ChemicalBook > CAS DataBase List > 4-Nitro-2-trifluoromethylphenol

4-Nitro-2-trifluoromethylphenol

Product Name: 4-Nitro-2-trifluoromethylphenol
CAS No.: 1548-61-4
Chemical Name: 4-Nitro-2-trifluoromethylphenol
Synonyms: 4-Nitro-2-trifluoromethylphenol;2-Trifluoromethyl-4-nitrophenol;4-Nitro-2-(trifluoromethyl)benzenol;Phenol, 4-nitro-2-(trifluoromethyl)-;1548-61-4 4-Nitro-2-(trifluoromethyl)benzenol
CBNumber: CB62367187
Molecular Formula: C7H4F3NO3
Formula Weight: 207.11
MOL File: 1548-61-4.mol

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4-Nitro-2-trifluoromethylphenol Property

Melting point:: 105-107°
Boiling point:: 259℃
Density: 1.554
Flash point:: 110℃
storage temp.: 2-8°C
solubility: DMSO (Slightly), Methanol (Slightly)
form: Solid
color: Yellow to Beige

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Safety

RIDADR: 2811
HazardClass: IRRITANT
PackingGroup: Ⅲ

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word: Warning

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N-Bromosuccinimide Price

TRC

Product number: N900805
Product name: 4-Nitro-2-(trifluoromethyl)phenol
Packaging: 1g
Price: $70
Updated: 2021/12/16

Matrix Scientific

Product number: 048553
Product name: 4-Nitro-2-(trifluoromethyl)phenol
Purity: 95+%
Packaging: 1g
Price: $14
Updated: 2021/12/16

ChemScene

Product number: CS-W004922
Product name: 4-Nitro-2-(trifluoromethyl)phenol
Purity: 97.44%
Packaging: 5g
Price: $54
Updated: 2021/12/16

Matrix Scientific

Product number: 048553
Product name: 4-Nitro-2-(trifluoromethyl)phenol
Purity: 95+%
Packaging: 5g
Price: $60
Updated: 2021/12/16

ChemScene

Product number: CS-W004922
Product name: 4-Nitro-2-(trifluoromethyl)phenol
Purity: 97.44%
Packaging: 10g
Price: $103
Updated: 2021/12/16

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4-Nitro-2-trifluoromethylphenol Chemical Properties,Usage,Production

Synthesis Reference(s)

The Journal of Organic Chemistry, 27, p. 4660, 1962 DOI: 10.1021/jo01059a515

Synthesis

654-76-2

1548-61-4

The general procedure for the synthesis of 2-trifluoromethyl-4-nitrophenol from 2-methoxy-5-nitrobenzotrifluoride was as follows: 6-methoxy-5-nitrobenzotrifluoride (24.73 g, 110.7 mmol) was dissolved in acetic acid (260 mL), 62% aqueous hydrobromic acid (130 mL) was added, and the reaction was heated to reflux for 96 hours. After the reaction was completed, it was cooled to room temperature and most of the solvent was removed by evaporation. The residue was dissolved in water and extracted with saturated NaHCO3 solution and ether (3×). The organic phases were combined, washed with 10% NaCl aqueous solution and dried over anhydrous Na2SO4. The solvent was evaporated under reduced pressure to give 19.27 g (83% yield) of 4-nitro-2-trifluoromethylphenol as a yellow solid. Mass spectrum (MS): 207 (M+), melting point (MP): 103-104 °C.

References

[1] Journal of Materials Chemistry, 2009, vol. 19, # 39, p. 7208 - 7215
[2] Patent: US2004/248951, 2004, A1. Location in patent: Page 16
[3] Patent: WO2007/4749, 2007, A1. Location in patent: Page/Page column 150
[4] Journal of Organic Chemistry, 1962, vol. 27, p. 4660 - 4662
[5] Patent: WO2005/80340, 2005, A1. Location in patent: Page/Page column 50

4-Nitro-2-trifluoromethylphenol Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 4-Nitro-2-trifluoromethylphenol manufacturers

Career Henan Chemical Co

Product: 4-Nitro-2-trifluoromethylphenol 1548-61-4
Price: US $1.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: 100kg
Release date: 2019-07-11

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