ChemicalBook > CAS DataBase List > 1-(4-BROMO-PHENYL)-1H-PYRROLE

1-(4-BROMO-PHENYL)-1H-PYRROLE

Product Name
1-(4-BROMO-PHENYL)-1H-PYRROLE
CAS No.
5044-39-3
Chemical Name
1-(4-BROMO-PHENYL)-1H-PYRROLE
Synonyms
1-(4-BROMOPHENYL)PYRROLE;1H-Pyrrole,1-(4-bromophenyl)-;1-(4-BROMO-PHENYL)-1H-PYRROLE
CBNumber
CB6271361
Molecular Formula
C10H8BrN
Formula Weight
222.08
MOL File
5044-39-3.mol
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1-(4-BROMO-PHENYL)-1H-PYRROLE Property

Melting point:
91-92 °C
Boiling point:
283.0±23.0 °C(Predicted)
Density 
1.38±0.1 g/cm3(Predicted)
storage temp. 
Sealed in dry,Room Temperature
pka
-5.87±0.70(Predicted)
Appearance
Light yellow to brown Solid
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Safety

HazardClass 
IRRITANT
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H302Harmful if swallowed

H317May cause an allergic skin reaction

Precautionary statements

P280Wear protective gloves/protective clothing/eye protection/face protection.

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N-Bromosuccinimide Price

TRC
Product number
B698575
Product name
1-(4-Bromo-phenyl)-1H-pyrrole
Packaging
100mg
Price
$45
Updated
2021/12/16
TRC
Product number
B698575
Product name
1-(4-Bromo-phenyl)-1H-pyrrole
Packaging
500mg
Price
$65
Updated
2021/12/16
SynQuest Laboratories
Product number
3H32-9-59
Product name
1-(4-Bromophenyl)pyrrole
Purity
98%
Packaging
250mg
Price
$45
Updated
2021/12/16
SynQuest Laboratories
Product number
3H32-9-59
Product name
1-(4-Bromophenyl)pyrrole
Purity
98%
Packaging
1g
Price
$92
Updated
2021/12/16
Matrix Scientific
Product number
056930
Product name
1-(4-Bromophenyl)pyrrole
Purity
98%
Packaging
1g
Price
$92
Updated
2021/12/16
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1-(4-BROMO-PHENYL)-1H-PYRROLE Chemical Properties,Usage,Production

Synthesis

696-59-3

106-40-1

5044-39-3

GENERAL METHODS: 4-Bromoaniline (1 mmol), 2,5-dimethoxytetrahydrofuran (1.1 mmol) and L-(+)-tartaric acid-choline chloride low eutectic solvent (DES, 1.5 g) were added sequentially to a 50 mL round-bottomed flask and the reaction mixture was stirred at 90°C. The reaction was carried out by thin-layer chromatography (TLC). The reaction process was monitored by thin layer chromatography (TLC). After completion of the reaction, the reaction mixture was cooled to room temperature and the target product 1-(4-bromophenyl)-1H-pyrrole was extracted with ethyl acetate. The extract was subjected to rotary evaporation to remove the solvent and the residue was purified by silica gel column chromatography to obtain the pure product. The low eutectic solvent (DES) was dried under vacuum and reused for the next round of reaction.

References

[1] Synlett, 2009, # 14, p. 2245 - 2248
[2] Chemistry of Heterocyclic Compounds, 2014, vol. 49, # 12, p. 1732 - 1739
[3] Journal of Organic Chemistry, 2006, vol. 71, # 25, p. 9341 - 9347
[4] Tetrahedron, 2012, vol. 68, # 39, p. 8147 - 8155
[5] Synthetic Communications, 2012, vol. 42, # 16, p. 2471 - 2477

1-(4-BROMO-PHENYL)-1H-PYRROLE Preparation Products And Raw materials

Raw materials

Preparation Products

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1-(4-BROMO-PHENYL)-1H-PYRROLE Suppliers

Key Organics Limited/Bionet Research
Tel
--
Fax
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Email
enquiries@keyorganics.ltd.uk
Country
United Kingdom
ProdList
6663
Advantage
50
Fulcrum Scientific Ltd.
Tel
--
Fax
--
Country
United Kingdom
ProdList
6565
Advantage
38
Bio-Farma
Tel
--
Fax
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Email
sales@bio-farma.com
Country
United Kingdom
ProdList
4236
Advantage
55
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View Lastest Price from 1-(4-BROMO-PHENYL)-1H-PYRROLE manufacturers

Honest Joy Holdings Limited
Product
1-(4-Bromophenyl)pyrrole 5044-39-3
Price
US $0.00/KG
Min. Order
1KG
Purity
99.2%
Supply Ability
100 tons
Release date
2022-01-17