N-Methyl-N-isopropylsulfamoyl amide

ChemicalBook > CAS DataBase List > N-Methyl-N-isopropylsulfamoyl amide

N-Methyl-N-isopropylsulfamoyl amide

Product Name: N-Methyl-N-isopropylsulfamoyl amide
CAS No.: 372136-76-0
Chemical Name: N-Methyl-N-isopropylsulfamoyl amide
Synonyms: METHYL ISO PROPYL SULFAMIDE;N-isopropyl-N-methylsulfamide;N-Methyl-N-isopropylsulfamide;2-[methyl(sulfamoyl)amino]propane;N-Methyl-N-isopropylsulfamoyl amide;[METHYL(PROPAN-2-YL)SULFAMOYL]AMINE;N-Methyl-N-(1-methylethyl)sulfamide;SulfaMide, N-Methyl-N-(1-Methylethyl)-;N-methyl-N-(1-methylethyl)aminosulfonamide
CBNumber: CB62659701
Molecular Formula: C4H12N2O2S
Formula Weight: 152.22
MOL File: 372136-76-0.mol

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N-Methyl-N-isopropylsulfamoyl amide Property

Boiling point:: 238.7±23.0 °C(Predicted)
Density: 1.199±0.06 g/cm3(Predicted)
storage temp.: Sealed in dry,Room Temperature
solubility: Acetone; Dichloromethane; Methanol
pka: 12.40±0.60(Predicted)
form: Solid
color: White
InChI: InChI=1S/C4H12N2O2S/c1-4(2)6(3)9(5,7)8/h4H,1-3H3,(H2,5,7,8)
InChIKey: PJNPCKSPJXQBHH-UHFFFAOYSA-N
SMILES: S(N(C)C(C)C)(N)(=O)=O

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P321Specific treatment (see … on this label).

P332+P313IF SKIN irritation occurs: Get medical advice/attention.

P362Take off contaminated clothing and wash before reuse.

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N-Bromosuccinimide Price

TRC

Product number: I872708
Product name: N-Isopropyl-N-methylsulfamide
Packaging: 500mg
Price: $610
Updated: 2021/12/16

Activate Scientific

Product number: AS147134
Product name: N-Methyl-N-isopropylsulfamoylamide
Purity: 95%
Packaging: 5G
Price: $553
Updated: 2021/12/16

AK Scientific

Product number: 3943DA
Product name: [Methyl(propan-2-yl)sulfamoyl]amine
Packaging: 10g
Price: $2665
Updated: 2021/12/16

Crysdot

Product number: CD13014420
Product name: N-Methyl-N-isopropylsulfamoylamide
Purity: 95+%
Packaging: 5g
Price: $780
Updated: 2021/12/16

Ambeed

Product number: A841146
Product name: N-Methyl-N-isopropylsulfamoylamide
Purity: 95%
Packaging: 100mg
Price: $29
Updated: 2021/12/16

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N-Methyl-N-isopropylsulfamoyl amide Chemical Properties,Usage,Production

Uses

N-Isopropyl-N-methylsulfamide is an intermediate in the synthesis of unlabeled Saflufenacil-d7 (S081802). Saflufenacil-d7 is the labeled version of Saflufenacil (S081800), which is a herbicide of the pyrimidinedione chemical class used for the preplant burndown and selective preemergence dicot weed control in different field crops. It was found to inhibit protoporphyrinogen IX oxidase (PPO) enzyme.

Synthesis

Add 160g of ethanol to a 500ml four-necked flask, stir and cool to -5℃. Then, pass 18g (1.06mol) of ammonia gas, control the temperature at -5～0℃ and add 40g (0.23mol) of N-methyl-N-isopropylaminosulfonyl chloride at 0℃. After the addition is completed, keep warm for 1 hour, then control the vacuum of the reaction solution to -0.07MPa, the water bath temperature to 40℃, and concentrate under reduced pressure to dry solid. Add the solid to 120g of dichloromethane, stir at room temperature for 30 minutes to dissolve, and filter to obtain the filtrate. The filtrate is concentrated to dryness under reduced pressure at -0.07MPa and water bath temperature at 40℃ to obtain 33.7g of the product N-Methyl-N-isopropylsulfamoyl amide (HPLC purity 98.2%, yield 95%).

N-Methyl-N-isopropylsulfamoyl amide Preparation Products And Raw materials

Raw materials

Preparation Products

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372136-76-0, N-Methyl-N-isopropylsulfamoyl amideRelated Search:

SulfaMide, N-Methyl-N-(1-Methylethyl)-

N-isopropyl-N-methylsulfamide

N-Methyl-N-isopropylsulfamoyl amide

N-methyl-N-(1-methylethyl)aminosulfonamide

[METHYL(PROPAN-2-YL)SULFAMOYL]AMINE

2-[methyl(sulfamoyl)amino]propane

N-Methyl-N-isopropylsulfamide

N-Methyl-N-(1-methylethyl)sulfamide

METHYL ISO PROPYL SULFAMIDE

372136-76-0