ChemicalBook > CAS DataBase List > 4-CHLORO-3-IODOANILINE

4-CHLORO-3-IODOANILINE

Product Name: 4-CHLORO-3-IODOANILINE
CAS No.: 573764-31-5
Chemical Name: 4-CHLORO-3-IODOANILINE
Synonyms: 3-iodo-4-chloroaniline;4-CHLORO-3-IODOANILINE;4-Chloro-3-iodoaniline97%;4-Chloro-3-iodobenzenamine;4-Chloro-3-iodoaniline 97%;4-Chloro-3-iodo-phenylamine;BenzenaMine, 4-chloro-3-iodo-
CBNumber: CB62457259
Molecular Formula: C6H5ClIN
Formula Weight: 253.47
MOL File: 573764-31-5.mol

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4-CHLORO-3-IODOANILINE Property

Melting point:: 70 °C
Boiling point:: 322.3±27.0 °C(Predicted)
Density: 2.015±0.06 g/cm3(Predicted)
storage temp.: under inert gas (nitrogen or Argon) at 2–8 °C
form: solid
pka: 3.00±0.10(Predicted)
color: Brown to very dark brown

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Safety

HS Code: 2921420090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Danger

Hazard statements

H301Toxic if swalloed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

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N-Bromosuccinimide Price

TRC

Product number: C368798
Product name: 4-Chloro-3-iodoaniline
Packaging: 100mg
Price: $60
Updated: 2021/12/16

AK Scientific

Product number: 6136AJ
Product name: 4-Chloro-3-iodoaniline
Packaging: 25g
Price: $431
Updated: 2021/12/16

Apolloscientific

Product number: OR46038
Product name: 4-Chloro-3-iodoaniline
Purity: 97%
Packaging: 5g
Price: $507
Updated: 2021/12/16

SynQuest Laboratories

Product number: 3630-M-X1
Product name: 4-Chloro-3-iodoaniline
Packaging: 5G
Price: $559
Updated: 2021/12/16

Oakwood

Product number: 334410
Product name: 4-Chloro-3-iodoaniline
Purity: 95+%
Packaging: 5g
Price: $1500
Updated: 2021/12/16

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4-CHLORO-3-IODOANILINE Chemical Properties,Usage,Production

Synthesis

74534-15-9

573764-31-5

2) Preparation of 4-chloro-3-iodoaniline (compounds 1-4): a mixture of compounds 1-3 (37 g, 0.13 mol), iron powder (29.3 g, 0.52 mol), and NH4Cl (7 g, 0.13 mol) was dissolved in EtOH/H2O (200 mL/100 mL) and the reaction was stirred for 3 hr at 75 °C. Upon completion of the reaction, the reaction mixture was filtered and concentrated under reduced pressure to remove most of the EtOH. the remaining mixture was extracted with ethyl acetate, washed sequentially with water and saturated saline, and the organic phase was dried with anhydrous Na2SO4. After concentration under reduced pressure, 3-iodo-4-chloroaniline (compounds 1-4) was obtained as a yellow solid (32 g, 97% yield).LCMS: m/z 254.0 [M + 1]+.1H NMR (400 MHz, CDCl3): δ 3.65 (br, 2H), 6.58 (dd, J = 8.8 Hz, 2.4 Hz, 1H), 7.15-7.17 (m, 2H).

References

[1] Patent: US2014/18368, 2014, A1. Location in patent: Paragraph 0162; 0164
[2] European Journal of Medicinal Chemistry, 2017, vol. 141, p. 721 - 733
[3] Journal of the American Chemical Society, 2007, vol. 129, # 51, p. 15919 - 15926
[4] Journal of the Chemical Society, 1951, p. 1774,1778
[5] Bioorganic and Medicinal Chemistry Letters, 2009, vol. 19, # 19, p. 5576 - 5581

4-CHLORO-3-IODOANILINE Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 4-CHLORO-3-IODOANILINE manufacturers

Career Henan Chemical Co

Product: 4-chloro-3-iodoaniline 573764-31-5
Price: US $1.00/KG
Min. Order: 1KG
Purity: 98%
Supply Ability: 200kg
Release date: 2018-12-25

573764-31-5, 4-CHLORO-3-IODOANILINERelated Search:

2,4－difluoro-3-chloroaniline

4-CHLORO-3-IODOANILINE

4-Chloro-3-iodoaniline 97%

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4-Chloro-3-iodo-phenylamine

4-Chloro-3-iodoaniline97%

3-iodo-4-chloroaniline

4-Chloro-3-iodobenzenamine

573764-31-5