2-(4-Methoxybenzyloxy)ethanol
- Product Name
- 2-(4-Methoxybenzyloxy)ethanol
- CAS No.
- 13807-89-1
- Chemical Name
- 2-(4-Methoxybenzyloxy)ethanol
- Synonyms
- 2-(4-Methoxybenzyloxy)ethanol;2-((4-methoxybenzyl)oxy)ethan-1-ol;2-[(4-methoxyphenyl)methoxy]ethanol;Ethanol, 2-[(4-methoxyphenyl)methoxy]-
- CBNumber
- CB62699556
- Molecular Formula
- C10H14O3
- Formula Weight
- 182.22
- MOL File
- 13807-89-1.mol
2-(4-Methoxybenzyloxy)ethanol Property
- Boiling point:
- 144 °C(Press: 4 Torr)
- Density
- 1.093±0.06 g/cm3(Predicted)
- storage temp.
- Sealed in dry,Room Temperature
- pka
- 14.36±0.10(Predicted)
- Appearance
- yellow oil
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- M335570
- Product name
- 2-(4-Methoxybenzyloxy)ethanol
- Packaging
- 100mg
- Price
- $330
- Updated
- 2021/12/16
- Product number
- 3821BB
- Product name
- 2-(4-Methoxybenzyloxy)ethanol
- Packaging
- 250mg
- Price
- $429
- Updated
- 2021/12/16
- Product number
- CD12146947
- Product name
- 2-((4-Methoxybenzyl)oxy)ethanol
- Purity
- 97%
- Packaging
- 5g
- Price
- $616
- Updated
- 2021/12/16
- Product number
- CM249150
- Product name
- 2-((4-Methoxybenzyl)oxy)ethanol
- Purity
- 97%
- Packaging
- 5g
- Price
- $617
- Updated
- 2021/12/16
- Product number
- 13807891
- Product name
- 2-((4-Methoxybenzyl)oxy)ethanol
- Packaging
- 5g
- Price
- $666.6
- Updated
- 2021/12/16
2-(4-Methoxybenzyloxy)ethanol Chemical Properties,Usage,Production
Synthesis
107-21-1
824-94-2
13807-89-1
The general procedure for the synthesis of 2-(4-methoxybenzyloxy)ethanol from ethylene glycol and 1-(chloromethyl)-4-methoxybenzene was as follows: potassium hydroxide (1.07 g, 19 mmol) was mixed with ethylene glycol (11 mL, 19 mmol), and the mixture was heated and stirred for 3 hours at 130 °C. Upon completion of the reaction, the mixture was cooled to room temperature, followed by the addition of 1-(chloromethyl)-4-methoxybenzene (3 g, 19 mmol). The reaction system was heated up to 350 °C under nitrogen protection for 16 hours. At the end of the reaction, water and ethyl acetate (EtOAc) were added to the system and the organic layer was separated. The organic layer was dried over anhydrous magnesium sulfate (MgSO4) and concentrated under reduced pressure. Purification was carried out by column chromatography (Redisep column), using ethyl acetate/cyclohexane as eluent, to give 2-(4-methoxybenzyloxy)ethanol as an oil. Yield: 2.26 g (66% yield).LC-MS (Method 2): retention time (Rt) 2.34 min, no molecular ion peak observed.
References
[1] Tetrahedron Letters, 2009, vol. 50, # 19, p. 2270 - 2273
[2] Angewandte Chemie - International Edition, 2009, vol. 48, # 49, p. 9346 - 9349
[3] Organic Letters, 2010, vol. 12, # 2, p. 384 - 387
[4] Chemistry - A European Journal, 2010, vol. 16, # 31, p. 9457 - 9461
[5] Journal of the American Chemical Society, 2016, vol. 138, # 7, p. 2190 - 2193
2-(4-Methoxybenzyloxy)ethanol Preparation Products And Raw materials
Raw materials
Preparation Products
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