ChemicalBook > CAS DataBase List > 3-amino-5-(trifluoromethyl)benzonitrile

3-amino-5-(trifluoromethyl)benzonitrile

Product Name: 3-amino-5-(trifluoromethyl)benzonitrile
CAS No.: 49674-28-4
Chemical Name: 3-amino-5-(trifluoromethyl)benzonitrile
Synonyms: 3-Amino-5-(trifluoromethyl);3-Amino-5-(trifluoromethyl)benzonitrile98%;Benzonitrile, 3-aMino-5-(trifluoroMethyl)-;3-Amino-5-(trifluoromethyl)benzonitrile 98%;3-Amino-5-cyanobenzotrifluoride, 5-Cyano-alpha,alpha,alpha-trifluoro-m-toluidine
CBNumber: CB62473358
Molecular Formula: C8H5F3N2
Formula Weight: 186.13
MOL File: 49674-28-4.mol

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3-amino-5-(trifluoromethyl)benzonitrile Property

Boiling point:: 279.3±40.0 °C(Predicted)
Density: 1.37±0.1 g/cm3(Predicted)
storage temp.: under inert gas (nitrogen or Argon) at 2–8 °C
pka: 1.57±0.10(Predicted)
form: crystalline powder
color: Peachy tan

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Safety

HS Code: 2926907090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

Precautionary statements

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P332+P313IF SKIN irritation occurs: Get medical advice/attention.

P337+P313IF eye irritation persists: Get medical advice/attention.

P362Take off contaminated clothing and wash before reuse.

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N-Bromosuccinimide Price

TRC

Product number: A633570
Product name: 3-Amino-5-(trifluoromethyl)benzonitrile
Packaging: 100mg
Price: $60
Updated: 2021/12/16

SynQuest Laboratories

Product number: 3837-3-40
Product name: 3-Amino-5-(trifluoromethyl)benzonitrile
Purity: 98%
Packaging: 250mg
Price: $61
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FA105104
Product name: 3-amino-5-(trifluoromethyl)benzonitrile
Packaging: 100mg
Price: $80
Updated: 2021/12/16

AK Scientific

Product number: W6521
Product name: 3-Amino-5-trifluoromethylbenzonitrile
Packaging: 250mg
Price: $81
Updated: 2021/12/16

Apolloscientific

Product number: PC49080
Product name: 3-Amino-5-(trifluoromethyl)benzonitrile
Purity: 98%
Packaging: 1g
Price: $109
Updated: 2021/12/16

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3-amino-5-(trifluoromethyl)benzonitrile Chemical Properties,Usage,Production

Synthesis

20566-80-7

49674-28-4

General procedure for the synthesis of 3-amino-5-cyanobenzotrifluoride from 3-nitro-5-(trifluoromethyl)benzonitrile (432.0 mg, 2.0 mmol): to a solution of 3-nitro-5-(trifluoromethyl)benzylnitrile in ethanol (5 mL) was added zinc powder (1.3 mg, 20 mmol) and aqueous ammonium chloride solution (5 mL). The reaction mixture was stirred at 60°C for 14 hours. After completion of the reaction, the organic layer was separated by filtration and the filtrate was concentrated under reduced pressure. The crude product was partitioned between water (5 mL) and ethyl acetate (5 mL) and the aqueous layer was extracted with ethyl acetate (10 mL). The organic layers were combined, dried over anhydrous sodium sulfate and concentrated under reduced pressure to give a residue. The residue was purified by column chromatography (eluent: petroleum ether/ethyl acetate = 2:1) to give a yellow solid product (300.0 mg, 81% yield).LCMS (Method B): 2.33 min [MH]+=187.1.

References

[1] Patent: WO2016/127213, 2016, A1. Location in patent: Page/Page column 119-120
[2] Patent: WO2010/66684, 2010, A2. Location in patent: Page/Page column 64

3-amino-5-(trifluoromethyl)benzonitrile Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 3-amino-5-(trifluoromethyl)benzonitrile manufacturers

Shaanxi Dideu Medichem Co. Ltd

Product: 3-amino-5-(trifluoromethyl)benzonitrile 49674-28-4
Price: US $0.00-0.00/KG
Min. Order: 10mg
Purity: 99%HPLC
Supply Ability: 2000tons
Release date: 2020-01-13

Honest Joy Holdings Limited

Product: 3-Amino-5-trifluoromethylbenzonitrile 49674-28-4
Price: US $0.00/KG
Min. Order: 1KG
Purity: 98.9%
Supply Ability: 100 tons
Release date: 2022-01-14

Career Henan Chemical Co

Product: 3-amino-5-(trifluoromethyl)benzonitrile 49674-28-4
Price: US $1.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: 100KG
Release date: 2019-12-19

49674-28-4, 3-amino-5-(trifluoromethyl)benzonitrileRelated Search:

Benzonitrile, 3-aMino-5-(trifluoroMethyl)-

3-Amino-5-cyanobenzotrifluoride, 5-Cyano-alpha,alpha,alpha-trifluoro-m-toluidine

3-Amino-5-(trifluoromethyl)benzonitrile98%

3-Amino-5-(trifluoromethyl)

3-Amino-5-(trifluoromethyl)benzonitrile 98%

49674-28-4