2,2,2-trifluoro-1-p-tolylethanol

Product Name: 2,2,2-trifluoro-1-p-tolylethanol
CAS No.: 446-65-1
Chemical Name: 2,2,2-trifluoro-1-p-tolylethanol
Synonyms: 2,2,2-trifluoro-1-p-tolylethano;2,2,2-trifluoro-1-p-tolylethanol;Benzenemethanol, 4-methyl-α-(trifluoromethyl)-;alpha-(Trifluoromethyl)-4-methylbenzyl Alcohol
CBNumber: CB62604594
Molecular Formula: C9H9F3O
Formula Weight: 190.16
MOL File: 446-65-1.mol

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2,2,2-trifluoro-1-p-tolylethanol Property

storage temp.: Keep in dark place,Sealed in dry,Room Temperature
Appearance: Colorless to off-white Solid-Liquid Mixture

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Safety

HS Code: 2906290090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC

Product number: T899393
Product name: 2,2,2-Trifluoro-1-(p-tolyl)ethanol
Packaging: 100mg
Price: $155
Updated: 2021/12/16

AK Scientific

Product number: 1839AL
Product name: 2,2,2-Trifluoro-1-(p-tolyl)ethanol
Packaging: 1g
Price: $172
Updated: 2021/12/16

Apolloscientific

Product number: PC201255
Product name: 2,2,2-Trifluoro-1-(p-tolyl)ethanol
Purity: 98%
Packaging: 1g
Price: $186
Updated: 2021/12/16

Apolloscientific

Product number: PC201255
Product name: 2,2,2-Trifluoro-1-(p-tolyl)ethanol
Purity: 98%
Packaging: 250mg
Price: $74
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: HCH0052309
Product name: 2,2,2-TRIFLUORO-1-(4-METHYLPHENYL)ETHANOL
Purity: 95.00%
Packaging: 1G
Price: $852.55
Updated: 2021/12/16

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2,2,2-trifluoro-1-p-tolylethanol Chemical Properties,Usage,Production

Synthesis

104-87-0

446-65-1

General procedure for the synthesis of 2,2,2-trifluoro-1-(p-tolyl)ethanol from p-toluylbenzaldehyde: 0.1 mL of a 1.0 M tetrahydrofuran solution of tetrabutylammonium fluoride was added to a 10 mL solution of THF containing 4-methylbenzaldehyde (1.2 g, 10 mmol) and TMSCF3 (1.8 mL, 12 mmol) at 0 °C. The reaction mixture was gradually warmed to room temperature and stirred continuously for 4 hours. Subsequently, the reaction mixture was treated with 12 mL of 1N HCl and stirring was continued overnight. After completion of the reaction, the product was extracted with ethyl acetate (3 x 20 mL). The organic layer was separated and dried with anhydrous sodium sulfate. Finally, the organic solvent was removed by evaporation to give 1.6 g of 1-(4-methylphenyl)-2,2,2-trifluoroethanol in 86% yield.

References

[1] Patent: US2009/5381, 2009, A1
[2] Patent: US2009/5382, 2009, A1
[3] Patent: US2009/29993, 2009, A1
[4] Journal of Organic Chemistry, 2013, vol. 78, # 2, p. 711 - 716
[5] Patent: WO2018/39386, 2018, A1. Location in patent: Page/Page column 288

2,2,2-trifluoro-1-p-tolylethanol Preparation Products And Raw materials

Raw materials

Preparation Products

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2,2,2-trifluoro-1-p-tolylethanol Suppliers

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View Lastest Price from 2,2,2-trifluoro-1-p-tolylethanol manufacturers

Shaanxi Dideu Medichem Co. Ltd

Product: 222-trifluoro-1-p-tolylethanol 446-65-1
Price: US $1.00-28.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: 20000KG
Release date: 2024-07-29

446-65-1, 2,2,2-trifluoro-1-p-tolylethanolRelated Search:

2,2,2-trifluoro-1-p-tolylethanol

alpha-(Trifluoromethyl)-4-methylbenzyl Alcohol

Benzenemethanol, 4-methyl-α-(trifluoromethyl)-

2,2,2-trifluoro-1-p-tolylethano

446-65-1