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Umbralisib

Product Name
Umbralisib
CAS No.
1532533-67-7
Chemical Name
Umbralisib
Synonyms
CS-2443;TGR1205;RP-5264;TGR-1202;Umbralisib;RP-5264 TGR-1202;RP5264;UMBRALISIB;TGR-1202(Umbralisib);Umbralisib (TGR-1202);RP5264; TGR1202; TGR 1202; RP-5264; RP 5264
CBNumber
CB62716383
Molecular Formula
C31H24F3N5O3
Formula Weight
571.55
MOL File
1532533-67-7.mol
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Umbralisib Property

Boiling point:
737.4±60.0 °C(Predicted)
Density 
1.43±0.1 g/cm3(Predicted)
storage temp. 
Store at -20°C
solubility 
DMF: 1 mg/ml; DMSO: 1 mg/ml
form 
solid
pka
3.79±0.30(Predicted)
color 
White to off-white
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
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N-Bromosuccinimide Price

TRC
Product number
R700975
Product name
RP5264
Packaging
2.5mg
Price
$85
Updated
2021/12/16
ChemScene
Product number
CS-5243
Product name
Umbralisib
Purity
98.55%
Packaging
5mg
Price
$120
Updated
2021/12/16
ChemScene
Product number
CS-5243
Product name
Umbralisib
Purity
98.55%
Packaging
10mg
Price
$220
Updated
2021/12/16
ChemScene
Product number
CS-5243
Product name
Umbralisib
Purity
98.55%
Packaging
25mg
Price
$440
Updated
2021/12/16
ChemScene
Product number
CS-5243
Product name
Umbralisib
Purity
98.55%
Packaging
50mg
Price
$580
Updated
2021/12/16
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Umbralisib Chemical Properties,Usage,Production

Description

Umbralisib (TGR-1202) tosylate is an orally active, potent and selective dual PI3Kδ and casein kinase-1-ε (CK1ε) inhibitor, with EC50 of 22.2 nM and 6.0 μM, respectively. Umbralisib tosylate exhibits unique immunomodulatory effects on chronic lymphocytic leukemia (CLL) T cells. Umbralisib tosylate can be used for haematological malignancies reseach. 

Uses

RP 5264 is a novel PI3K inhibitor that enhances Brentuximab Vedotin-induced lymphoma cell death.

brand name

Ukonig

General Description

Class: lipid kinase; Treatment: MZL, FL; Other name: TGR-1202; Elimination half-life = 91 h; Protein binding > 99.7%

Pharmacokinetics

Umbralisib has a prolonged half-life of 91 h, which enables once-daily dosing. However, the recommended dosage of 800 mg is the highest among all the PI3K inhibitors in use, presumably due to its limited oral bioavailability.

Synthesis

The synthesis of Umbralisib is as follows:
To a solution of intermediate 13 (0.134 g, 0.494 mmol) in THF (2.0 ml), intermediate 5 (0.150 g, 0.494 mmol) and triphenylphosphine (0.194 g, 0.741 mml) were added and stirred at RT for 5 min. Diisopropylazodicarboxylate ( 0.15 ml, 0.749 mmol) was added heated to 45°C. After 2h, the reaction mixture was quenched with with water and extracted with ethyl acetate. The organic layer was dried over sodium sulphate and concentrated under reduced pressure. The crude product was purified by column chromatography with ethyl acetate : petroleum ether to afford Umbralisib as an off-white solid (0.049 g, 20 %).

target

PI3Kδ, CK1ε

Umbralisib Preparation Products And Raw materials

Raw materials

Preparation Products

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Umbralisib Suppliers

A.J Chemicals
Tel
--
Fax
--
Email
sales@ajchem.in
Country
India
ProdList
6100
Advantage
58

1532533-67-7, UmbralisibRelated Search:


  • TGR-1202
  • RP-5264
  • RP-5264 TGR-1202
  • TGR1205
  • Umbralisib
  • Umbralisib (TGR-1202)
  • 4H-1-Benzopyran-4-one, 2-[(1S)-1-[4-amino-3-[3-fluoro-4-(1-methylethoxy)phenyl]-1H-pyrazolo[3,4-d]pyrimidin-1-yl]ethyl]-6-fluoro-3-(3-fluorophenyl)-
  • (S)-2-(1-(4-AMINO-3-(3-FLUORO-4-ISOPROPOXYPHENYL)-1H-PYRAZOLO[3,4-D]PYRIMIDIN-1-YL)ETHYL)-6-FLUORO-3-(3-FLUOROPHENYL)-4H-CHROMEN-4-ONE
  • RP5264;UMBRALISIB
  • CS-2443
  • RP5264; TGR1202; TGR 1202; RP-5264; RP 5264
  • TGR-1202(Umbralisib)
  • inhibit,RP-5264,lymphocytic leukemia,lymphoma,CLL T cells,Inhibitor,Umbralisib,haematological malignancies,cancer,orally active,PI3K,RP 5264,Phosphoinositide 3-kinase,Casein Kinase
  • 1532533-67-7