5-Iodo-2-nitrophenol

Product Name: 5-Iodo-2-nitrophenol
CAS No.: 27783-55-7
Chemical Name: 5-Iodo-2-nitrophenol
Synonyms: 5-Iodo-2-nitrophenol;Phenol, 5-iodo-2-nitro-
CBNumber: CB62548111
Molecular Formula: C6H4INO3
Formula Weight: 265.01
MOL File: 27783-55-7.mol

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5-Iodo-2-nitrophenol Property

Melting point:: 96 °C
Boiling point:: 312.9±32.0 °C(Predicted)
Density: 2.176±0.06 g/cm3(Predicted)
storage temp.: 2-8°C(protect from light)
form: fine crystals
pka: 6.16±0.13(Predicted)
color: Bright lemon/yellow

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Safety

HS Code: 2908990000

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Danger

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H317May cause an allergic skin reaction

H318Causes serious eye damage

H410Very toxic to aquatic life with long lasting effects

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P270Do not eat, drink or smoke when using this product.

P272Contaminated work clothing should not be allowed out of the workplace.

P273Avoid release to the environment.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P333+P313IF SKIN irritation or rash occurs: Get medical advice/attention.

P391Collect spillage. Hazardous to the aquatic environment

P501Dispose of contents/container to..…

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N-Bromosuccinimide Price

Apolloscientific

Product number: OR400054
Product name: 5-Iodo-2-nitrophenol
Packaging: 1g
Price: $164
Updated: 2021/12/16

SynQuest Laboratories

Product number: 4654-H-10
Product name: 5-Iodo-2-nitrophenol
Packaging: 1g
Price: $192
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: HCH0367481
Product name: 5-IODO-2-NITROPHENOL
Purity: 95.00%
Packaging: 5MG
Price: $499.02
Updated: 2021/12/16

SynQuest Laboratories

Product number: 4654-H-10
Product name: 5-Iodo-2-nitrophenol
Packaging: 5G
Price: $600
Updated: 2021/12/16

Apolloscientific

Product number: OR400054
Product name: 5-Iodo-2-nitrophenol
Packaging: 5g
Price: $521
Updated: 2021/12/16

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5-Iodo-2-nitrophenol Chemical Properties,Usage,Production

Synthesis

626-02-8

27783-55-7

50590-07-3

General procedure for the synthesis of 5-iodo-2-nitrophenol and 3-iodo-4-nitrophenol from 3-iodophenol: 3.0 mL of fuming nitric acid (75 mmol) in 12 mL of glacial acetic acid was added slowly and dropwise to a 60 mL solution of glacial acetic acid containing 15.03 g (68.3 mmol) of 3-iodophenol over a 25-minute period, and the reaction flask was placed in an ice bath to cool. The reaction mixture was continued to be stirred at room temperature for 30 min, after which the reaction solution was decanted into ice water. The reaction mixture was concentrated under vacuum, dissolved in 150 mL of water and subsequently extracted with dichloromethane (2 x 300 mL). The combined organic phases were dried with anhydrous magnesium sulfate and concentrated to give 17 g of crude product. Separation by silica gel medium pressure chromatography (eluent ratio 1:2 ethyl acetate:hexane) afforded 3-iodo-4-nitrophenol (6.93 g, 26.1 mmol, 38% yield) with a melting point of 121-123 °C; 1H NMR (CDCl3, 300 MHz) δ 7.98 (d, 1H, J = 9 Hz), 7.54 (d, 1H, J = 3 Hz) , 6.92 (dd, 1H, J = 9, 3 Hz), 5.54 (bs, 1H); IR (KBr) ν 3150 (wide), 1600, 1580, 1512, 1404, 1336, 1298, 1212, 1121, 1023, 870 cm?1; and 3-iodo-6-nitrophenol (3.07 g, 11.6 mmol. 17% yield) with a melting point of 92-94 °C after recrystallization from dichloromethane/hexane (literature value 96 °C; Hodgson, HH et al., 1927); 1H NMR (CDCl3, 300 MHz) δ 10.53 (s, 1H), 7.76 (d, 1H, J = 9.0 Hz), 7.59 (d, 1H, J = 2.0 Hz), 7.33 ( dd, 1H, J = 9.0, 2.0 Hz); 13C NMR (CDCl3) δ 105.2 (C-3), 125.6 (C-5), 129.2 (C-2), 129.7 (C-4), 133.4 (C-6), 154.6 (C-1); IR (KBr) ν 3430 (broad), 1604, 1571, 1518, 1463, 1317, 1225, 1172, 1055, 888 cm?1; elemental analysis (C6H4INO3) calculated values: C, 27.19; H, 1.52; N, 5.29. measured values: C, 27.36; H, 1.57; N, 5.15.

References

[1] Tetrahedron, 2010, vol. 66, # 47, p. 9252 - 9262
[2] Bioorganic and Medicinal Chemistry, 2005, vol. 13, # 16, p. 4960 - 4971
[3] Patent: WO2005/95347, 2005, A1. Location in patent: Page/Page column 41
[4] Journal of the Chemical Society, 1927, p. 634
[5] Journal of the Chemical Society, 1925, vol. 127, p. 1602

5-Iodo-2-nitrophenol Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 5-Iodo-2-nitrophenol manufacturers

Career Henan Chemical Co

Product: 5-Iodo-2-nitrophenol 27783-55-7
Price: US $2.00/KG
Min. Order: 1KG
Purity: 98%MIN
Supply Ability: ASK
Release date: 2019-12-24

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