3-broMo-5-Methanesulfonylaniline

Product Name: 3-broMo-5-Methanesulfonylaniline
CAS No.: 62606-00-2
Chemical Name: 3-broMo-5-Methanesulfonylaniline
Synonyms: 3-broMo-5-Methanesulfonylaniline;3-BroMo-5-(Methylsulfonyl)aniline;3-Bromo-5-(methylsulphonyl)aniline;3-Bromo-5-(methylsulfonyl)benzenamine;3-Bromo-5-(methylsulphonyl)aniline 98%;Benzenamine, 3-bromo-5-(methylsulfonyl)-;3-bromo-5-methylsulfonyl-aniline - [B87119]
CBNumber: CB62595650
Molecular Formula: C7H8BrNO2S
Formula Weight: 250.11
MOL File: 62606-00-2.mol

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3-broMo-5-Methanesulfonylaniline Property

Boiling point:: 452.9±45.0 °C(Predicted)
Density: 1.671±0.06 g/cm3(Predicted)
storage temp.: Keep in dark place,Inert atmosphere,Room temperature
pka: 1.58±0.10(Predicted)
Appearance: White to yellow Solid

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Safety

HS Code: 2921420090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P280Wear protective gloves/protective clothing/eye protection/face protection.

P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.

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N-Bromosuccinimide Price

Biosynth Carbosynth

Product number: FB143485
Product name: 3-Bromo-5-(methylsulfonyl)aniline
Packaging: 50mg
Price: $80
Updated: 2021/12/16

SynQuest Laboratories

Product number: 8663-9-05
Product name: 3-Bromo-5-(methylsulfonyl)aniline
Packaging: 250mg
Price: $116
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FB143485
Product name: 3-Bromo-5-(methylsulfonyl)aniline
Packaging: 100mg
Price: $125
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FB143485
Product name: 3-Bromo-5-(methylsulfonyl)aniline
Packaging: 250mg
Price: $200
Updated: 2021/12/16

SynQuest Laboratories

Product number: 8663-9-05
Product name: 3-Bromo-5-(methylsulfonyl)aniline
Packaging: 1g
Price: $287
Updated: 2021/12/16

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3-broMo-5-Methanesulfonylaniline Chemical Properties,Usage,Production

Uses

3-Bromo-5-(methylsulfonyl)aniline is used in the preparation of WDR5-?MYC inhibitors.

Synthesis

62606-15-9

62606-00-2

General procedure for the synthesis of 3-bromo-5-(methylsulfonyl)aniline from 1-bromo-3-(methylsulfonyl)-5-nitrobenzene: 1-bromo-3-(methylsulfonyl)-5-nitrobenzene (100 mg, 0.4 mmol) was dissolved in tetrahydrofuran (THF, 10 mL). Raney nickel catalyst was added and the hydrogenation reaction was carried out under 1 bar hydrogen pressure. Upon completion of the reaction, the mixture was filtered to remove the catalyst and the filtrate was subsequently concentrated. 3-Bromo-5-(methylsulfonyl)aniline (30 mg, 0.16 mmol, 40% yield) was finally obtained as a yellow solid.

References

[1] Patent: EP1953163, 2008, A1. Location in patent: Page/Page column 13
[2] Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1977, p. 14 - 17

3-broMo-5-Methanesulfonylaniline Preparation Products And Raw materials

Raw materials

Preparation Products

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62606-00-2, 3-broMo-5-MethanesulfonylanilineRelated Search:

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62606-00-2