ChemicalBook > CAS DataBase List > 4-N-HEXYLOXYBROMOBENZENE

4-N-HEXYLOXYBROMOBENZENE

Product Name: 4-N-HEXYLOXYBROMOBENZENE
CAS No.: 30752-19-3
Chemical Name: 4-N-HEXYLOXYBROMOBENZENE
Synonyms: TIMTEC-BB SBB008641;P-HEXYLOXYBROMOBENZENE;4-HEXYLOXYBROMOBENZENE;1-bromo-4-hexoxybenzene;4-N-HEXYLOXYBROMOBENZENE;P-BROMO(HEXYLOXY)BENZENE;1-(4-BROMOPHENOXY)HEXANE;1-BROMO-4-HEXYLOXYBENZENE;4-BROMOPHENYL HEXYL ETHER;4-Bromo-(hexyloxy)-benzene
CBNumber: CB6225324
Molecular Formula: C12H17BrO
Formula Weight: 257.17
MOL File: 30752-19-3.mol

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4-N-HEXYLOXYBROMOBENZENE Property

Boiling point:: 154°C/12mmHg(lit.)
Density: 1,23 g/cm³
refractive index: 1.5240
Flash point:: >110°(230°F)
storage temp.: Sealed in dry,Room Temperature
form: clear liquid
color: Colorless to Light yellow
CAS DataBase Reference: 30752-19-3(CAS DataBase Reference)
EPA Substance Registry System: p-Bromophenylhexyl ether (30752-19-3)

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Safety

TSCA: Yes
HS Code: 2909303890

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TCI Chemical

Product number: B3876
Product name: 1-Bromo-4-hexyloxybenzene
Purity: >98.0%(GC)
Packaging: 5g
Price: $54
Updated: 2025/07/31

TCI Chemical

Product number: B3876
Product name: 1-Bromo-4-hexyloxybenzene
Purity: >98.0%(GC)
Packaging: 25g
Price: $155
Updated: 2025/07/31

TRC

Product number: N497260
Product name: 4-N-Hexyloxybromobenzene
Packaging: 100mg
Price: $60
Updated: 2021/12/16

TRC

Product number: N497260
Product name: 4-N-Hexyloxybromobenzene
Packaging: 500mg
Price: $75
Updated: 2021/12/16

SynQuest Laboratories

Product number: 2607-9-10
Product name: 1-(4-Bromophenoxy)hexane
Purity: 97%
Packaging: 1g
Price: $25
Updated: 2021/12/16

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4-N-HEXYLOXYBROMOBENZENE Chemical Properties,Usage,Production

Synthesis

106-41-2

111-25-1

30752-19-3

Example 3.1 Synthesis of 1-bromo-4-(hexyloxy)benzene: Increase the temperature of the oil bath to 65 °C. In a 500 mL round-bottomed flask fitted with a stirrer, 10 g (57.8 mmol, 1.0 eq.) of 4-bromophenol and 26.36 g (190.7 mmol, 3.3 eq.) of potassium carbonate were added sequentially, followed by 202.3 mL of acetone. The reaction vessel was sealed, a condenser tube was fitted and purged continuously with argon for 10 min. After completion of the purge, 8.9 mL (64 mmol, 1.1 eq.) of bromohexane was slowly added via syringe, and the reaction mixture was stirred under reflux conditions in an oil bath for 24 hours. The progress of the reaction was monitored by thin layer chromatography (silica gel plate, hexane as the unfolding agent) and after confirming the completion of the reaction, the crude reaction mixture was filtered to remove potassium carbonate. Water was added to the filtrate and extracted twice with ether. The ether extracts were combined and dried with magnesium sulfate, followed by filtration to remove the desiccant. The solvent was removed by distillation under reduced pressure and the crude product obtained was purified by silica gel column chromatography (eluent hexane) to give 13.96 g (93.9% yield) of the target product 1-bromo-4-(hexyloxy)benzene as a clear liquid.GC-MS analysis showed the correct molecular ion peaks.1H NMR (500 MHz, CDCl3, internal standard TMS, δ 7.26 ppm): δ 7.355 (m, 2H), 6.770 (m, 2H), 3.912 (t, J = 6.75 Hz, 2H), 1.764 (m, 2H), 1.49-1.40 (m, 2H), 1.37-1.30 (m, 4H), 0.905 (t, J = 7.0 Hz, 3H).

References

[1] Angewandte Chemie - International Edition, 2014, vol. 53, # 12, p. 3168 - 3172
[2] Angew. Chem., 2014, vol. 126, # 12, p. 3232 - 3236,5
[3] European Journal of Organic Chemistry, 2013, # 26, p. 5917 - 5922
[4] Chemistry - A European Journal, 2017, vol. 23, # 17, p. 4149 - 4159
[5] Helvetica Chimica Acta, 2009, vol. 92, # 6, p. 1023 - 1033

4-N-HEXYLOXYBROMOBENZENE Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 4-N-HEXYLOXYBROMOBENZENE manufacturers

Career Henan Chemical Co

Product: p-Hexyloxybromobenzene 30752-19-3
Price: US $1.00/KG
Min. Order: 1KG
Purity: 98%
Supply Ability: 200kg
Release date: 2018-12-25

30752-19-3, 4-N-HEXYLOXYBROMOBENZENERelated Search:

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1-(4-BROMOPHENOXY)HEXANE

1-BROMO-4-HEXYLOXYBENZENE

1-BROMO-4-N-HEXYLOXYBENZENE

4-BROMOPHENYL HEXYL ETHER

4-N-HEXYLOXYBROMOBENZENE

P-HEXYLOXYBROMOBENZENE

P-BROMO(HEXYLOXY)BENZENE

TIMTEC-BB SBB008641

4-Bromo-(hexyloxy)-benzene

1-bromo-4-hexoxybenzene

4-HEXYLOXYBROMOBENZENE

1-(Hexyloxy)-4-bromobenzene

4-(Hexyloxy)phenyl bromide

1-(4-Bromophenoxy)hexane 4-Bromophenyl Hexyl Ether

1-Bromo-4-hexyloxybenzene &gt

Benzene, 1-bromo-4-(hexyloxy)-

1-Bromo-4-(hexyloxy)benzene b

30752-19-3