(5-BroMothiazol-2-yl)Methanol

Product Name: (5-BroMothiazol-2-yl)Methanol
CAS No.: 911052-85-2
Chemical Name: (5-BroMothiazol-2-yl)Methanol
Synonyms: 5-Bromo-2-thiazolemethanol;5-BroMothiazole-2-Methanol;2-Thiazolemethanol, 5-bromo-;(5-BroMothiazol-2-yl)Methanol;5-Bromo-2-(hydroxymethyl)thiazole;(5-Bromothiazol-2-yl)methanol?New;(5-bromo-1,3-thiazol-2-yl)methanol;5-Bromo-2-(hydroxymethyl)-1,3-thiazole;5-Bromo-2-(hydroxymethyl)-1,3-thiazole 95+%
CBNumber: CB62553795
Molecular Formula: C4H4BrNOS
Formula Weight: 194.05
MOL File: 911052-85-2.mol

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(5-BroMothiazol-2-yl)Methanol Property

Boiling point:: 277.6±20.0 °C(Predicted)
Density: 1.899±0.06 g/cm3(Predicted)
storage temp.: under inert gas (nitrogen or Argon) at 2–8 °C
pka: 12.74±0.10(Predicted)
Appearance: White to off-white Solid

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Safety

HS Code: 2934208090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P270Do not eat, drink or smoke when using this product.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P321Specific treatment (see … on this label).

P330Rinse mouth.

P332+P313IF SKIN irritation occurs: Get medical advice/attention.

P362Take off contaminated clothing and wash before reuse.

P501Dispose of contents/container to..…

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N-Bromosuccinimide Price

TRC

Product number: B712100
Product name: (5-Bromo-1,3-thiazol-2-yl)methanol
Packaging: 1g
Price: $45
Updated: 2021/12/16

AK Scientific

Product number: 5203AC
Product name: (5-Bromothiazol-2-yl)methanol
Packaging: 100mg
Price: $159
Updated: 2021/12/16

SynQuest Laboratories

Product number: 8H01-9-04
Product name: 5-Bromo-2-(hydroxymethyl)-1,3-thiazole
Packaging: 250mg
Price: $175
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: HCH0367149
Product name: (5-BROMOTHIAZOL-2-YL)METHANOL
Purity: 95.00%
Packaging: 5MG
Price: $495.46
Updated: 2021/12/16

SynQuest Laboratories

Product number: 8H01-9-04
Product name: 5-Bromo-2-(hydroxymethyl)-1,3-thiazole
Packaging: 1g
Price: $590
Updated: 2021/12/16

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(5-BroMothiazol-2-yl)Methanol Chemical Properties,Usage,Production

Synthesis

933752-44-4

911052-85-2

General procedure for the synthesis of 2-(hydroxymethyl)-5-bromothiazole using 5-bromothiazole-2-carboxaldehyde as starting material: a methanol (1.00 mL) solution of 5-bromothiazole-2-carboxaldehyde (0.100 g, 0.521 mmol) was slowly added dropwise to a methanol (2.0 mL) solution of sodium borohydride (0.030 g, 0.781 mmol) under stirring conditions. After the dropwise addition, the reaction mixture was allowed to stand at room temperature for 5 minutes, followed by continued stirring for 1 hour. Upon completion of the reaction, the solvent was removed by rotary evaporator under reduced pressure. The residue was dissolved and partitioned between ethyl acetate and water. After separation of the organic layer, the aqueous phase was further extracted with ethyl acetate. All organic layers were combined, dried with anhydrous magnesium sulfate, filtered and concentrated under reduced pressure to afford 2-(hydroxymethyl)-5-bromothiazole (0.067 g, 66% yield) as a dark-colored oil.LCMS analysis showed the [M + H]+ peak at 195.9.

References

[1] Patent: WO2012/149236, 2012, A1. Location in patent: Page/Page column 136
[2] Patent: WO2004/46101, 2004, A2. Location in patent: Page 31-32

(5-BroMothiazol-2-yl)Methanol Preparation Products And Raw materials

Raw materials

Preparation Products

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(5-BroMothiazol-2-yl)Methanol Suppliers

China 55 India 1 United Kingdom 1 United States 8 Global 65

PharmaBlock Sciences (Nanjing),Inc.

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911052-85-2