1-[(2-Bromophenyl)thio]-2,4-dimethylbenzene

Product Name: 1-[(2-Bromophenyl)thio]-2,4-dimethylbenzene
CAS No.: 960203-41-2
Chemical Name: 1-[(2-Bromophenyl)thio]-2,4-dimethylbenzene
Synonyms: VortioxetineImpurity63;Vortioxetine Hydrobromide impurity L;(2-Bromophenyl)(2,4-dimethylphenyl)sulfane;1-[(2-Bromophenyl)thio]-2,4-dimethylbenzene;1-(2-broMophenylsulfanyl)-2,4-diMethylbenzene;Benzene, 1-[(2-broMophenyl)thio]-2,4-diMethyl-
CBNumber: CB62614416
Molecular Formula: C14H13BrS
Formula Weight: 293.22
MOL File: 960203-41-2.mol

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1-[(2-Bromophenyl)thio]-2,4-dimethylbenzene Property

Boiling point:: 329.2±30.0 °C(Predicted)
Density: 1.40
storage temp.: 2-8°C
solubility: Chloroform (Sparingly), Methanol (Slightly)
form: Low-Melting Solid
color: White to Off-White

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

Precautionary statements

P280Wear protective gloves/protective clothing/eye protection/face protection.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

Ambeed

Product number: A235581
Product name: (2-Bromophenyl)(2,4-dimethylphenyl)sulfane
Purity: 97%
Packaging: 1g
Price: $30
Updated: 2021/12/16

Crysdot

Product number: CD12001427
Product name: (2-Bromophenyl)(2,4-dimethylphenyl)sulfane
Purity: 97%
Packaging: 10g
Price: $140
Updated: 2021/12/16

Ambeed

Product number: A235581
Product name: (2-Bromophenyl)(2,4-dimethylphenyl)sulfane
Purity: 97%
Packaging: 10g
Price: $145
Updated: 2021/12/16

Chemenu

Product number: CM256008
Product name: (2-Bromophenyl)(2,4-dimethylphenyl)sulfane
Purity: 95+%
Packaging: 10g
Price: $148
Updated: 2021/12/16

Alichem

Product number: 960203412
Product name: (2-Bromophenyl)(2,4-dimethylphenyl)sulfane
Packaging: 10g
Price: $150.8
Updated: 2021/12/16

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1-[(2-Bromophenyl)thio]-2,4-dimethylbenzene Chemical Properties,Usage,Production

Synthesis

583-55-1

94602-20-7

960203-41-2

100 g of S-(2,4-dimethylphenyl)ethylthioate was suspended in 500 ml of degassed toluene. Under nitrogen protection, Pd(dba)2 (3.25 g, 0.006 mol), rac-BINAP (6.4 g, 0.01 mol) and sodium tert-butoxide (62.5 g, 0.65 mol) were added sequentially. After warming the reaction mixture to 45-55 °C, 2-iodo-1-bromobenzene (165 g, 0.583 mol) was slowly added dropwise. Subsequently, the reaction system was warmed to 90-100 °C under nitrogen atmosphere and kept at this temperature for 3 hours. After completion of the reaction, it was cooled to room temperature, 400 ml of water was added and stirred for 15-20 minutes. After static layering, the organic phase was separated and concentrated under reduced pressure to give a viscous oily material, which was the target product (2-bromophenyl)(2,4-dimethylphenyl)thiolane (162 g, 100% yield).

References

[1] Patent: WO2016/135636, 2016, A1. Location in patent: Page/Page column 19

1-[(2-Bromophenyl)thio]-2,4-dimethylbenzene Preparation Products And Raw materials

Raw materials

Preparation Products

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1-[(2-Bromophenyl)thio]-2,4-dimethylbenzene Suppliers

China 71 India 1 United States 4 Global 76

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View Lastest Price from 1-[(2-Bromophenyl)thio]-2,4-dimethylbenzene manufacturers

Career Henan Chemical Co

Product: 1-[(2-Bromophenyl)thio]-2,4-dimethylbenzene 960203-41-2
Price: US $1.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: 100KG
Release date: 2018-08-08

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1-[(2-Bromophenyl)thio]-2,4-dimethylbenzene

Benzene, 1-[(2-broMophenyl)thio]-2,4-diMethyl-

1-(2-broMophenylsulfanyl)-2,4-diMethylbenzene

(2-Bromophenyl)(2,4-dimethylphenyl)sulfane

Vortioxetine Hydrobromide impurity L

VortioxetineImpurity63

960203-41-2