ChemicalBook > CAS DataBase List > 3-Ethynylpiperidine hydrochloride

3-Ethynylpiperidine hydrochloride

Product Name: 3-Ethynylpiperidine hydrochloride
CAS No.: 959918-19-5
Chemical Name: 3-Ethynylpiperidine hydrochloride
Synonyms: 3-ETHYNYLPIPERIDINE HCL;3-Ethynylpiperidine hydrochloride;Piperidine, 3-ethynyl-, hydrochloride (1:1)
CBNumber: CB62490050
Molecular Formula: C7H12ClN
Formula Weight: 145.63
MOL File: 959918-19-5.mol

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3-Ethynylpiperidine hydrochloride Property

storage temp.: under inert gas (nitrogen or Argon) at 2-8°C
Appearance: White to yellow Solid

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P321Specific treatment (see … on this label).

P332+P313IF SKIN irritation occurs: Get medical advice/attention.

P362Take off contaminated clothing and wash before reuse.

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N-Bromosuccinimide Price

TRC

Product number: E939510
Product name: 3-Ethynylpiperidinehydrochloride
Packaging: 50mg
Price: $110
Updated: 2021/12/16

AK Scientific

Product number: Y6534
Product name: 3-Ethynyl-piperidinehydrochloride
Packaging: 100mg
Price: $149
Updated: 2021/12/16

AK Scientific

Product number: Y6534
Product name: 3-Ethynyl-piperidinehydrochloride
Packaging: 250mg
Price: $192
Updated: 2021/12/16

Activate Scientific

Product number: AS40990
Product name: 3-Ethynylpiperidine HCl
Purity: 95%
Packaging: 250mg
Price: $229
Updated: 2021/12/16

Matrix Scientific

Product number: 119218
Product name: 3-Ethynylpiperidine hydrochloride
Purity: 95+%
Packaging: 250mg
Price: $389
Updated: 2021/12/16

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3-Ethynylpiperidine hydrochloride Chemical Properties,Usage,Production

Synthesis

664362-16-7

959918-19-5

General procedure for the synthesis of 3-ethynylpiperidine hydrochloride from 3-ethynylpiperidine-1-carboxylic acid tert-butyl ester: Preparation of Intermediate 35 (Method V); Synthesis of 3-ethynylpiperidine hydrochloride: to Intermediate 33 (1.50 g, 7.18 mmol) was added a dioxane solution (50 mL) of 4 M HCl. The reaction mixture was stirred at room temperature for 16 hours. After completion of the reaction, the mixture was concentrated in vacuum. The residue was ground with ether (Et2O) to give 3-alkynylpiperidine hydrochloride (0.91 g, 86% yield).1H NMR (DMSO-d6) δ: 9.02 (2H, br.s), 3.38-3.24 (1H, m), 3.21-3.08 (2H, m), 2.94-2.76 (3H, m), 2.00-1.87 (1H, m), 1.83-1.73 (1H, m), 1.73-1.60 (1H, m), 1.60-1.48 (1H, m).

References

[1] Patent: WO2007/141504, 2007, A1. Location in patent: Page/Page column 59
[2] Bioorganic and Medicinal Chemistry Letters, 2016, vol. 26, # 8, p. 1993 - 1996

3-Ethynylpiperidine hydrochloride Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 3-Ethynylpiperidine hydrochloride manufacturers

Career Henan Chemical Co

Product: 3-Ethynylpiperidine hydrochloride 959918-19-5
Price: US $1.00/g
Min. Order: 1g
Purity: 99%
Supply Ability: 200kg
Release date: 2019-12-26

959918-19-5, 3-Ethynylpiperidine hydrochlorideRelated Search:

3-Ethynylpiperidine hydrochloride

Piperidine, 3-ethynyl-, hydrochloride (1:1)

3-ETHYNYLPIPERIDINE HCL

959918-19-5

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