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3-methyl-1H-pyrazol-5-ol

Product Name
3-methyl-1H-pyrazol-5-ol
CAS No.
132712-71-1
Chemical Name
3-methyl-1H-pyrazol-5-ol
Synonyms
5-Methyl-2H-pyrazol-3-ol;3-methyl-1H-pyrazol-5-ol;3-METHYL-1H-PYRAZOLE-5-OL;1H-Pyrazol-5-ol, 3-Methyl-
CBNumber
CB62112280
Molecular Formula
C4H6N2O
Formula Weight
98.1
MOL File
132712-71-1.mol
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3-methyl-1H-pyrazol-5-ol Property

Boiling point:
309.7±22.0 °C(Predicted)
Density 
1.296±0.06 g/cm3(Predicted)
storage temp. 
2-8°C
pka
3.51±0.23(Predicted)
Appearance
Off-white to light yellow Solid
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC
Product number
B495223
Product name
3-Methyl-1h-pyrazol-5-ol
Packaging
50mg
Price
$45
Updated
2021/12/16
TRC
Product number
B495223
Product name
3-Methyl-1h-pyrazol-5-ol
Packaging
100mg
Price
$60
Updated
2021/12/16
Ambeed
Product number
A229777
Product name
3-Methyl-1H-pyrazol-5-ol
Purity
98%
Packaging
10g
Price
$7
Updated
2021/12/16
Ambeed
Product number
A229777
Product name
3-Methyl-1H-pyrazol-5-ol
Purity
98%
Packaging
25g
Price
$11
Updated
2021/12/16
Aronis compounds
Product number
a07322
Product name
3-methyl-1H-pyrazol-5-ol
Packaging
20mg
Price
$30
Updated
2021/12/16
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3-methyl-1H-pyrazol-5-ol Chemical Properties,Usage,Production

Synthesis

161374-07-8

5953-85-5

17356-08-0

57-13-6

132712-71-1

The general procedure for the synthesis of compound (CAS:5953-85-5), compound (CAS:17356-08-0), urea and 3-methyl-1H-pyrazol-5-ol from compound (CAS:161374-07-8) was as follows: a-h of DHH (0.01 mol) was mixed with excess hydrazine hydrate (5 mL) and heated to reflux for 6 hr. . After completion of the reaction, the mixture was cooled and poured into crushed ice. The solid products a-d were collected by filtration, crystallized with ethanol and finally dried. Evaporation of the filtrate gave a solid residue, which was isolated by graded crystallization from water to obtain pyrazole and urea (a) or thiourea (b). 2.4.1. Synthesis of 3-methyl-1H-pyrazol-5-ol (13). Yield: 42-55% (based on a-h); Melting point: 221-223 °C (literature value [49]: 220-222 °C); 1H-NMR (DMSO-d6) δ (ppm): 2.47 (s, 3H, -CH3), 6.83 (s, 1H, Ar-H), 10.07 (s, 1H, OH), 12.10 (s, 1H, NH) .

References

[1] Journal of Chemistry, 2018, vol. 2018,

3-methyl-1H-pyrazol-5-ol Preparation Products And Raw materials

Raw materials

Preparation Products

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3-methyl-1H-pyrazol-5-ol Suppliers

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132712-71-1, 3-methyl-1H-pyrazol-5-olRelated Search:


  • 3-methyl-1H-pyrazol-5-ol
  • 5-Methyl-2H-pyrazol-3-ol
  • 1H-Pyrazol-5-ol, 3-Methyl-
  • 3-METHYL-1H-PYRAZOLE-5-OL
  • 132712-71-1