(1H-imidazol-4-yl)methanamine hydrochloride
- Product Name
- (1H-imidazol-4-yl)methanamine hydrochloride
- CAS No.
- 66247-84-5
- Chemical Name
- (1H-imidazol-4-yl)methanamine hydrochloride
- Synonyms
- (1H-Imidazol-4-yl);(1H-IMidazol-4-yl)MethanaMine, HCl;4-(Aminomethyl)imidazole Hydrochloride;(1H-Imidazol-5-yl)methanamine hydrochloride;(1H-imidazol-4-yl)methanamine hydrochloride
- CBNumber
- CB62522108
- Molecular Formula
- C4H8ClN3
- Formula Weight
- 133.57942
- MOL File
- 66247-84-5.mol
(1H-imidazol-4-yl)methanamine hydrochloride Property
- storage temp.
- under inert gas (nitrogen or Argon) at 2-8°C
- Appearance
- White to off-white Solid
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P302+P352IF ON SKIN: wash with plenty of soap and water.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P321Specific treatment (see … on this label).
P332+P313IF SKIN irritation occurs: Get medical advice/attention.
P362Take off contaminated clothing and wash before reuse.
N-Bromosuccinimide Price
- Product number
- I577328
- Product name
- (1H-Imidazol-4-yl)methanaminehydrochloride
- Packaging
- 250mg
- Price
- $75
- Updated
- 2021/12/16
- Product number
- W7724
- Product name
- (1H-Imidazol-4-yl)methanaminehydrochloride
- Packaging
- 5g
- Price
- $1110
- Updated
- 2021/12/16
- Product number
- 119061
- Product name
- (1H-Imidazol-4-yl)methanamine hydrochloride
- Purity
- 95+%
- Packaging
- 5g
- Price
- $1764
- Updated
- 2021/12/16
- Product number
- W7724
- Product name
- (1H-Imidazol-4-yl)methanaminehydrochloride
- Packaging
- 100mg
- Price
- $136
- Updated
- 2021/12/16
- Product number
- W7724
- Product name
- (1H-Imidazol-4-yl)methanaminehydrochloride
- Packaging
- 250mg
- Price
- $209
- Updated
- 2021/12/16
(1H-imidazol-4-yl)methanamine hydrochloride Chemical Properties,Usage,Production
Uses
(1H-Imidazol-4-yl)methanamine, HCl
Synthesis
3034-50-2
66247-84-5
General procedure for the synthesis of (1H-imidazol-4-yl)methanamine hydrochloride from 4-imidazolecarboxaldehyde: 12.0 g (124 mmol) of 4-formylimidazole was co-combined with 750 mg of nickel Nguyenne in a methanol solution of 1000 mL of ammonia, and oscillated for 30 min at 40 °C. Subsequently, the mixture was transferred to a Parr reactor and hydrogenated under hydrogen atmosphere at 5 bar pressure and 40 °C for 14 hours. Upon completion of the reaction, 750 mg of Ruanne nickel was added additionally and the mixture was hydrogenated again for 14 h at 50 °C, hydrogen atmosphere and 5 bar pressure. The reaction mixture was filtered and concentrated under reduced pressure. Methanol, toluene and ethanol were added sequentially to the residue and each addition was concentrated to dryness under reduced pressure. The residue was mixed with a methanolic solution of ether hydrochloric acid and again concentrated to dryness under reduced pressure. Finally, the residue was mixed with methanol and dichloromethane, respectively, and each time concentrated to dryness under reduced pressure. The product 21.2 g (quantitative yield) was obtained. rt value: 0.49 min (D). Molecular formula: C4H7N3-2HCl (molecular weight: 170.04 / 97.12). Mass spectral data: (M + H)+ = 98.
References
[1] Patent: US2008/51578, 2008, A1. Location in patent: Page/Page column 34
(1H-imidazol-4-yl)methanamine hydrochloride Preparation Products And Raw materials
Raw materials
Preparation Products
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