4-Fluoro-2-iodo-1-nitrobenzene

Product Name: 4-Fluoro-2-iodo-1-nitrobenzene
CAS No.: 41860-64-4
Chemical Name: 4-Fluoro-2-iodo-1-nitrobenzene
Synonyms: 4-Fluoro-2-iodonitrobenzene;2-iodo-4-fluoronitrobenzene;1-Fluoro-3-iodo-4-nitrobenzene;4-Fluoro-2-iodo-1-nitrobenzene;Benzene, 4-fluoro-2-iodo-1-nitro-;4-Fluoro-2-iodo-1-nitrobenzene 96%;4-Fluoro-2-iodo-1-nitrobenzene ,95%
CBNumber: CB62512024
Molecular Formula: C6H3FINO2
Formula Weight: 267
MOL File: 41860-64-4.mol

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4-Fluoro-2-iodo-1-nitrobenzene Property

Melting point:: 30 °C
Boiling point:: 148°C/20mmHg(lit.)
Density: 2.093±0.06 g/cm3(Predicted)
storage temp.: 2-8°C(protect from light)
form: powder to lump
color: Light yellow to Brown

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Safety

HS Code: 2904990090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

Precautionary statements

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P332+P313IF SKIN irritation occurs: Get medical advice/attention.

P337+P313IF eye irritation persists: Get medical advice/attention.

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N-Bromosuccinimide Price

TCI Chemical

Product number: F1178
Product name: 4-Fluoro-2-iodo-1-nitrobenzene
Purity: >98.0%(GC)
Packaging: 1g
Price: $34
Updated: 2025/07/31

TCI Chemical

Product number: F1178
Product name: 4-Fluoro-2-iodo-1-nitrobenzene
Purity: >98.0%(GC)
Packaging: 5g
Price: $122
Updated: 2025/07/31

TRC

Product number: F598818
Product name: 4-Fluoro-2-iodo-1-nitrobenzene
Packaging: 100mg
Price: $45
Updated: 2021/12/16

TRC

Product number: F598818
Product name: 4-Fluoro-2-iodo-1-nitrobenzene
Packaging: 500mg
Price: $65
Updated: 2021/12/16

TRC

Product number: F598818
Product name: 4-Fluoro-2-iodo-1-nitrobenzene
Packaging: 1g
Price: $75
Updated: 2021/12/16

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4-Fluoro-2-iodo-1-nitrobenzene Chemical Properties,Usage,Production

Synthesis

2369-11-1

41860-64-4

The general procedure for the synthesis of 2-iodo-4-fluoronitrobenzene from 5-fluoro-2-nitroaniline was as follows: 5-fluoro-2-nitroaniline (70.0 g, 448 mmol) was dissolved in 37% aqueous hydrochloric acid (350 mL) at 0 °C, and an aqueous solution of sodium nitrite (32.2 g, 469 mmol) was added slowly and dropwise (100 mL). The reaction mixture was stirred at 0 °C for 1 h. Subsequently, an aqueous solution of potassium iodide (82.0 g, 490 mmol) (100 mL) was added dropwise. The reaction mixture was continued to be stirred at room temperature for 2 hours. After completion of the reaction, the product was extracted with ethyl acetate. The organic layer was washed with saturated saline, dried over anhydrous magnesium sulfate and subsequently purified by fast column chromatography to afford the target product 2-iodo-4-fluoronitrobenzene (98.6 g, 368 mmol, 83% yield). The structure of the product was confirmed by 1H NMR (400 MHz, CDCl3): δ 7.15-7.23 (m, 1H), 7.75 (dd, J = 3.50 Hz, J = 7.60 Hz, 1H), 7.97 (dd, J = 1.6 Hz, J = 8.8 Hz, 1H).

References

[1] Patent: US2008/300242, 2008, A1. Location in patent: Page/Page column 63
[2] Organic Letters, 2010, vol. 12, # 8, p. 1696 - 1699

4-Fluoro-2-iodo-1-nitrobenzene Preparation Products And Raw materials

Raw materials

Preparation Products

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4-Fluoro-2-iodo-1-nitrobenzene Suppliers

Americas 1 China 66 Europe 1 India 4 Japan 1 United Kingdom 2 United States 7 Global 82

J & K SCIENTIFIC LTD.

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Xinyanhe Pharmatech Co.,Ltd

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View Lastest Price from 4-Fluoro-2-iodo-1-nitrobenzene manufacturers

Shaanxi Dideu Medichem Co. Ltd

Product: 4-Fluoro-2-iodo-1-nitrobenzene 41860-64-4
Price: US $0.00-0.00/KG
Min. Order: 10mg
Purity: 99%HPLC
Supply Ability: 2000tons
Release date: 2020-01-19

Career Henan Chemical Co

Product: 4-Fluoro-2-iodo-1-nitrobenzene 41860-64-4
Price: US $9.80/KG
Min. Order: 1KG
Purity: 97%-99%
Supply Ability: 1kg -1000kg
Release date: 2020-01-03

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