5-BENZYLOXY-2-BROMOBENZALDEHYDE

Product Name: 5-BENZYLOXY-2-BROMOBENZALDEHYDE
CAS No.: 85604-06-4
Chemical Name: 5-BENZYLOXY-2-BROMOBENZALDEHYDE
Synonyms: 5-Bezyloxy-2-bromobenzaldehyde;5-BENZYLOXY-2-BROMOBENZALDEHYDE;2-Bromo-5-phenylmethoxybenzaldehyde;Benzaldehyde, 2-bromo-5-(phenylmethoxy)-
CBNumber: CB62447195
Molecular Formula: C14H11BrO2
Formula Weight: 291.14
MOL File: 85604-06-4.mol

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5-BENZYLOXY-2-BROMOBENZALDEHYDE Property

Melting point:: 44-46 °C
Boiling point:: 401.3±30.0 °C(Predicted)
Density: 1.441±0.06 g/cm3(Predicted)
storage temp.: under inert gas (nitrogen or Argon) at 2-8°C
solubility: Chloroform (Slightly), Ethyl Acetate (Slightly)
form: Solid
color: Off-White to Pale Beige

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P280Wear protective gloves/protective clothing/eye protection/face protection.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC

Product number: B280085
Product name: 5-(Benzyloxy)-2-bromobenzaldehyde
Packaging: 500mg
Price: $85
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: HCH0320172
Product name: 5-BENZYLOXY-2-BROMOBENZALDEHYDE
Purity: 95.00%
Packaging: 5MG
Price: $503.1
Updated: 2021/12/16

AK Scientific

Product number: J96498
Product name: 5-Benzyloxy-2-bromobenzaldehyde
Packaging: 25g
Price: $540
Updated: 2021/12/16

AOBChem

Product number: 10173
Product name: 5-Bezyloxy-2-bromobenzaldehyde
Purity: 95%
Packaging: 5g
Price: $157
Updated: 2021/12/16

Chemenu

Product number: CM185828
Product name: 5-(Benzyloxy)-2-bromobenzaldehyde
Purity: 95+%
Packaging: 5g
Price: $171
Updated: 2021/12/16

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5-BENZYLOXY-2-BROMOBENZALDEHYDE Chemical Properties,Usage,Production

Synthesis

2973-80-0

100-39-0

85604-06-4

Example 396: Synthesis of (1E,6E)-1-(5-benzyloxy-2-bromophenyl)-7-(4-hydroxyphenyl)hepta-1,6-diene-3,5-dione (CU531); (1) Synthesis of 5-benzyloxy-2-bromobenzaldehyde; To 2-bromo-5-hydroxybenzaldehyde (100 mg, 0.50 mmol), potassium carbonate (138 mg, 1.00 mmol) and tetrabutylammonium iodide (18 mg, 0.05 mmol) in a suspension of 1.0 mL of dry N,N-dimethylformamide, benzyl bromide (89 μL, 0.74 mmol) was slowly added at 0 °C. The reaction mixture was stirred overnight at room temperature, then diluted with ether, washed sequentially with water, saturated aqueous NaHCO3 and brine, and dried over anhydrous MgSO4. After filtration, the filtrate was concentrated under reduced pressure and the residue was purified by silica gel column chromatography (eluent: hexane/ethyl acetate = 95/5 to 80/20) to afford 5-(benzyloxy)-2-bromobenzaldehyde as a colorless oil (140 mg, 97% yield).

References

[1] Bulletin of the Korean Chemical Society, 2010, vol. 31, # 7, p. 2047 - 2050
[2] Patent: EP2123637, 2009, A1. Location in patent: Page/Page column 110
[3] Patent: US2011/82295, 2011, A1. Location in patent: Page/Page column 14
[4] Journal of Organic Chemistry, 2016, vol. 81, # 20, p. 10062 - 10070
[5] Journal of Organic Chemistry, 1999, vol. 64, # 13, p. 4949 - 4952

5-BENZYLOXY-2-BROMOBENZALDEHYDE Preparation Products And Raw materials

Raw materials

Preparation Products

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5-BENZYLOXY-2-BROMOBENZALDEHYDE Suppliers

China 45 India 1 United States 5 Global 51

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85604-06-4, 5-BENZYLOXY-2-BROMOBENZALDEHYDERelated Search:

5-BENZYLOXY-2-BROMOTOLUENE 3-BENZYLOXY-6-BROMO-2-FLUOROBENZALDEHYDE 2-Bromo-4-methoxy-5-(benzyloxy)benzaldehyde 2-Bromo-4-methoxy-5-benzyloxybenzoic acid 5-BENZYLOXY-2-BROMOBENZALDEHYDE

5-BENZYLOXY-2-BROMOBENZALDEHYDE

5-Bezyloxy-2-bromobenzaldehyde

Benzaldehyde, 2-bromo-5-(phenylmethoxy)-

2-Bromo-5-phenylmethoxybenzaldehyde

85604-06-4