4-Morpholin-4-ylpyridin-2-amine

Product Name: 4-Morpholin-4-ylpyridin-2-amine
CAS No.: 722549-98-6
Chemical Name: 4-Morpholin-4-ylpyridin-2-amine
Synonyms: inopyridine;2-Amino-4-morphoL;2-AMINO-4-MORPHOLINOPYRIDINE;4-Morpholin-4-ylpyridin-2-amine;4-Morpholin-4-ylpyridin-2-ylamine;2-Pyridinamine, 4-(4-morpholinyl)-;2-Amino-4-(morpholin-4-yl)pyridine;4-(Morpholin-4-yl)pyridin-2-amine, 4-(2-Aminopyridin-4-yl)morpholine
CBNumber: CB61873854
Molecular Formula: C9H13N3O
Formula Weight: 179.22
MOL File: 722549-98-6.mol

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4-Morpholin-4-ylpyridin-2-amine Property

Boiling point:: 391.7±42.0 °C(Predicted)
Density: 1.208±0.06 g/cm3(Predicted)
storage temp.: under inert gas (nitrogen or Argon) at 2–8 °C
pka: 8.75±0.11(Predicted)

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Safety

HS Code: 2933399990

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P271Use only outdoors or in a well-ventilated area.

P280Wear protective gloves/protective clothing/eye protection/face protection.

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N-Bromosuccinimide Price

TRC

Product number: A576770
Product name: 2-Amino-4-morpholinopyridine
Packaging: 500mg
Price: $200
Updated: 2021/12/16

Matrix Scientific

Product number: 081218
Product name: 4-Morpholin-4-ylpyridin-2-amine
Purity: 97%
Packaging: 1g
Price: $342
Updated: 2021/12/16

Apolloscientific

Product number: OR30943
Product name: 2-Amino-4-(morpholin-4-yl)pyridine
Packaging: 1g
Price: $363
Updated: 2021/12/16

AK Scientific

Product number: V7487
Product name: 2-Amino-4-morpholinopyridine
Packaging: 5g
Price: $578
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: CHM0068195
Product name: 4-MORPHOLIN-4-YLPYRIDIN-2-AMINE
Purity: 95.00%
Packaging: 1G
Price: $832.18
Updated: 2021/12/16

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4-Morpholin-4-ylpyridin-2-amine Chemical Properties,Usage,Production

Uses

2-Amino-4-morpholinopyridine is a useful reactant for organic reactions and synthesis.

Synthesis

110-91-8

202216-99-7

722549-98-6

Example 1: 4-Chloropyridin-2-amine (800 mg, 6.22 mmol) was mixed with morpholine (8.0 mL) in N,N-dimethylacetamide (DMA, 2 mL) in a sealed vessel. The reaction mixture was placed in a microwave reactor (CSA Discover) and heated at 20 °C for 5 min. After completion of the reaction, it was cooled to room temperature and the reaction mixture was concentrated under reduced pressure to remove the solvent. The crude product was purified by silica gel column chromatography with an eluent ratio of dichloromethane/methanol/ammonia (95:5:0.5, v/v/v) to afford 837 mg of the target compound 2-amino-4-(4-morpholinyl)pyridine as a yellow solid in 75% yield. The structure of the product was confirmed by 1H NMR (DMSO-d6): δ 7.70-7.64 (m, 1H), 6.59-6.54 (m, 1H), 6.05-6.00 (m, 1H), 3.74-3.65 (m, 4H), 3.45-3.37 (m, 4H). Mass spectrometry analysis showed that the measured value of [M+H]+ was 180.11 (calculated value: 179.20). Elemental analysis results (C9H13N3O1-0.1H2O) calculated values: C, 59.72; H, 7.35; N, 23.21; measured values: C, 59.66; H, 7.25; N, 23.20.

References

[1] Patent: WO2004/58760, 2004, A1. Location in patent: Page 68

4-Morpholin-4-ylpyridin-2-amine Preparation Products And Raw materials

Raw materials

Preparation Products

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4-Morpholin-4-ylpyridin-2-amine Suppliers

China 55 Germany 1 India 1 United Kingdom 2 United States 7 Global 66

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View Lastest Price from 4-Morpholin-4-ylpyridin-2-amine manufacturers

Career Henan Chemical Co

Product: 4-Morpholin-4-ylpyridin-2-amine 722549-98-6
Price: US $1.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: 100KG
Release date: 2020-01-14

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722549-98-6

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