin-6-ylhydrazine Property

Melting point:: 74-75 °C
Boiling point:: 248.0±23.0 °C(Predicted)
Density: 1.31±0.1 g/cm3(Predicted)
storage temp.: Inert atmosphere,Store in freezer, under -20°C
pka: 6.19±0.20(Predicted)
Appearance: Yellow to brown Solid

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Safety

HazardClass: IRRITANT

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC

Product number: H716543
Product name: 3-Hydrazinyl-6-methylpyridazine
Packaging: 250mg
Price: $40
Updated: 2021/12/16

TRC

Product number: H716543
Product name: 3-Hydrazinyl-6-methylpyridazine
Packaging: 500mg
Price: $55
Updated: 2021/12/16

TRC

Product number: H716543
Product name: 3-Hydrazinyl-6-methylpyridazine
Packaging: 1g
Price: $90
Updated: 2021/12/16

Matrix Scientific

Product number: 027744
Product name: 3-Hydrazino-6-methylpyridazine
Packaging: 500mg
Price: $38
Updated: 2021/12/16

AK Scientific

Product number: W5942
Product name: 3-Hydrazinyl-6-methylpyridazine
Packaging: 1g
Price: $128
Updated: 2021/12/16

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3-Methylpyridazin-6-ylhydrazine Chemical Properties,Usage,Production

Uses

3-Hydrazinyl-6-methylpyridazine is used in preparation of 2-(3-oxo-2H,3H-[1,2,4]triazolo[4,3-b]pyridazin-2-yl)acetamide and 2-(3-oxo-[1,2,4]triazolo[4,3-a]pyrimidin-2-yl)acetamide derivatives as GPR139 receptor modulators.

Synthesis

1121-79-5

38956-79-5

General procedure for the synthesis of 3-hydrazino-6-methylpyridazine from 3-chloro-6-methylpyridazine:[Ref. Example 35] Hydrazine monohydrate (45 mL) was added to a suspension of 3-chloro-6-methylpyridazine (3.00 g) in ethanol (45 mL), and the resulting mixture was heated and refluxed for 2.5 hours. Upon completion of the reaction, the mixture was cooled in air and the solvent was subsequently removed by evaporation under reduced pressure to give a residue. The residue was purified by silica gel column chromatography using chloroform-methanol-water (7:3:1, v/v) as the lower solvent as eluent, resulting in the title compound 3-hydrazino-6-methylpyridazine (2.35 g, 81% yield) as a solid. The structure of the product was confirmed by 1H-NMR (400 MHz, DMSO-d6): δ 2.39 (3H, s), 4.20 (2H, br), 6.94 (1H, d, J = 9.3 Hz), 7.18 (1H, d, J = 9.3 Hz), 7.64 (1H, br).ESI-MS m/z: 125 ([M + H]+).

References

[1] Patent: EP1785418, 2007, A1. Location in patent: Page/Page column 53
[2] Patent: WO2008/51808, 2008, A2. Location in patent: Page/Page column 107
[3] Journal of Heterocyclic Chemistry, 1983, vol. 20, p. 1259 - 1261
[4] Journal of the Chemical Society, 1950, p. 3236,3239
[5] Patent: US2484029, 1946,

3-Methylpyridazin-6-ylhydrazine Preparation Products And Raw materials

Raw materials

Preparation Products

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3-Methylpyridazin-6-ylhydrazine Suppliers

China 81 Germany 1 India 1 Switzerland 1 United Kingdom 2 United States 4 Global 90

Achemica

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Email: contact@achemica.com
Country: Switzerland
ProdList: 6155
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View Lastest Price from 3-Methylpyridazin-6-ylhydrazine manufacturers

Shanghai Rlavie Technology Co ltd

Product: 3-Hydrazinyl-6-methylpyridazine 38956-79-5
Price: US $0.00-0.00/KG
Min. Order: 1g
Purity: 98%minHPLC
Supply Ability: 50kgs/month
Release date: 2021-11-14

Dideu Industries Group Limited

Product: 3-Methylpyridazin-6-ylhydrazine 38956-79-5
Price: US $1.10/g
Min. Order: 1g
Purity: 99.00%
Supply Ability: 100 Tons Min
Release date: 2021-11-02

Career Henan Chemical Co

Product: 3-Methylpyridazin-6-ylhydrazine 38956-79-5
Price: US $6.60/KG
Min. Order: 1KG
Purity: 97%-99%
Supply Ability: 1kg -1000kg
Release date: 2020-01-02

38956-79-5, 3-Methylpyridazin-6-ylhydrazineRelated Search:

picodralazine 3-METHYL-6-(1-METHYLHYDRAZINO)PYRIDAZINE 4-Methyl-1-hydrazinophthalizine Hydrochloride 4-Methyl-1-hydrazino-phthalazine 3-Methylpyridazin-6-ylhydrazine Prizidilol 2-(6-hydrazino-3-pyridazinyl)-1H-indole ACETONE N-[6-(2,4-DICHLOROBENZYL)-3-PYRIDAZINYL]HYDRAZONE 3-(2,4-DICHLOROBENZYL)-6-HYDRAZINOPYRIDAZINE [4-(3,4-DIMETHYL-PHENYL)-PHTHALAZIN-1-YL]-HYDRAZINE 3-HYDRAZINO-6-(4-METHYLBENZYL)PYRIDAZINE 3-(2-FLUOROBENZYL)-6-HYDRAZINOPYRIDAZINE 1-HYDRAZINO-4-(4-METHYLPHENYL)PHTHALAZINE 3-HYDRAZINO-6-(2-THIENYL)PYRIDAZINE AURORA KA-6554 3-(2,4-DICHLOROBENZYL)-6-(1-METHYLHYDRAZINO)PYRIDAZINE (4-PHENYL-PHTHALAZIN-1-YL)-HYDRAZINE (1E,4Z)-1-(2-[6-(2,4-DICHLOROBENZYL)-3-PYRIDAZINYL]HYDRAZINO)-5-(2-THIENYL)-1,4-PENTADIEN-3-ONE

3-Hydrazinyl-6-methylpyridazine

3-Methylpyridazin-6-ylhydrazine

(6-methylpyridazin-3-yl)hydrazine

(6-methyl-3-pyridazinyl)hydrazine

3-Methylpyridazin-6-ylhydrazine ISO 9001：2015 REACH

Pyridazine, 3-hydrazinyl-6-methyl-

38956-79-5

Pyrazines, Pyrimidines & Pyridazines