ChemicalBook > CAS DataBase List > 2-Amino-3-cyanopyridine-5-boronic Acid Pinacol Ester
2-Amino-3-cyanopyridine-5-boronic Acid Pinacol Ester
- Product Name
- 2-Amino-3-cyanopyridine-5-boronic Acid Pinacol Ester
- CAS No.
- 1246372-66-6
- Chemical Name
- 2-Amino-3-cyanopyridine-5-boronic Acid Pinacol Ester
- Synonyms
- 2-amino-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)nicotinonitrile;2-amino-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)pyridine-3-carbonitrile;3-Pyridinecarbonitrile, 2-amino-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-
- CBNumber
- CB62538385
- Molecular Formula
- C12H16BN3O2
- Formula Weight
- 245.09
- MOL File
- 1246372-66-6.mol
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2-Amino-3-cyanopyridine-5-boronic Acid Pinacol Ester Property
- storage temp.
- Keep in dark place,Inert atmosphere,Room temperature
- InChI
- InChI=1S/C12H16BN3O2/c1-11(2)12(3,4)18-13(17-11)9-5-8(6-14)10(15)16-7-9/h5,7H,1-4H3,(H2,15,16)
- InChIKey
- KRNXYPYYVHFVQS-UHFFFAOYSA-N
- SMILES
- C1(N)=NC=C(B2OC(C)(C)C(C)(C)O2)C=C1C#N
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Safety
- HS Code
- 2933399990
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N-Bromosuccinimide Price
American Custom Chemicals Corporation
- Product number
- BOR0006287
- Product name
- 2-AMINO-5-(4,4,5,5-TETRAMETHYL-1,3,2-DIOXABOROLAN-2-YL)NICOTINONITRILE
- Purity
- 95.00%
- Packaging
- 1G
- Price
- $592.2
- Updated
- 2021/12/16
AK Scientific
- Product number
- 3810DT
- Product name
- 2-Amino-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)nicotinonitrile
- Packaging
- 5g
- Price
- $2085
- Updated
- 2021/12/16
Crysdot
- Product number
- CD11316942
- Product name
- 2-Amino-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)nicotinonitrile
- Purity
- 95+%
- Packaging
- 5g
- Price
- $2176
- Updated
- 2021/12/16
Alichem
- Product number
- 1246372666
- Product name
- 2-Amino-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)nicotinonitrile
- Packaging
- 1g
- Price
- $684.52
- Updated
- 2021/12/16
Crysdot
- Product number
- CD11316942
- Product name
- 2-Amino-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)nicotinonitrile
- Purity
- 95+%
- Packaging
- 1g
- Price
- $724
- Updated
- 2021/12/16
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2-Amino-3-cyanopyridine-5-boronic Acid Pinacol Ester Chemical Properties,Usage,Production
Synthesis
2-amino-5-bromonicotinonitrile (50 g, 0.224 mol), bis (pinacolato) diboron (85.6 g, 0.337 mol), KOAc (44.1 g, 0.449 mol) and Pd (dppf) Cl2. CH2C12 (2.77 g, 3.4 mmol) was charged into a flask. Dioxane (400 mL) was added. The reaction mixture was stirred at 100 ℃ for 2 h under Ar. When LC-MS indicated that the reaction was completed, the mixture was cooled to room temperature. Subsequently, the mixture was filtered through diatomite, concentrated, diluted with a mixture of ethyl acetate and hexane (3:1, 1000 mL), filtered through silica gel (300-400 mesh), concentrated, crystallized and dried to give 2-Amino-3-cyanopyridine-5-boronic Acid Pinacol Ester (32 g, 66%) as a white solid.
2-Amino-3-cyanopyridine-5-boronic Acid Pinacol Ester Preparation Products And Raw materials
Raw materials
Preparation Products
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2-Amino-3-cyanopyridine-5-boronic Acid Pinacol Ester Suppliers
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View Lastest Price from 2-Amino-3-cyanopyridine-5-boronic Acid Pinacol Ester manufacturers
Career Henan Chemical Co
- Product
- 2-amino-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)nicotinonitrile 1246372-66-6
- Price
- US $2.00/KG
- Min. Order
- 1g
- Purity
- 98%min
- Supply Ability
- ask
- Release date
- 2020-01-08