2-BENZYL-5-METHOXY-1H-BENZO[D]IMIDAZOLE

Product Name: 2-BENZYL-5-METHOXY-1H-BENZO[D]IMIDAZOLE
CAS No.: 40608-76-2
Chemical Name: 2-BENZYL-5-METHOXY-1H-BENZO[D]IMIDAZOLE
Synonyms: 2-BENZYL-5-METHOXY-1H-BENZO[D]IMIDAZOLE;1H-Benzimidazole, 6-methoxy-2-(phenylmethyl)-
CBNumber: CB62454197
Molecular Formula: C15H14N2O
Formula Weight: 238.28
MOL File: 40608-76-2.mol

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2-BENZYL-5-METHOXY-1H-BENZO[D]IMIDAZOLE Property

storage temp.: Sealed in dry,Room Temperature
Appearance: Off-white to light yellow Solid

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

American Custom Chemicals Corporation

Product number: CHM0377264
Product name: 2-BENZYL-5-METHOXY-1H-BENZO[D]IMIDAZOLE
Purity: 95.00%
Packaging: 5MG
Price: $499.29
Updated: 2021/12/16

Ambeed

Product number: A157972
Product name: 2-Benzyl-5-methoxy-1H-benzo[d]imidazole
Purity: 97%
Packaging: 100mg
Price: $47
Updated: 2021/12/16

Ambeed

Product number: A157972
Product name: 2-Benzyl-5-methoxy-1H-benzo[d]imidazole
Purity: 97%
Packaging: 250mg
Price: $93
Updated: 2021/12/16

Alichem

Product number: 40608762
Product name: 2-Benzyl-5-methoxy-1H-benzo[d]imidazole
Packaging: 250mg
Price: $176.55
Updated: 2021/12/16

Chemenu

Product number: CM154828
Product name: 2-Benzyl-5-methoxy-1H-benzo[d]imidazole
Purity: 97%
Packaging: 1g
Price: $386
Updated: 2021/12/16

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2-BENZYL-5-METHOXY-1H-BENZO[D]IMIDAZOLE Chemical Properties,Usage,Production

Synthesis

103-82-2

102-51-2

40608-76-2

GENERAL METHOD: Under stirring conditions, 4-methoxy-o-phenylenediamine (1.85 mmol) was dissolved in xylene (10 mL), followed by the addition of phenylacetic acid (2.77 mmol) and boric acid (0.185 mmol). The reaction mixture was refluxed for 16 hours. After completion of the reaction, it was cooled to room temperature, the reaction mixture was concentrated under reduced pressure and diluted with ethyl acetate (50 mL). The organic phase was washed with saturated sodium bicarbonate solution (2 x 50 mL), dried over anhydrous sodium sulfate and subsequently concentrated under reduced pressure. Purification of the residue by silica gel column chromatography (eluent: 10-15% hexane solution of ethyl acetate) afforded 2-benzyl-5-methoxy-1H-benzo[d]imidazole (3u) in 67% yield; white solid; melting point 109-111 °C; IR (KBr) 3009, 2847, 1510, 1466, 1410, 1248, 1175, 1029, 775 cm^-1; 1H NMR (400 MHz, DMSO-d6) δ 12.04-12.14 (m, 1H), 7.18-7.44 (m, 6H), 6.91-7.07 (m, 1H), 6.70-6.79 (m, 1H), 4.12 (s, 2H), 3.75 (s, 3H); 13C NMR (100 MHz, DMSO-d6) δ 155.5, 137.9, 128.8, 128.5, 126.6, 118.7, 110.1, 101.3, 94.5, 55.4, 34.9; HRMS calculated value of C15H14N2O m/z 238.1182, measured value 238.1180.

References

[1] Bioorganic and Medicinal Chemistry, 2016, vol. 24, # 8, p. 1872 - 1878
[2] Zhurnal Obshchei Khimii, 1949, vol. 19, p. 1545,1550
[3] J. Gen. Chem. USSR (Engl. Transl.), 1949, vol. 19, p. 1555

2-BENZYL-5-METHOXY-1H-BENZO[D]IMIDAZOLE Preparation Products And Raw materials

Raw materials

Preparation Products

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2-BENZYL-5-METHOXY-1H-BENZO[D]IMIDAZOLE Suppliers

China 17 India 1 United States 3 Global 21

Shanghai Litong Chemical Technology Co.,Ltd.

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BePharm Ltd

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Zhejiang J&C Biological Technology Co.,Limited

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Zhengzhou Alpha Chemical Co. LTD

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Shanghai Haohong Pharmaceutical Co., Ltd.

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View Lastest Price from 2-BENZYL-5-METHOXY-1H-BENZO[D]IMIDAZOLE manufacturers

Zhejiang J&C Biological Technology Co.,Limited

Product: 2-BENZYL-5-METHOXY-1H-BENZO[D]IMIDAZOLE 40608-76-2
Price: US $0.00/gram
Min. Order: 1gram
Purity: 99%
Supply Ability: 10kg
Release date: 2022-02-17

40608-76-2, 2-BENZYL-5-METHOXY-1H-BENZO[D]IMIDAZOLERelated Search:

1,4-Epoxy-1H,3H-(1,4)oxazepino(4,3-a)benzimidazole, 4,5-dihydro-8-meth oxy-1-phenyl- 2-BENZYL-5-METHOXY-1H-BENZO[D]IMIDAZOLE

2-BENZYL-5-METHOXY-1H-BENZO[D]IMIDAZOLE

1H-Benzimidazole, 6-methoxy-2-(phenylmethyl)-

40608-76-2