2-Chloro-1,3-dimethoxy-benzene
- Product Name
- 2-Chloro-1,3-dimethoxy-benzene
- CAS No.
- 7051-15-2
- Chemical Name
- 2-Chloro-1,3-dimethoxy-benzene
- Synonyms
- 2-chloro-m-phenylene ether;2-Chloro-1,3-dimethoxy-benzene;Benzene, 2-chloro-1,3-dimethoxy-
- CBNumber
- CB62475918
- Molecular Formula
- C8H9ClO2
- Formula Weight
- 172.61
- MOL File
- 7051-15-2.mol
2-Chloro-1,3-dimethoxy-benzene Property
- Melting point:
- 69-71 °C(Solv: hexane (110-54-3))
- Boiling point:
- 233.7±20.0 °C(Predicted)
- Density
- 1.155±0.06 g/cm3(Predicted)
- storage temp.
- Sealed in dry,Room Temperature
- Appearance
- White to off-white Solid
Safety
- HS Code
- 2909309090
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- 0916AC
- Product name
- 2-Chloro-1,3-dimethoxybenzene
- Packaging
- 5g
- Price
- $597
- Updated
- 2021/12/16
- Product number
- HCH0357687
- Product name
- 2-CHLORO-1,3-DIMETHOXYBENZENE
- Purity
- 95.00%
- Packaging
- 5MG
- Price
- $503.49
- Updated
- 2021/12/16
- Product number
- SC-04260
- Product name
- 2-Chloro-1,3-dimethoxy-benzene
- Purity
- 95+%
- Packaging
- 10g
- Price
- $550
- Updated
- 2021/12/16
- Product number
- CD12041159
- Product name
- 2-Chloro-1,3-dimethoxybenzene
- Purity
- 98%
- Packaging
- 10g
- Price
- $653
- Updated
- 2021/12/16
- Product number
- 7051152
- Product name
- 2,6-Dimethoxychlorobenzene
- Packaging
- 500mg
- Price
- $839.45
- Updated
- 2021/12/16
2-Chloro-1,3-dimethoxy-benzene Chemical Properties,Usage,Production
Synthesis
6201-65-6
74-88-4
7051-15-2
General procedure: With reference to the method reported by An et al [1], 2-chloro-1,3-benzenediol (1.0 eq.) was dissolved in acetone (0.1 M), potassium carbonate (5.0 eq.) was added and stirred for 10 min. Subsequently, iodomethane (2.6 eq.) was added and the reaction mixture was stirred under reflux conditions for 16 hours. After completion of the reaction, it was cooled to room temperature, water was added and extracted three times with ether. The organic phases were combined, dried with anhydrous magnesium sulfate and concentrated under reduced pressure. The residue was purified by silica gel column chromatography to afford the target product 2-chloro-1,3-dimethoxybenzene (4c). 2-Chloro-1,3-dimethoxybenzene (4c): light yellow solid (76 mg, 0.44 mmol, 88% yield). Thin layer chromatography (TLC) (unfolding agent: hexane/ethyl acetate=10:1) Rf value was 0.38; infrared spectra (ATR) νmax: 3011 (w), 2966 (w), 2947 (w), 2840 (w), 1594 (m), 1472 (m), 1435 (m), 1299 (m), 1253 (m), 1191 (w). 1174 (w), 1099 (m), 1053 (m), 1025 (m), 849 (w), 764 (m), 709 (m), 654 (m), 597 (m) cm-1; UV-Vis spectra λmax (logε): 280 (3.08), 274 (3.10), 230 (3.79) nm.
References
[1] Beilstein Journal of Organic Chemistry, 2013, vol. 9, p. 2767 - 2777
2-Chloro-1,3-dimethoxy-benzene Preparation Products And Raw materials
Raw materials
Preparation Products
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