2-bromo-1-(bromomethyl)-4-nitrobenzene
- Product Name
- 2-bromo-1-(bromomethyl)-4-nitrobenzene
- CAS No.
- 940-05-6
- Chemical Name
- 2-bromo-1-(bromomethyl)-4-nitrobenzene
- Synonyms
- 2-broMo-4-nitrobenzyl broMide;2-bromo-1-(bromomethyl)-4-nitrobenzene;Benzene, 2-bromo-1-(bromomethyl)-4-nitro-
- CBNumber
- CB61546556
- Molecular Formula
- C7H5Br2NO2
- Formula Weight
- 294.93
- MOL File
- 940-05-6.mol
2-bromo-1-(bromomethyl)-4-nitrobenzene Property
- Melting point:
- 73-74°
- Boiling point:
- 348.0±27.0 °C(Predicted)
- Density
- 2.006±0.06 g/cm3(Predicted)
- storage temp.
- under inert gas (nitrogen or Argon) at 2-8°C
- Appearance
- White to off-white Solid
Safety
- HazardClass
- IRRITANT
- HS Code
- 2916399090
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Danger
- Hazard statements
-
H302Harmful if swallowed
H314Causes severe skin burns and eye damage
- Precautionary statements
-
P280Wear protective gloves/protective clothing/eye protection/face protection.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P310Immediately call a POISON CENTER or doctor/physician.
N-Bromosuccinimide Price
- Product number
- 046927
- Product name
- 2-Bromo-1-(bromomethyl)-4-nitrobenzene
- Purity
- >95%
- Packaging
- 500mg
- Price
- $208
- Updated
- 2021/12/16
- Product number
- 4754-9-18
- Product name
- 2-Bromo-4-nitrobenzyl bromide
- Packaging
- 250mg
- Price
- $221
- Updated
- 2021/12/16
- Product number
- 046927
- Product name
- 2-Bromo-1-(bromomethyl)-4-nitrobenzene
- Purity
- >95%
- Packaging
- 1g
- Price
- $320
- Updated
- 2021/12/16
- Product number
- 4754-9-18
- Product name
- 2-Bromo-4-nitrobenzyl bromide
- Packaging
- 1g
- Price
- $552
- Updated
- 2021/12/16
- Product number
- HCH0065896
- Product name
- 2-BROMO-1-(BROMOMETHYL)-4-NITROBENZENE
- Purity
- 95.00%
- Packaging
- 500MG
- Price
- $720.84
- Updated
- 2021/12/16
2-bromo-1-(bromomethyl)-4-nitrobenzene Chemical Properties,Usage,Production
Synthesis
585-79-5
940-05-6
General procedure for the synthesis of 2-bromo-4-nitrobenzyl bromide from m-bromonitrobenzene: A mixture of 2-bromo-6-nitrobenzene (1.08 g, 5.00 mmol) and N-bromosuccinimide (908 mg, 5.10 mmol) was dissolved in carbon tetrachloride (15 mL), and α,α'-azobisisobutyronitrile (AIBN) (28 mg) was added as initiator. The reaction mixture was stirred at 70 °C for 3 hours. Subsequently, additional AIBN (82 mg) was added in batches at the same temperature and stirring was continued for 4 hours. After completion of the reaction, the reaction mixture was diluted with chloroform and filtered to remove the precipitate. The filtrate was distilled under reduced pressure to remove the solvent and the crude product obtained was purified by silica gel column chromatography (eluent: hexane/ethyl acetate=1/1) to afford the target compound 2-bromo-1-(bromomethyl)-4-nitrobenzene (493 mg, 33% yield). The product was characterized by 1H-NMR (CDCl3): δ 4.62 (2H, s), 7.65 (1H, d, J=8.4Hz), 8.17 (1H, dd, J=8.4,2.2Hz), 8.46 (1H, d, J=2.2Hz).
References
[1] Patent: EP1844768, 2007, A1. Location in patent: Page/Page column 39
2-bromo-1-(bromomethyl)-4-nitrobenzene Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 2-bromo-1-(bromomethyl)-4-nitrobenzene manufacturers
- Product
- 2-broMo-4-nitrobenzyl broMide 940-05-6
- Price
- US $0.00/kg
- Min. Order
- 1kg
- Purity
- 98%
- Supply Ability
- 1000kg
- Release date
- 2025-09-29
- Product
- 2-bromo-1-(bromomethyl)-4-nitrobenzene 940-05-6
- Price
- US $0.00/kg
- Min. Order
- 20kg
- Purity
- 99%
- Supply Ability
- 20 tons
- Release date
- 2025-03-31