ChemicalBook > CAS DataBase List > N-[4-(2-CHLOROPROPANOYL)PHENYL]ACETAMIDE

N-[4-(2-CHLOROPROPANOYL)PHENYL]ACETAMIDE

Product Name: N-[4-(2-CHLOROPROPANOYL)PHENYL]ACETAMIDE
CAS No.: 81112-08-5
Chemical Name: N-[4-(2-CHLOROPROPANOYL)PHENYL]ACETAMIDE
Synonyms: N-[4-(2-CHLOROPROPANOYL)PHENYL]ACETAMIDE;Acetamide, N-[4-(2-chloro-1-oxopropyl)phenyl]-
CBNumber: CB6298528
Molecular Formula: C11H12ClNO2
Formula Weight: 225.67
MOL File: Mol file

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N-[4-(2-CHLOROPROPANOYL)PHENYL]ACETAMIDE Property

Melting point:: 119-120 °C(Solv: ethanol (64-17-5); water (7732-18-5))
Boiling point:: 429.9±25.0 °C(Predicted)
Density: 1.237±0.06 g/cm3(Predicted)
storage temp.: under inert gas (nitrogen or Argon) at 2-8°C
pka: 14.47±0.70(Predicted)

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Hazard and Precautionary Statements (GHS)

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N-Bromosuccinimide Price

TRC

Product number: C350925
Product name: N-[4-(2-Chloropropanoyl)phenyl]acetamide
Packaging: 500mg
Price: $155
Updated: 2021/12/16

AK Scientific

Product number: 7210AJ
Product name: N-[4-(2-Chloropropanoyl)phenyl]acetamide
Packaging: 1g
Price: $76
Updated: 2021/12/16

AK Scientific

Product number: 7210AJ
Product name: N-[4-(2-Chloropropanoyl)phenyl]acetamide
Packaging: 5g
Price: $114
Updated: 2021/12/16

AK Scientific

Product number: 7210AJ
Product name: N-[4-(2-Chloropropanoyl)phenyl]acetamide
Packaging: 10g
Price: $150
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: HCH0062010
Product name: N-[4-(2-CHLOROPROPANOYL)PHENYL]ACETAMIDE
Purity: 95.00%
Packaging: 1G
Price: $794.34
Updated: 2021/12/16

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N-[4-(2-CHLOROPROPANOYL)PHENYL]ACETAMIDE Chemical Properties,Usage,Production

Synthesis

7623-09-8

103-84-4

81112-08-5

a) Synthesis of 1-(4-acetamidophenyl)-2-chloropropanone: 118 g (0.93 mol) of 2-chloropropionyl chloride was added slowly and dropwise over a period of 1.5 h to a mixture containing 69.2 g (0.50 mol) of N-phenylacetamide and 525 mL of carbon disulfide. Subsequently, 205 g (1.50 mol) of aluminum chloride was added to the reaction system and the mixture was heated to reflux for 1 hour. Upon completion of the reaction, the supernatant was decanted and the residue was hydrolyzed with 1900 mL of ice water and 385 mL of 4N hydrochloric acid. The precipitate formed was separated by filtration and the precipitate was dissolved in benzene. The benzene solution was azeotropically distilled using a Dean-Stark apparatus to remove water. The hot solution was treated with activated carbon (CXA) and cooled to give 102.4 g (yield: 90.82%) of the target compound 1-(4-acetamidophenyl)-2-chloropropanone as a micron colored powder. Melting point (Kofler assay): 120°C.

References

[1] Organic Letters, 2017, vol. 19, # 10, p. 2548 - 2551
[2] Patent: US5128349, 1992, A
[3] Patent: US4677228, 1987, A
[4] Patent: WO2018/86703, 2018, A1. Location in patent: Page/Page column 200
[5] Tetrahedron Letters, 1981, vol. 22, # 43, p. 4305 - 4308

N-[4-(2-CHLOROPROPANOYL)PHENYL]ACETAMIDE Preparation Products And Raw materials

Raw materials

Preparation Products

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81112-08-5, N-[4-(2-CHLOROPROPANOYL)PHENYL]ACETAMIDERelated Search:

N-[4-(2-CHLOROPROPANOYL)PHENYL]ACETAMIDE

Acetamide, N-[4-(2-chloro-1-oxopropyl)phenyl]-

81112-08-5

811112-08-5