Quinoxaline, 6-(chloromethyl)-
- Product Name
- Quinoxaline, 6-(chloromethyl)-
- CAS No.
- 477776-17-3
- Chemical Name
- Quinoxaline, 6-(chloromethyl)-
- Synonyms
- 6-(Chloromethyl)quinoxaline;Quinoxaline, 6-(chloromethyl)-
- CBNumber
- CB61860320
- Molecular Formula
- C9H7ClN2
- Formula Weight
- 0
- MOL File
- 477776-17-3.mol
Quinoxaline, 6-(chloromethyl)- Property
- storage temp.
- under inert gas (nitrogen or Argon) at 2-8°C
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H319Causes serious eye irritation
H332Harmful if inhaled
H335May cause respiratory irritation
- Precautionary statements
-
P280Wear protective gloves/protective clothing/eye protection/face protection.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P310Immediately call a POISON CENTER or doctor/physician.
N-Bromosuccinimide Price
- Product number
- A142308
- Product name
- 6-(Chloromethyl)quinoxaline
- Purity
- 95+%
- Packaging
- 100mg
- Price
- $94
- Updated
- 2021/12/16
- Product number
- A142308
- Product name
- 6-(Chloromethyl)quinoxaline
- Purity
- 95+%
- Packaging
- 250mg
- Price
- $187
- Updated
- 2021/12/16
- Product number
- CD11118864
- Product name
- 6-(Chloromethyl)quinoxaline
- Purity
- 95+%
- Packaging
- 250mg
- Price
- $277
- Updated
- 2021/12/16
- Product number
- CD11118864
- Product name
- 6-(Chloromethyl)quinoxaline
- Purity
- 95+%
- Packaging
- 1g
- Price
- $554
- Updated
- 2021/12/16
- Product number
- 477776173
- Product name
- 6-(Chloromethyl)quinoxaline
- Packaging
- 1g
- Price
- $896.66
- Updated
- 2021/12/16
Quinoxaline, 6-(chloromethyl)- Chemical Properties,Usage,Production
Synthesis
6344-72-5
477776-17-3
The general procedure for the synthesis of 6-(chloromethyl)quinoxaline from 6-methylquinoxaline is as follows: Example 1: Catalytic air dehydrogenation of 6-hydroxymethyl-methyl-quinoxaline In a 500 mL round-bottomed flask, 6-methylquinoxaline (10 g, 69.4 mmol) was dissolved in 240 g of acetonitrile with N-chlorosuccinimide (14 g, 105.3 mmol). Benzoyl peroxide (0.4 g, 1.65 mmol) was added as initiator. A reflux condenser was installed and the reaction mixture was heated and refluxed for 6 hours, followed by the addition of benzoyl peroxide (0.1 g). The reflux reaction was continued for a total reaction time of 12 hours. Upon completion of the reaction, the reaction solution was analyzed by gas chromatography (GC), which showed the generation of 6-(chloromethyl)quinoxaline with 80% selectivity and 60% conversion.
References
[1] Patent: US6559308, 2003, B1
Quinoxaline, 6-(chloromethyl)- Preparation Products And Raw materials
Raw materials
Preparation Products
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