3-methyl-1H-pyrazol-5-ol
- Product Name
- 3-methyl-1H-pyrazol-5-ol
- CAS No.
- 132712-71-1
- Chemical Name
- 3-methyl-1H-pyrazol-5-ol
- Synonyms
- 5-Methyl-2H-pyrazol-3-ol;3-methyl-1H-pyrazol-5-ol;3-METHYL-1H-PYRAZOLE-5-OL;1H-Pyrazol-5-ol, 3-Methyl-
- CBNumber
- CB62112280
- Molecular Formula
- C4H6N2O
- Formula Weight
- 98.1
- MOL File
- 132712-71-1.mol
3-methyl-1H-pyrazol-5-ol Property
- Boiling point:
- 309.7±22.0 °C(Predicted)
- Density
- 1.296±0.06 g/cm3(Predicted)
- storage temp.
- 2-8°C
- pka
- 3.51±0.23(Predicted)
- Appearance
- Off-white to light yellow Solid
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H319Causes serious eye irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- B495223
- Product name
- 3-Methyl-1h-pyrazol-5-ol
- Packaging
- 50mg
- Price
- $45
- Updated
- 2021/12/16
- Product number
- B495223
- Product name
- 3-Methyl-1h-pyrazol-5-ol
- Packaging
- 100mg
- Price
- $60
- Updated
- 2021/12/16
- Product number
- A229777
- Product name
- 3-Methyl-1H-pyrazol-5-ol
- Purity
- 98%
- Packaging
- 10g
- Price
- $7
- Updated
- 2021/12/16
- Product number
- A229777
- Product name
- 3-Methyl-1H-pyrazol-5-ol
- Purity
- 98%
- Packaging
- 25g
- Price
- $11
- Updated
- 2021/12/16
- Product number
- a07322
- Product name
- 3-methyl-1H-pyrazol-5-ol
- Packaging
- 20mg
- Price
- $30
- Updated
- 2021/12/16
3-methyl-1H-pyrazol-5-ol Chemical Properties,Usage,Production
Synthesis
161374-07-8
5953-85-5
17356-08-0
57-13-6
132712-71-1
The general procedure for the synthesis of compound (CAS:5953-85-5), compound (CAS:17356-08-0), urea and 3-methyl-1H-pyrazol-5-ol from compound (CAS:161374-07-8) was as follows: a-h of DHH (0.01 mol) was mixed with excess hydrazine hydrate (5 mL) and heated to reflux for 6 hr. . After completion of the reaction, the mixture was cooled and poured into crushed ice. The solid products a-d were collected by filtration, crystallized with ethanol and finally dried. Evaporation of the filtrate gave a solid residue, which was isolated by graded crystallization from water to obtain pyrazole and urea (a) or thiourea (b). 2.4.1. Synthesis of 3-methyl-1H-pyrazol-5-ol (13). Yield: 42-55% (based on a-h); Melting point: 221-223 °C (literature value [49]: 220-222 °C); 1H-NMR (DMSO-d6) δ (ppm): 2.47 (s, 3H, -CH3), 6.83 (s, 1H, Ar-H), 10.07 (s, 1H, OH), 12.10 (s, 1H, NH) .
References
[1] Journal of Chemistry, 2018, vol. 2018,
3-methyl-1H-pyrazol-5-ol Preparation Products And Raw materials
Raw materials
Preparation Products
3-methyl-1H-pyrazol-5-ol Suppliers
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