N-(3-cyanophenyl)benzamide

Product Name: N-(3-cyanophenyl)benzamide
CAS No.: 141990-91-2
Chemical Name: N-(3-cyanophenyl)benzamide
Synonyms: N-(3-Cyanophenyl);N-(3-cyanophenyl)benzamide;Benzamide, N-(3-cyanophenyl)-
CBNumber: CB61813942
Molecular Formula: C14H10N2O
Formula Weight: 222.24
MOL File: 141990-91-2.mol

More

Less

N-(3-cyanophenyl)benzamide Property

storage temp.: Sealed in dry,Room Temperature

More

Less

Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P280Wear protective gloves/protective clothing/eye protection/face protection.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

More

Less

N-Bromosuccinimide Price

TRC

Product number: C955915
Product name: N-(3-Cyanophenyl)benzamide
Packaging: 25mg
Price: $45
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FC143783
Product name: N-(3-Cyanophenyl)benzamide
Packaging: 250mg
Price: $70
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FC143783
Product name: N-(3-Cyanophenyl)benzamide
Packaging: 500mg
Price: $125
Updated: 2021/12/16

Matrix Scientific

Product number: 075386
Product name: N-(3-Cyanophenyl)benzamide
Purity: 95+%
Packaging: 250mg
Price: $260
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FC143783
Product name: N-(3-Cyanophenyl)benzamide
Packaging: 2g
Price: $372
Updated: 2021/12/16

More

Less

N-(3-cyanophenyl)benzamide Chemical Properties,Usage,Production

Synthesis

93-58-3

2237-30-1

141990-91-2

GENERAL PROCEDURE: Pure m-aminobenzonitrile (1.00 mmol) and methyl benzoate (1.00 mmol) with DABAL-Me3 (202 mg, 0.8 eq.) are placed in a 5 mL microwaveable vial and dry tetrahydrofuran (1 mL) is added under argon protection. For coupled spouses containing acidic hydrogen, additional DABAL-Me3 (410 mg, 1.6 eq. total) is added. The vials were quickly capped and placed in a CEM Discover microwave reactor. Irradiation was carried out at 130 °C for 8 min at 290 W power, followed by programmed cooling (~20 min). The reaction was quenched by careful addition of 2 M hydrochloric acid (4 mL) or saturated potassium sodium tartrate solution (4 mL) (note: methane may be released). The reaction mixture is extracted with dichloromethane, dried over magnesium sulfate and concentrated to give pure N-(3-cyanophenyl)benzamide directly. For further purification, the amides lacking highly polar functional groups can be separated by column chromatography using 3:2 to 2:3 hexane:ethyl acetate as eluent; for amides containing polar functional groups such as side-chain amines, alcohols, etc., dichloromethane containing 2% v/v methanol is used as eluent.

References

[1] Tetrahedron, 2013, vol. 69, # 46, p. 9890 - 9897

N-(3-cyanophenyl)benzamide Preparation Products And Raw materials

Raw materials

Preparation Products

More

Less

N-(3-cyanophenyl)benzamide Suppliers

China 23 India 1 Russia 1 Ukraine 1 United Kingdom 1 United States 6 Global 33

SynAsst Chemical.

Tel: 021-60343070
Fax: 021-35122006
Country: China
ProdList: 12740
Advantage: 55

Shanghai Jovan Biochemical Technology Co. Ltd.

Tel: +86-021-61654350
Fax: +86-021-61654350
Email: 1245958370@qq.com
Country: China
ProdList: 2982
Advantage: 50

DebyeTec.com Inc.

Tel: 18086626237 18086626237
Fax: qq:2693528373
Email: 2693528373@qq.com
Country: China
ProdList: 2966
Advantage: 56

Chengdu Research Accelerators Technology Co., Ltd.

Tel: 028-64353063
Fax: 028-64353063 QQ:784253935
Email: reacchemical@163.com
Country: China
ProdList: 5253
Advantage: 58

Zhengzhou kangnuochenrui Chemical Technology Co.,Ltd

Tel: 18210788515; 18210788515
Fax: 18210788515
Email: zhuzixin999@163.c0m
Country: China
ProdList: 4993
Advantage: 55

ShangHai Angti Biotechnology Co., Ltd.

Tel: 13764913901
Fax: -
Email: info@angtibio.com
Country: China
ProdList: 4976
Advantage: 55

Amadis Chemical Company Limited

Tel: 571-89925085
Fax: 0086-571-89925065
Email: sales@amadischem.com
Country: China
ProdList: 131957
Advantage: 58

Yantai ShengKailun Chemical Technology Co., Ltd.

Tel: 13356901049
Fax: QQ：1025383091
Email: 3119594100@qq.com
Country: China
ProdList: 7964
Advantage: 55

Hangzhou Molcore Biopharmatech Co.,Ltd

Tel: 400-711-5280 86-571-81025280
Fax: 86-571-85806285
Email: sales@molcore.com
Country: China
ProdList: 9967
Advantage: 58

Aikon International Limited

Tel: 025-66061636 19370895928
Fax: (3)02557626880
Email: qqyang@aikonchem.com
Country: China
ProdList: 15812
Advantage: 58

141990-91-2, N-(3-cyanophenyl)benzamideRelated Search:

N-(3-cyanophenyl)benzamide

N-(3-Cyanophenyl)

Benzamide, N-(3-cyanophenyl)-

141990-91-2